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1.发明申请PROCESS FOR CONTINUOUSLY PREPARING METHYL MERCAPTAN FROM CARBON COMPOUNDS, SULFUR AND HYDROGEN 有权从碳化合物，硫和氢气中连续制备甲基丙烯酸的方法公开(公告)号：US20110015443A1
公开(公告)日：2011-01-20
申请号：US12837017
申请日：2010-07-15
申请人： Jan-Olaf Barth , Christoph Weckbecker , Hubert Redlingshöefer , Johannes A. Lercher , Christoph Kaufmann
发明人： Jan-Olaf Barth , Christoph Weckbecker , Hubert Redlingshöefer , Johannes A. Lercher , Christoph Kaufmann
IPC分类号： C07C319/08 , C07C319/06 , C07C319/28
CPC分类号： C07C319/02 , C01B17/161 , C07C319/08 , Y02P20/127 , Y02P20/582 , C07C321/04
摘要： The invention relates to a process for continuously preparing methyl mercaptan by reacting a mixture comprising carbon compounds with sulfur and hydrogen, wherein the carbon disulfide and hydrogen sulfide compounds which form are subsequently converted to methyl mercaptan.
摘要翻译： 本发明涉及通过使包含碳化合物的混合物与硫和氢反应连续制备甲基硫醇的方法，其中形成的二硫化碳和硫化氢化合物随后转化成甲硫醇。
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2.发明授权公开(公告)号：US09745262B2
公开(公告)日：2017-08-29
申请号：US12837017
申请日：2010-07-15
申请人： Jan-Olaf Barth , Christoph Weckbecker , Hubert Redlingshoefer , Johannes A. Lercher , Christoph Kaufmann
发明人： Jan-Olaf Barth , Christoph Weckbecker , Hubert Redlingshoefer , Johannes A. Lercher , Christoph Kaufmann
IPC分类号： C07C319/08 , C07C319/06 , C07C319/28 , C07C319/02 , C01B17/16
CPC分类号： C07C319/02 , C01B17/161 , C07C319/08 , Y02P20/127 , Y02P20/582 , C07C321/04
摘要： The invention relates to a process for continuously preparing methyl mercaptan by reacting a mixture comprising carbon compounds with sulfur and hydrogen, wherein the carbon disulfide and hydrogen sulfide compounds which form are subsequently converted to methyl mercaptan.
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公开(公告)号：US20060229474A1
公开(公告)日：2006-10-12
申请号：US11278894
申请日：2006-04-06
IPC分类号： C07C319/08
CPC分类号： C07C319/08 , C07C321/04
摘要： The invention relates to a process for the continuous production of methylmercaptan by reacting a starting gas mixture of methanol and hydrogen sulphide in the gas phase at a reaction temperature between 200 and 600° C. and an operating pressure of 1.5 to 40 bar on a catalyst in a multi-bed reactor.
摘要翻译： 本发明涉及一种通过在气相中在甲醇和硫化氢的起始气体混合物在200-600℃的反应温度和1.5至40巴的操作压力下在催化剂上连续生产甲基硫醇的方法。 在多床反应器中。
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4.发明授权公开(公告)号：US07994366B2
公开(公告)日：2011-08-09
申请号：US12126322
申请日：2008-05-23
申请人： Jan-Olaf Barth , Hubert Redlingshoefer , Caspar-Heinrich Finkeldei , Christoph Weckbecker , Klaus Huthmacher
发明人： Jan-Olaf Barth , Hubert Redlingshoefer , Caspar-Heinrich Finkeldei , Christoph Weckbecker , Klaus Huthmacher
IPC分类号： C07C321/00
CPC分类号： C07C319/02 , B01J21/063 , B01J23/28 , B01J23/34 , B01J23/36 , B01J37/0205 , Y02P20/127 , C07C321/04
摘要： Provided is a process for continuously preparing methyl mercaptan by reacting a reactant mixture comprising solid, liquid and/or gaseous carbon- and/or hydrogen-containing compounds with air or oxygen, and/or water and sulfur.
摘要翻译： 本发明提供一种通过使含有固体，液体和/或气态的含碳和/或含氢化合物的反应物混合物与空气或氧气和/或水和硫反应来连续制备甲硫醇的方法。
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公开(公告)号：US20100041548A1
公开(公告)日：2010-02-18
申请号：US12509120
申请日：2009-07-24
申请人： Yiquan YANG , Qi Wang , Renchun Lin , Hongbin Zhang , Youzhu Yuan , Weiping Fang , Quanxing Zheng , Shenjun Dai , Xingguo Yan , Aiping Chen , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher , Hubert Redlingshöfer , Sabine Ackermann
发明人： Yiquan YANG , Qi Wang , Renchun Lin , Hongbin Zhang , Youzhu Yuan , Weiping Fang , Quanxing Zheng , Shenjun Dai , Xingguo Yan , Aiping Chen , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher , Hubert Redlingshöfer , Sabine Ackermann
CPC分类号： B01J37/0203 , B01J23/28 , B01J23/8872 , B01J37/0201 , C07C319/02 , Y02P20/582 , C07C321/04
摘要： The present invention refers to a continuous process for the manufacture of methyl mercaptan using Mo—O—K-based catalysts. It is further described that the total selectivity of methylmercaptan can be increased by at least 1% by lowering the total gas hourly space velocity. The invention further refers to a process for the preparation of a solid, preformed catalyst system.
摘要翻译： 本发明涉及使用Mo-O-K系催化剂制造甲硫醇的连续方法。 进一步描述的是，通过降低总气体时空速度，甲基硫醇的总选择性可以增加至少1％。 本发明还涉及制备固体预成型催化剂体系的方法。
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公开(公告)号：US07569731B2
公开(公告)日：2009-08-04
申请号：US10595333
申请日：2004-09-29
申请人： Yiquan Yang , Qi Wang , Renchun Lin , Hongbin Zhang , Youzhu Yuan , Weiping Fang , Quanxing Zheng , Shenjun Dai , Xingguo Yan , Aiping Chen , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher , Hubert Redlingshöfer , Sabine Ackermann
发明人： Yiquan Yang , Qi Wang , Renchun Lin , Hongbin Zhang , Youzhu Yuan , Weiping Fang , Quanxing Zheng , Shenjun Dai , Xingguo Yan , Aiping Chen , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher , Hubert Redlingshöfer , Sabine Ackermann
IPC分类号： C07C319/16
CPC分类号： B01J37/0203 , B01J23/28 , B01J23/8872 , B01J37/0201 , C07C319/02 , Y02P20/582 , C07C321/04
摘要： The present invention refers to a continuous process for the manufacture of methyl mercaptan using Mo—O—K-based catalysts. It is further described that the total selectivity of methylmercaptan can be increased by at least 1% by lowering the total gas hourly space velocity. The invention further refers to a process for the preparation of a solid, preformed catalyst system.
摘要翻译： 本发明涉及使用Mo-O-K系催化剂制造甲硫醇的连续方法。 进一步描述的是，通过降低总气体时空速度，甲基硫醇的总选择性可以增加至少1％。 本发明还涉及制备固体预成型催化剂体系的方法。
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公开(公告)号：US20060243342A1
公开(公告)日：2006-11-02
申请号：US11399451
申请日：2006-04-07
申请人： Jan-Olaf Barth , Achim Fischer , Wolfgang Bock , Werner Burkhardt , Christoph Weckbecker , Klaus Huthmacher
发明人： Jan-Olaf Barth , Achim Fischer , Wolfgang Bock , Werner Burkhardt , Christoph Weckbecker , Klaus Huthmacher
IPC分类号： B65B1/20
CPC分类号： B01J8/003 , B01J8/06 , B01J2208/00752
摘要： The invention relates to a method for filling apparatuses for chemical production with solids using a controllable metering device, and an apparatus, displaceable from place to place, for carrying out the method. The apparatus is suitable in particular for filling heat exchangers, absorption columns, distillation columns or tube-bundle reactors with solids.
摘要翻译： 本发明涉及一种用于使用可控计量装置填充具有固体的化学品生产装置的方法，以及用于执行该方法的可移位的装置。 该装置特别适用于填充具有固体的热交换器，吸收塔，蒸馏塔或管束反应器。
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8.发明授权Supported Mo—O—K—MexOy catalyst for the synthesis of methanethiol from high H2S-containing syngas 有权支持的Mo-O-K-Mex用于从高H 2 S的合成气合成甲硫醇的催化剂公开(公告)号：US09409153B2
公开(公告)日：2016-08-09
申请号：US12810688
申请日：2008-11-28
申请人： Yiquan Yang , Yingjuan Hao , Aiping Chen , Qi Wang , Lingmei Yang , Qiaoling Li , Shenjun Dai , Weiping Fang , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher
发明人： Yiquan Yang , Yingjuan Hao , Aiping Chen , Qi Wang , Lingmei Yang , Qiaoling Li , Shenjun Dai , Weiping Fang , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher
IPC分类号： B01J21/08 , B01J23/04 , B01J23/28 , B01J23/88 , B01J23/882 , B01J23/883 , B01J23/00 , B01J23/887 , B01J37/02 , B01J37/16 , C07C319/02 , B01J21/06
CPC分类号： B01J23/28 , B01J21/063 , B01J23/002 , B01J23/8872 , B01J37/0207 , B01J37/16 , B01J2523/00 , C07C319/02 , C07C321/04 , B01J2523/13 , B01J2523/68
摘要： This invention is related to a preparation method of a supported catalyst Mo—O—K-MexOy for the synthesis of methanethiol from H2S-containing syngas. The catalyst comprises of an active component of Mo—O—K-based species, an active promoter and a support denoted as metal (or metals)-carrier. The support is prepared by electroless plating method in such a way that the metal or metals chosen are plated onto the surface of the carrier. Transition metal, especially Fe, Co or Ni are selected to be the plating metal, while SiO2, Al2O3 or TiO2 are selected to be carrier. The catalyst thus prepared is found to be efficient for the synthesis of methanethiol from H2S-containing syngasor carbon oxides/hydrogen mixtures, especially regarding a minor formation of the by-product CO2.
摘要翻译： 本发明涉及用于从含H2S的合成气合成甲硫醇的负载型催化剂Mo-O-K-MexOy的制备方法。 该催化剂包括Mo-O-K基活性组分，活性促进剂和表示为金属（或金属）载体的载体。 通过化学镀方法制备载体，使得所选择的金属或金属镀在载体的表面上。 选择过渡金属，特别是Fe，Co或Ni作为电镀金属，而选择SiO 2，Al 2 O 3或TiO 2作为载体。 发现如此制备的催化剂对于从含H2S的合成气碳氢氧化物/氢混合物合成甲硫醇是有效的，特别是对副产物CO 2的次要形成。
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9.发明申请MO CONTAINING CATALYST, A PREPARATION METHOD AND A METHOD FOR PREPARING METHYL MERCAPTAN 有权含MO催化剂，制备方法和制备甲基丙烯酸甲酯的方法公开(公告)号：US20100094059A1
公开(公告)日：2010-04-15
申请号：US12439926
申请日：2007-05-25
申请人： Yiquan Yang , Aiping Chen , Qi Wang , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher
发明人： Yiquan Yang , Aiping Chen , Qi Wang , Jan-Olaf Barth , Christoph Weckbecker , Klaus Huthmacher
IPC分类号： C07C319/02 , B01J27/057 , B01J29/04 , B01J23/28
CPC分类号： B01J23/28 , B01J21/08 , B01J23/8872 , B01J27/0576 , B01J35/002 , B01J37/0201 , B01J37/0203 , B01J37/0205 , B01J37/20 , C07C319/02 , C07C321/04
摘要： A method is described to prepare a Mo containing supported catalyst comprising TeO2 as active promoter and a process for preparing methanethiol in the presence of said catalyst.
摘要翻译： 描述了一种制备包含TeO 2作为活性促进剂的Mo载体催化剂的方法和在所述催化剂存在下制备甲硫醇的方法。
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10.发明申请公开(公告)号：US20090308138A1
公开(公告)日：2009-12-17
申请号：US12278927
申请日：2007-01-11
CPC分类号： B01J8/06 , B01J8/0015 , B01J8/003 , B01J8/004 , B01J19/249 , B01J19/30 , B01J2208/00539 , B01J2208/00548 , B01J2208/00681 , B01J2208/00752 , B01J2208/00769 , B01J2208/021 , B01J2208/022 , B01J2219/245 , B01J2219/2471 , B01J2219/2481 , B01J2219/30207 , B01J2219/30215 , B01J2219/30223 , B01J2219/308 , B01J2219/3083 , B01J2219/3086
摘要： The invention relates to a process for measuring the uniform filling of reactors or columns with solid bodies and to an apparatus for performing the process.
摘要翻译： 本发明涉及一种用于测量具有固体的反应器或塔的均匀填充的方法以及用于执行该过程的装置。
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