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1.发明授权Aminoguanidine bicarbonate with particular properties and method for making same 有权具有特殊性质的氨基胍碳酸氢盐及其制备方法公开(公告)号：US06884912B1
公开(公告)日：2005-04-26
申请号：US10031113
申请日：2000-06-08
IPC分类号： C07C277/08 , C07C277/02 , C07C279/02 , C07C281/16
CPC分类号： C07C277/02 , C07C279/02
摘要： The invention concerns a method for making aminoguanidine bicarbonate from an aqueous solution of cyanamide and an aqueous solution of hydrazine in the presence of CO2. The invention is characterised in that it consists in proceeding with an amount of cyamide slightly higher than the stoichiometric quantity. The invention also concerns quasi-spherical agglomerates of aminoguanidine bicarbonate crystals.
摘要翻译： 本发明涉及一种在CO 2 2存在下由氨腈水溶液和肼水溶液制备氨基胍碳酸氢盐的方法。 本发明的特征在于其进行量稍高于化学计量的cyamide。 本发明还涉及氨基胍碳酸氢盐晶体的准球形附聚物。
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公开(公告)号：US06504033B1
公开(公告)日：2003-01-07
申请号：US09390286
申请日：1999-09-03
申请人： Paul Bourdauducq
发明人： Paul Bourdauducq
IPC分类号： C07D24908
CPC分类号： C07D249/08 , C07D231/12 , C07D233/56
摘要： The present invention relates to a process for the preparation of products of formula (1): in which R denotes H or an alkyl group containing from 1 to 10 carbon atoms, it being possible for this alkyl group to be substituted by one or more aryl, heteroaryl, hydroxyl or alkenyl groups, in which process hydrazine is reacted with a deficiency of carboxylic acid RCOOH and then the water of reaction and optionally the water of dilution of the hydrazine and of the acid is removed. It is particularly useful for preparing 4-amino-1,2,4-triazole.
摘要翻译： 本发明涉及制备式（1）的产物的方法：其中R表示H或含有1至10个碳原子的烷基，该烷基可能被一个或多个芳基取代 ，杂芳基，羟基或烯基，其中肼与羧酸RCOOH的缺乏反应，然后除去反应水和任选的肼的稀释水和酸的水，特别适用于制备4 - 氨基-1,2,4-三唑。
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公开(公告)号：US5345007A
公开(公告)日：1994-09-06
申请号：US148257
申请日：1993-11-05
CPC分类号： C07C29/36
摘要： A process for the preparation of octadienols, comprising the hydrodimerization reaction of 1,3-butadiene with water in the presence of a transition metal in the metal form or in the form of a compound of the said metal, of a water-soluble tertiary or quaternary phosphorus-containing compound and of at least one nitrogen-containing compound selected from the group consisting of a tertiary amine and a quaternary ammonium salt of general formula (I) or (II): ##STR1## in which R.sub.p, R.sub.q and R.sub.s are identical or different and each is a methyl or ethyl group; R.sub.r is an alkyl group containing from 6 to 22 carbon atoms; X is a counter-anion selected from the group consisting ofHCO.sub.3.sup.-, CO.sub.3.sup.2-, HSO.sub.3.sup.-, SO.sub.3.sup.2-, SiO.sub.3.sup.2-,PO.sub.4.sup.3-, HPO.sub.3.sup.2-, AsO.sub.4.sup.3-, SO.sub.4.sup.2-, HSO.sub.4.sup.-, RSO.sub.3.sup.-, RCO.sub.2.sup.-, and OH.sup.-, R being an alkyl group; the said reaction being carried out in the presence of carbon dioxide.
摘要翻译： 一种制备辛二烯醇的方法，包括1,3-丁二烯与水在金属形式的过渡金属或所述金属的化合物存在下的水分解反应的水溶性叔或 含有季铵的化合物和选自叔胺和通式（I）或（II）的季铵盐的至少一种含氮化合物：（I）图像（II） ）其中Rp，Rq和R 5相同或不同，并且各自为甲基或乙基; Rr是含有6-22个碳原子的烷基; X是选自HCO3-，CO32-，HSO3-，SO32-，SiO32-，PO43-，HPO32-，AsO43-，SO42-，HSO4-，RSO3-，RCO2-和OH的抗衡阴离子 - ，R为烷基; 所述反应在二氧化碳存在下进行。
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公开(公告)号：US06562311B1
公开(公告)日：2003-05-13
申请号：US09744558
申请日：2001-01-25
IPC分类号： C01B2116
CPC分类号： C01B21/16 , C07C251/88
摘要： The invention concerns a method for preparing methyl ethyl ketone azine which consists in: (a) reacting ammonia, hydrogen peroxide and methyl ethyl ketone in the presence of a working solution to form an azine; (b) separating the working solution and the azine possibly containing methyl ethyl ketone which has not reacted and butanol-2; (c) recycling the working solution to step (a) after optional treatment; (d) separating the methyl ethyl ketone and the butanol-2 from the azine. The butanol-2 of the flow in step (d) is either purged or dehydrogenated in MEK and recycled at step (a).
摘要翻译： 本发明涉及一种制备甲乙酮吖嗪的方法，该方法包括：（a）在工作溶液存在下使氨，过氧化氢和甲基乙基酮反应形成吖嗪; （b）分离可能含有未反应的甲基乙基酮和丁醇-2的工作溶液和吖嗪; （c）在任选处理后将工作溶液循环到步骤（a）; （d）从吖嗪中分离甲基乙基酮和丁醇-2。 在步骤（d）中的流程的丁醇-2在MEK中被吹扫或脱氢，并在步骤（a）中再循环。
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公开(公告)号：US6113661A
公开(公告)日：2000-09-05
申请号：US147658
申请日：1999-05-04
CPC分类号： C10L1/1852 , C10L1/026 , C10L1/1855 , C10L1/1985
摘要： A fuel composition containing, as a major portion, at least one fuel base, and, as a minor portion, at least one oxygenated compound, which contains at least 0.05% by weight of at least one trialkoxyalkane of the formula (I): ##STR1## wherein: X is a divalent hydrocarbon-containing group C.sub.n H.sub.2n, wherein n is 1, 2, or 3, each hydrogen atom optionally being substituted by a hydrocarbon-containing residue;R.sub.1, R'.sub.1, and R".sub.1 are each independently linear or branched alkyl groups containing from 1 to 10 carbon atoms and optionally at least one oxygen atom, two of each of R.sub.1, R'.sub.1 and R".sub.1 groups optionally being connected to form a heterocyclic ring containing 5 or 6 atoms; andR.sub.2 is a hydrogen atom or a linear C.sub.1 -C.sub.4 alkyl radical, or R.sub.2 and hydrocarbon-containing residue X, together by bonding, form a ring containing 5 or 6 carbon atoms.
摘要翻译： PCT No.PCT / FR98 / 01168 Sec。 371日期1999年5月4日 102（e）日期1999年5月4日PCT提交1998年6月8日PCT公布。 第WO98 / 56879号公报 日期1998年12月17日一种燃料组合物，其主要含有至少一种燃料基质，以及作为少部分含有至少一种含氧化合物的燃料组合物，其含有至少0.05重量％的至少一种下式的三烷氧基烷烃 （I）：其中：X是含二价烃的基团C n H 2n，其中n是1,2或3，每个氢原子任选地被含烃残基取代; R1，R'1和R'1各自独立地是含有1至10个碳原子和任选的至少一个氧原子的直链或支链烷基，任选地，R 1，R'1和R“ 连接形成含有5或6个原子的杂环; 并且R2是氢原子或直链C 1 -C 4烷基，或R 2和含烃残基X一起通过键合形成含有5或6个碳原子的环。
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6.发明授权Process for preparing azoiminoethers and azocarboxylic acid esters and novel azocboxylic acid mixed esters 有权制备偶氮二异氰醚和偶氮羧酸酯和新型偶氮羧酸混合酯的方法公开(公告)号：US06407219B1
公开(公告)日：2002-06-18
申请号：US09889147
申请日：2001-09-28
申请人： Paul Bourdauducq
发明人： Paul Bourdauducq
IPC分类号： C07C25706
CPC分类号： C07C245/04 , C07C257/06 , C07C257/14
摘要： The invention concerns a method for preparing an azoiminoether hydrochloride which consists in reacting an azonitrile with an alcohol and hydrochloric acid in an aromatic solvent, wherein the molar ratio R=HCl/azonitrile is >2 when the alcohol is methanol and >3 when the alcohol is ethanol or a higher alcohol. The invention also concerns a method for preparing an azocarboxylic acid ester which consists in the synthesis of an azoiminoether hydrochloride by the inventive method and, hydrolysis in the presence of the resulting azoiminoether hydrochloride. Said methods enable to obtain liquid composition of azocarboxylic acid esters. The invention further concerns mixed azoiminoether salts of formula (II′). The invention also concerns mixed azoiminocarboxylic acid esters corresponding to the formula (III′).
摘要翻译： 本发明涉及一种制备偶氮二甲苯醚盐酸盐的方法，该方法包括使偶氮腈与醇和盐酸在芳族溶剂中反应，其中当醇为甲醇时，R = HCl /偶氮的摩尔比> 2，当醇 是乙醇或高级醇。 本发明还涉及一种制备偶氮羧酸酯的方法，其包括通过本发明方法合成偶氮二甲苯醚盐酸盐，并在所得的偶氮二甲苯醚盐酸盐存在下进行水解。 所述方法能够获得偶氮羧酸酯的液体组合物。 本发明还涉及式（II'）的混合偶氮仿生醚盐。 本发明还涉及对应于式（III'）的混合偶氮二羧酸酯。
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公开(公告)号：US6040456A
公开(公告)日：2000-03-21
申请号：US965144
申请日：1997-11-06
申请人： Paul Bourdauducq
发明人： Paul Bourdauducq
IPC分类号： C07D249/08 , C07D521/00
CPC分类号： C07D249/08 , C07D231/12 , C07D233/56
摘要： The present invention relates to a process for the preparation of products of formula (1): ##STR1## in which R denotes H or an alkyl group containing from 1 to 10 carbon atoms, it being possible for this alkyl group to be substituted by one or more aryl, heteroaryl, hydroxyl or alkenyl groups, in which process hydrazine is reacted with a deficiency of carboxylic acid RCOOH and then the water of reaction and optionally the water of dilution of the hydrazine and of the acid is removed.It is particularly useful for preparing 4-amino-1,2,4-triazole.
摘要翻译： 本发明涉及制备式（1）的产物的方法：其中R表示H或含有1至10个碳原子的烷基，该烷基可能被一个或多个芳基取代 ，杂芳基，羟基或烯基，其中肼与羧酸RCOOH的缺乏反应，然后除去反应水和任选的肼和酸的稀释水。 对于制备4-氨基-1,2,4-三唑特别有用。
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