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    BaX TYPE ZEOLITE GRANULE AND PROCESS FOR PREPARING THE SAME
    1.
    发明申请
    BaX TYPE ZEOLITE GRANULE AND PROCESS FOR PREPARING THE SAME 有权
    BaX型沸石颗粒及其制备方法

    公开(公告)号：US20130012377A1

    公开(公告)日：2013-01-10

    申请号：US13541395

    申请日：2012-07-03

    申请人： Jeong Kwon Suh ,  Beom Sik Kim ,  Yun Ho Jeong ,  Jin Suk Lee ,  Won Young Kim ,  Ho Sik Chang

    发明人： Jeong Kwon Suh ,  Beom Sik Kim ,  Yun Ho Jeong ,  Jin Suk Lee ,  Won Young Kim ,  Ho Sik Chang

    IPC分类号： B01J20/18 ,  B01J20/30

    CPC分类号： C01B39/48 ,  B01J20/18 ,  B01J20/183 ,  B01J20/186 ,  B01J20/28004 ,  B01J20/2803 ,  B01J20/3007 ,  B01J20/3028 ,  B01J20/3042 ,  B01J20/305 ,  B01J20/3078 ,  B01J20/3085 ,  C07C7/13 ,  C07C2529/08 ,  C07C15/08

    摘要： The present invention provides a method for preparing a BaX type zeolite granules comprising: adding a carbohydrate-based molding promoter to NaX type zeolite powder and thereto subsequently spraying and blending alumina sol and silica sol to form granules of the mixture; heating the formed granules to convert the alumina and silica component to aluminosilica so as to generate pores inside the formed granules; hydrothermally treating the resulted granules in a sodium hydroxide aqueous solution under the conditions for zeolite synthesis, thereby converting a portion of the aluminosilica to zeolite; and carrying out ion-exchanging by Ba ions. The present invention also provides BaX type zeolite granules which have excellent strength and can be suitably used as an adsorbent in simulated moving bed (SMB) application.

    摘要翻译： 本发明提供一种制备BaX型沸石颗粒的方法，包括：向NaX型沸石粉末中加入碳水化合物型成型助剂，随后喷涂和混合氧化铝溶胶和二氧化硅溶胶以形成混合物颗粒; 加热形成的颗粒以将氧化铝和二氧化硅组分转化成铝硅石，以在形成的颗粒内产生孔; 在沸石合成条件下将所得颗粒水解处理在氢氧化钠水溶液中，从而将一部分铝硅石转化为沸石; 并通过Ba离子进行离子交换。 本发明还提供了具有优异强度并可适用于模拟移动床（SMB）应用中的吸附剂的BaX型沸石颗粒。

    PROCESS FOR POLYMERIZATION OR COPOLYMERIZATION OF ETHYLENE
    3.
    发明申请
    PROCESS FOR POLYMERIZATION OR COPOLYMERIZATION OF ETHYLENE 失效
    乙烯的聚合或共聚方法

    公开(公告)号：US20090221771A1

    公开(公告)日：2009-09-03

    申请号：US12160773

    申请日：2006-12-28

    申请人： Sang Yull Kim ,  Ho Sik Chang ,  Chun Byung Yang

    发明人： Sang Yull Kim ,  Ho Sik Chang ,  Chun Byung Yang

    IPC分类号： C08F4/50

    CPC分类号： C08F10/00 ,  C08F110/02 ,  C08F4/6565 ,  C08F2500/12 ,  C08F2500/18 ,  C08F4/651

    摘要： Provided is a process for polymerization and copolymerization of ethylene, specifically comprising carrying out polymerization or copolymerization ethylene in the presence of (a) a solid complex titanium catalyst which is produced by the process comprising: (i) preparing a magnesium compound solution by contacting a halogenated magnesium compound and an alcohol for allowing a reaction; (ii) reacting the resulted magnesium compound solution with an ester compound having at least one hydroxyl group and a silicon compound having at least one alkoxy group; (iii) reacting the resulted solution with a mixture of a titanium compound and a silicon compound to obtain a solid titanium catalyst component; (iv) washing the resulted solid titanium catalyst component with a halogenated saturated hydrocarbon compound; and (v) further reacting the washed solid titanium catalyst component with a titanium compound to obtain a solid complex titanium catalyst, and (b) an organometallic compound from Group II or III of Periodic table of elements. According to the present invention, it is possible to provide a process for polymerization or copolymerization of ethylene in which the catalyst activity is improved and a polymer of high bulk density is provided, with the use of a catalyst prepared by a simple process.

    摘要翻译： 提供了一种乙烯的聚合和共聚方法，特别包括在（a）固体络合物钛催化剂的存在下进行聚合或共聚乙烯，所述固体络合物钛催化剂通过以下方法制备，所述方法包括：（i）通过使 卤化镁化合物和用于允许反应的醇; （ii）使得到的镁化合物溶液与具有至少一个羟基的酯化合物和具有至少一个烷氧基的硅化合物反应; （iii）使所得溶液与钛化合物和硅化合物的混合物反应，得到固体钛催化剂组分; （iv）用卤化饱和烃化合物洗涤得到的固体钛催化剂组分; 和（v）使洗涤的固体钛催化剂组分与钛化合物进一步反应以获得固体络合物钛催化剂，和（b）元素周期表第II或III族的有机金属化合物。 根据本发明，通过使用通过简单的方法制备的催化剂，可以提供改进催化剂活性的乙烯的聚合或共聚方法和提供高堆积密度的聚合物。

    Process for polymerization or copolymerization of ethylene
    4.
    发明授权
    Process for polymerization or copolymerization of ethylene 失效
    乙烯的聚合或共聚方法

    公开(公告)号：US07754833B2

    公开(公告)日：2010-07-13

    申请号：US12160773

    申请日：2006-12-28

    申请人： Sang Yull Kim ,  Ho Sik Chang ,  Chun Byung Yang

    发明人： Sang Yull Kim ,  Ho Sik Chang ,  Chun Byung Yang

    IPC分类号： C08F4/44

    CPC分类号： C08F10/00 ,  C08F110/02 ,  C08F4/6565 ,  C08F2500/12 ,  C08F2500/18 ,  C08F4/651

    摘要： Provided is a process for polymerization and copolymerization of ethylene, specifically comprising carrying out polymerization or copolymerization ethylene in the presence of (a) a solid complex titanium catalyst which is produced by the process comprising: (i) preparing a magnesium compound solution by contacting a halogenated magnesium compound and an alcohol for allowing a reaction; (ii) reacting the resulted magnesium compound solution with an ester compound having at least one hydroxyl group and a silicon compound having at least one alkoxy group; (iii) reacting the resulted solution with a mixture of a titanium compound and a silicon compound to obtain a solid titanium catalyst component; (iv) washing the resulted solid titanium catalyst component with a halogenated saturated hydrocarbon compound; and (v) further reacting the washed solid titanium catalyst component with a titanium compound to obtain a solid complex titanium catalyst, and (b) an organometallic compound from Group II or III of Periodic table of elements. According to the present invention, it is possible to provide a process for polymerization or copolymerization of ethylene in which the catalyst activity is improved and a polymer of high bulk density is provided, with the use of a catalyst prepared by a simple process.

    摘要翻译： 提供了一种乙烯的聚合和共聚方法，特别包括在（a）固体络合物钛催化剂的存在下进行聚合或共聚乙烯，所述固体络合物钛催化剂通过以下方法制备，所述方法包括：（i）通过使 卤化镁化合物和用于允许反应的醇; （ii）使得到的镁化合物溶液与具有至少一个羟基的酯化合物和具有至少一个烷氧基的硅化合物反应; （iii）使所得溶液与钛化合物和硅化合物的混合物反应，得到固体钛催化剂组分; （iv）用卤化饱和烃化合物洗涤得到的固体钛催化剂组分; 和（v）使洗涤的固体钛催化剂组分与钛化合物进一步反应以获得固体络合物钛催化剂，和（b）元素周期表第II或III族的有机金属化合物。 根据本发明，通过使用通过简单的方法制备的催化剂，可以提供改进催化剂活性的乙烯的聚合或共聚方法和提供高堆积密度的聚合物。