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公开(公告)号：US08541485B2
公开(公告)日：2013-09-24
申请号：US13263283
申请日：2010-05-24
申请人： James M. Nelson , Matthew N. Archibald , Wendy L. Thompson , Jeremy A. Miller , Randy A. Larson , Terence D. Spawn
发明人： James M. Nelson , Matthew N. Archibald , Wendy L. Thompson , Jeremy A. Miller , Randy A. Larson , Terence D. Spawn
CPC分类号： B01J19/1887 , B01D1/222 , B01J19/1862 , B01J19/2415 , B01J2219/0004 , B01J2219/00094 , B01J2219/00765 , C08J3/2053 , C08J3/215
摘要： A method of making a filled resin includes the steps of: Providing a wiped film evaporator with an internal evaporator chamber maintained under vacuum and having an internal chamber wall maintained at an elevated temperature; introducing solvent-borne particles and organic matrix into the internal chamber; and compounding the solvent-borne particles and the organic matrix in the internal evaporator chamber by forming a thin film against the internal chamber wall, the thin film including organic matrix and particles, and the vacuum conditions and elevated temperature being sufficient to remove solvent from the particles and organic matrix to provide the filled resin. Less than about 10% of the particles in the resulting filled resin are agglomerated.
摘要翻译： 制造填充树脂的方法包括以下步骤：提供具有保持在真空下并具有保持在升高的温度下的内部室壁的内部蒸发器室的擦拭膜蒸发器; 将溶剂型颗粒和有机基质引入内室; 并通过在内部室壁上形成薄膜来将溶剂型颗粒和有机基质混合在内部蒸发器室中，该薄膜包括有机基质和颗粒，并且真空条件和升高的温度足以从 颗粒和有机基质提供填充树脂。 所得填充树脂中少于约10％的颗粒团聚。
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公开(公告)号：US20110048923A1
公开(公告)日：2011-03-03
申请号：US12988092
申请日：2009-04-17
CPC分类号： C09C3/12 , B82Y30/00 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/22 , C09C1/043 , C09C1/3081 , C09C1/346 , C09C1/3684 , C09C1/407 , C09C1/62 , C09C3/08 , C09C3/10
摘要： A method for the preparation of functionalized particles includes providing a feedstock made of particles, a surface treatment agent reactive with the particles, and solvent. The feedstock is exposed to microwave radiation to heat the feedstock and react the particles with the surface treatment agent to provide the functionalized particles in less than about 60 minutes.
摘要翻译： 制备官能化颗粒的方法包括提供由颗粒制成的原料，与颗粒反应的表面处理剂和溶剂。 将原料暴露于微波辐射以加热原料并使颗粒与表面处理剂反应，以在小于约60分钟内提供官能化颗粒。
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公开(公告)号：US08487019B2
公开(公告)日：2013-07-16
申请号：US12933526
申请日：2009-03-26
申请人： James M. Nelson , Matthew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
发明人： James M. Nelson , Matthew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
CPC分类号： C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
摘要： A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix.
摘要翻译： 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂，使得官能化颗粒占填充树脂的至少约20重量％。 提供官能化颗粒的步骤还可以包括提供（i）未处理颗粒的原料，（ii）与颗粒反应的表面处理剂，和（iii）溶剂，并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面，成品树脂包含至少约20重量％的有机基质中的官能化颗粒。
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公开(公告)号：US20110021797A1
公开(公告)日：2011-01-27
申请号：US12933741
申请日：2009-03-26
申请人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, JR.
发明人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, JR.
IPC分类号： C07F7/02
CPC分类号： C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
摘要： A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
摘要翻译： 制备官能化颗粒的方法包括提供包含颗粒的原料，与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器，由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号：US08394977B2
公开(公告)日：2013-03-12
申请号：US12933741
申请日：2009-03-26
申请人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, Jr.
发明人： Grant F. Tiefenbruck , Matthew N. Archibald , James M. Nelson , Wendy L. Thompson , William J. Schultz , Peter D. Condo , Brant U. Kolb , Jimmie R. Baran, Jr.
IPC分类号： C07F7/00
CPC分类号： C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
摘要： A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
摘要翻译： 制备官能化颗粒的方法包括提供包含颗粒的原料，与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器，由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号：US08318120B2
公开(公告)日：2012-11-27
申请号：US12988092
申请日：2009-04-17
CPC分类号： C09C3/12 , B82Y30/00 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/22 , C09C1/043 , C09C1/3081 , C09C1/346 , C09C1/3684 , C09C1/407 , C09C1/62 , C09C3/08 , C09C3/10
摘要： A method for the preparation of functionalized particles includes providing a feedstock made of particles, a surface treatment agent reactive with the particles, and solvent. The feedstock is exposed to microwave radiation to heat the feedstock and react the particles with the surface treatment agent to provide the functionalized particles in less than about 60 minutes.
摘要翻译： 制备官能化颗粒的方法包括提供由颗粒制成的原料，与颗粒反应的表面处理剂和溶剂。 将原料暴露于微波辐射以加热原料并使颗粒与表面处理剂反应，以在小于约60分钟内提供官能化颗粒。
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公开(公告)号：US09221970B2
公开(公告)日：2015-12-29
申请号：US13133878
申请日：2009-12-17
申请人： William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
发明人： William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
IPC分类号： C08L63/00
CPC分类号： C08L63/00
摘要： Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin, and to coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
摘要翻译： 描述了包含分散在可固化树脂中的表面改性纳米碳酸钙颗粒的组合物，以及包含这种组合物的涂料和纤维复合材料。 表面改性剂包括与方解石离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂也可以包括能够与可固化树脂反应的反应性基团。 还描述了制备纳米碳酸钙复合材料和涂覆由这种纳米碳酸钙复合材料制备的纤维复合材料的方法。
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公开(公告)号：US20110028605A1
公开(公告)日：2011-02-03
申请号：US12933526
申请日：2009-03-26
申请人： James M. Nelson , Matthrew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
发明人： James M. Nelson , Matthrew N. Archibald , Brant U. Kolb , Wendy L. Thompson , William J. Schultz , Steven C. Hackett
CPC分类号： C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
摘要： A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix.
摘要翻译： 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂，使得官能化颗粒占填充树脂的至少约20重量％。 提供官能化颗粒的步骤还可以包括提供（i）未处理颗粒的原料，（ii）与颗粒反应的表面处理剂，和（iii）溶剂，并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面，成品树脂包含至少约20重量％的有机基质中的官能化颗粒。
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公开(公告)号：US20110245376A1
公开(公告)日：2011-10-06
申请号：US13133878
申请日：2009-12-17
申请人： William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
发明人： William J. Schultz , Chad A. Haraldson , Nathan E. Schultz , Wendy L. Thompson , James E. Thorson , Douglas P. Goetz , Steven C. Hackett , James M. Nelson
CPC分类号： C08L63/00
摘要： Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin, and to coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
摘要翻译： 描述了包含分散在可固化树脂中的表面改性纳米碳酸钙颗粒的组合物，以及包含这种组合物的涂料和纤维复合材料。 表面改性剂包括与方解石离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂也可以包括能够与可固化树脂反应的反应性基团。 还描述了制备纳米碳酸钙复合材料和涂覆由这种纳米碳酸钙复合材料制备的纤维复合材料的方法。
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10.发明授权公开(公告)号：US08659221B2
公开(公告)日：2014-02-25
申请号：US13218610
申请日：2011-08-26
申请人： Vivian W. Jones , Sergey A. Lamansky , James M. Nelson , Ha T. Le
发明人： Vivian W. Jones , Sergey A. Lamansky , James M. Nelson , Ha T. Le
CPC分类号： B82Y20/00 , G02B6/0053 , H01L51/504 , H01L51/5271 , H01L51/5275
摘要： A light extraction film having multi-periodic zones of engineered nanostructures. The light extraction film includes a flexible substrate, a layer of low index engineered nanostructures applied to the substrate, and a high index backfill layer applied over the nanostructures. The multi-periodic zones include a repeating zone of the nanostructures having multi-periodic characteristics. The repeating zone includes first and second sets of nanostructures having different periodic pitches. The multi-periodic zones can be used to enhance the light output and tune the angular luminosity of organic light emitting diode devices.
摘要翻译： 具有工程纳米结构多周期区的光萃取膜。 光提取膜包括柔性基底，施加到基底的低折射率工程纳米结构层，以及施加在纳米结构上的高指数回填层。 多周期区域包括具有多周期特性的纳米结构的重复区域。 重复区包括具有不同周期性间距的第一和第二组纳米结构。 多周期区域可用于增强光输出并调节有机发光二极管器件的角度发光度。
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