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公开(公告)号:US20240182316A1
公开(公告)日:2024-06-06
申请号:US18553099
申请日:2022-04-01
Applicant: IDEMITSU KOSAN CO.,LTD.
Inventor: Hideki YAMAMOTO , Futoshi UTSUNO , Daisuke MORI , Hiroyuki HIGUCHI
CPC classification number: C01D15/02 , B01D9/0018 , B01D61/44 , B01J19/245 , C01D15/08 , C25B3/07 , C25B15/08 , B01D2009/0086
Abstract: A method for producing a lithium compound, by which a high purity lithium compound can be produced from low-grade lithium carbonate containing impurities, such as salt water. The method includes: mixing lithium carbonate, an acid containing an organic acid, and water in a reaction tank 1 to produce an aqueous organic acid lithium solution containing an organic acid lithium; mixing the organic acid lithium and a metal hydroxide in a reaction tank 2 to produce an aqueous lithium hydroxide solution; and returning an organic acid, which is regenerated by using an electrochemical device from an organic acid metal by-produced by producing the aqueous lithium hydroxide solution to the reaction tank 1 and using the regenerated organic acid as the organic acid. An apparatus for producing a lithium compound, including the reaction tank 1, the reaction tank 2, the electrochemical device, and a return pipe, which each have a specific function.
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公开(公告)号:US20230378525A1
公开(公告)日:2023-11-23
申请号:US18030286
申请日:2021-10-08
Applicant: IDEMITSU KOSAN CO.,LTD.
Inventor: Kota TERAI , Katsuhito KONDO , Takeshi MAKINO , Atsushi SATO , Hiroyuki HIGUCHI
IPC: H01M10/0562
CPC classification number: H01M10/0562 , H01M2300/0068
Abstract: An object of the present invention is to provide sulfide solid electrolyte glass ceramics that have a high ionic conductivity and an enhanced water resistance, and is also to provide a method of producing the sulfide solid electrolyte glass ceramics. Sulfide solid electrolyte glass ceramics that have peaks at 20.2° and 23.6° in an X-ray diffractometry (XRD) using the CuKα line, a crystallite diameter of 30 nm or more, and a P2S64− phosphorus proportion obtained by a solid 31P-NMR spectroscopy of 4.5% by mol or less, and a method of producing the sulfide solid electrolyte glass ceramics are provided.
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公开(公告)号:US20240332603A1
公开(公告)日:2024-10-03
申请号:US18578874
申请日:2022-07-14
Inventor: Kota TERAI , Futoshi UTSUNO , Hiroyuki HIGUCHI , Kiyoharu TADANAGA , Akira MIURA , Nataly Carolina ROSERO NAVARRO
IPC: H01M10/0562 , C01B25/14
CPC classification number: H01M10/0562 , C01B25/14 , C01P2002/72 , C01P2002/82 , C01P2002/86 , C01P2006/40 , H01M2300/008
Abstract: Provided is a sulfide solid electrolyte that has a novel crystal structure and exhibits an ionic conductivity, the sulfide solid electrolyte containing a lithium atom, a phosphorus atom, a sulfur atom, and at least one kind of halogen atom selected from a chlorine atom and a bromine atom, and having a specific diffraction peak in powdery X-ray diffractometry using CuKα line, and a method for producing a sulfide solid electrolyte, the method including mixing a solvent 1 having a heteroatom and a raw material 1 containing specific atoms to prepare a mixture, preparing a solution that contains a raw material 2 containing a halogen atom and a solvent 2 having a heteroatom, mixing the mixture and the solution to prepare a fluid, and heating the fluid.
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公开(公告)号:US20230178794A1
公开(公告)日:2023-06-08
申请号:US17927451
申请日:2021-02-17
Applicant: IDEMITSU KOSAN CO.,LTD.
Inventor: Naoya MASUDA , Futoshi UTSUNO , Hiroyuki HIGUCHI
IPC: H01M10/0562 , H01M4/485
CPC classification number: H01M10/0562 , H01M4/485 , H01M2004/021
Abstract: To provide an electrode composite material that is excellent in conductivity through the excellent contact state of a solid electrolyte and an electrode active material, and is capable of exhibiting a high battery capability, containing the sulfide solid electrolyte and the electrode active material, having an electron conductivity parameter X represented by the prescribed expression satisfying 0.30≤X≤2.10.
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公开(公告)号:US20160036054A1
公开(公告)日:2016-02-04
申请号:US14781747
申请日:2014-03-26
Applicant: IDEMITSU KOSAN CO., LTD.
Inventor: Kazuaki YANAGI , Hiroyuki HIGUCHI , Hiromichi KOSHIKA , Shinichi KUROKAWA
IPC: H01M4/58 , H01M10/0562 , H01M10/0525 , H01M4/62
CPC classification number: H01M4/5815 , H01M4/136 , H01M4/1397 , H01M4/62 , H01M4/625 , H01M4/663 , H01M4/80 , H01M10/0525 , H01M10/0562 , H01M2220/30 , H01M2300/0068
Abstract: A composite material including an alkali metal sulfide, a conductive aid having fine pores and a solid electrolyte, wherein the alkali metal sulfide, the conductive aid and the solid electrolyte are aggregated and the half width of a peak of the alkali metal sulfide measured by X-ray diffraction is 1.0° or more.
Abstract translation: 包括碱金属硫化物,具有细孔的导电助剂和固体电解质的复合材料,其中所述碱金属硫化物,导电助剂和固体电解质被聚集,并且所述碱金属硫化物的峰的半值宽度由X 射线衍射为1.0°以上。
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公开(公告)号:US20240010813A1
公开(公告)日:2024-01-11
申请号:US18251966
申请日:2021-11-05
Inventor: Atsutaka KATO , Mari YAMAMOTO , Masanari TAKAHASHI , Futoshi UTSUNO , Hiroyuki HIGUCHI
IPC: C08K3/32 , C08L53/02 , H01M10/052 , H01M10/0562 , H01M4/13 , H01M4/62 , H01B1/10
CPC classification number: C08K3/32 , C08L53/02 , H01M10/052 , H01M10/0562 , H01M4/13 , H01M4/622 , H01B1/10 , C08L2207/04 , C08L2203/20 , H01M2300/0068
Abstract: A resin composition containing a compound including phosphorus and sulfur as constituent elements and having a disulfide bond, and a thermoplastic resin.
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公开(公告)号:US20220376291A1
公开(公告)日:2022-11-24
申请号:US17626939
申请日:2020-07-17
Inventor: Atsutaka KATO , Mari YAMAMOTO , Masanari TAKAHASHI , Futoshi UTSUNO , Hiroyuki HIGUCHI
IPC: H01M10/0562 , C01B25/14 , H01M4/62
Abstract: A compound comprising phosphorus atoms and sulfur atoms as constituent elements and having a peak in Raman spectroscopy, the peak being attributable to a disulfide bond bonding between two phosphorus atoms.
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公开(公告)号:US20170222261A1
公开(公告)日:2017-08-03
申请号:US15492564
申请日:2017-04-20
Applicant: IDEMITSU KOSAN CO., LTD.
Inventor: Takayoshi KAMBARA , Hiroyuki HIGUCHI , Hiroyuki TAMURA , Masaru NAKAGAWA , Tadanori JUNKE
IPC: H01M10/0562 , H01M4/131 , H01M4/485 , H01M10/0525
CPC classification number: H01M10/0562 , C03C3/321 , C03C3/323 , C03C4/14 , C03C10/0072 , H01B1/122 , H01M4/131 , H01M4/485 , H01M10/052 , H01M10/0525 , H01M2220/20 , H01M2220/30 , H01M2300/0068 , H01M2300/008 , Y02P70/54 , Y02T10/7011
Abstract: A solid electrolyte glass at least including: at least one alkali metal element; a phosphorus (P) element; a sulfur (S) element; and one or more halogen elements selected from I, Cl, Br and F; wherein the solid electrolyte glass has two exothermic peaks that are separated from each other in a temperature range of 150° C. to 350° C. as determined by differential scanning calorimetry (in a dry nitrogen atmosphere at a temperature-elevating speed of 10° C./min from 20 to 600° C.).
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公开(公告)号:US20240222633A1
公开(公告)日:2024-07-04
申请号:US18288221
申请日:2022-04-22
Inventor: Atsutaka KATO , Mari YAMAMOTO , Masanari TAKAHASHI , Futoshi UTSUNO , Hiroyuki HIGUCHI
IPC: H01M4/62 , C01B25/14 , H01M4/13 , H01M10/0562
CPC classification number: H01M4/621 , C01B25/14 , H01M4/13 , H01M10/0562 , C01P2002/72 , C01P2002/82 , C01P2002/85 , C01P2002/86 , C01P2006/40 , H01M2300/0068
Abstract: One of the purposes of the present invention is to provide: a compound which can be used as a binder having ion conductivity; and a battery which contains the compound. One aspect of the present invention is a compound comprising P and S as constituent elements, a group comprising one or more elements selected from the group consisting of O, N and halogen, the group bonding to the P, and a disulfide bond.
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公开(公告)号:US20170194662A1
公开(公告)日:2017-07-06
申请号:US15442800
申请日:2017-02-27
Applicant: IDEMITSU KOSAN CO., LTD
Inventor: Takayoshi KAMBARA , Tadanori JUNKE , Ryo ABURATANI , Hiroyuki HIGUCHI , Masaru NAKAGAWA , Tsuyoshi OTA , Yoshikatsu Seino
IPC: H01M10/0562 , C03C10/16 , H01B1/12 , H01M10/0525
CPC classification number: H01M10/0562 , C03C10/16 , C03C2205/00 , H01B1/122 , H01M10/052 , H01M10/0525 , H01M10/054 , H01M2300/0068 , H01M2300/008
Abstract: A solid electrolyte including an alkali metal element, phosphorous, sulfur and halogen as constituent components.
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