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公开(公告)号：US08608824B2
公开(公告)日：2013-12-17
申请号：US13063321
申请日：2009-09-02
申请人： Jochen Steiner , Ekkehard Schwab , Andreas Keller , Otto Watzenberger , Ulrich Gräβle , Manfred Julius
发明人： Jochen Steiner , Ekkehard Schwab , Andreas Keller , Otto Watzenberger , Ulrich Gräβle , Manfred Julius
CPC分类号： B01J23/745 , B01J23/78 , B01J37/086 , C07C1/044 , C07C2523/745 , C10G2/332 , C10G2400/20 , C10J3/00 , C10J2300/0916 , C10J2300/093 , C10J2300/1659 , C10K1/00 , Y02P20/125 , Y02P20/145 , Y02P20/52 , C07C11/02
摘要： Integrated process, in which pure carbonyl iron powder (CIP) is prepared by decomposition of pure iron pentacarbonyl (IPC) in a plant A, carbon monoxide (CO) liberated in the decomposition of the IPC is used in plant A for the preparation of further CIP from iron or is fed to an associated plant B for the preparation of synthesis gas or is fed to an associated plant C for the preparation of hydrocarbons from synthesis gas, and the CIP prepared in plant A is used as catalyst or catalyst component in an associated plant C for the preparation of hydrocarbons from synthesis gas from plant B.
摘要翻译： 通过在植物A中分解纯铁五羰基（IPC）制备纯羰基铁粉（CIP）的综合方法，在植物A中使用在IPC分解中释放出的一氧化碳（CO）用于制备进一步的 将CIP从铁中加入到相关联的工厂B中用于制备合成气，或者将其进料到合成工厂C用于从合成气制备烃，并将在工厂A中制备的CIP用作催化剂或催化剂组分 联合植物C用于从植物B的合成气制备烃。
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2.发明申请公开(公告)号：US20110162484A1
公开(公告)日：2011-07-07
申请号：US13063321
申请日：2009-09-02
申请人： Jochen Steiner , Ekkehard Schwab , Andreas Keller , Otto Watzenberger , Ulrich Grässle , Manfred Julius
发明人： Jochen Steiner , Ekkehard Schwab , Andreas Keller , Otto Watzenberger , Ulrich Grässle , Manfred Julius
IPC分类号： B22F9/22
CPC分类号： B01J23/745 , B01J23/78 , B01J37/086 , C07C1/044 , C07C2523/745 , C10G2/332 , C10G2400/20 , C10J3/00 , C10J2300/0916 , C10J2300/093 , C10J2300/1659 , C10K1/00 , Y02P20/125 , Y02P20/145 , Y02P20/52 , C07C11/02
摘要： Integrated process, in which pure carbonyl iron powder (CIP) is prepared by decomposition of pure iron pentacarbonyl (IPC) in a plant A, carbon monoxide (CO) liberated in the decomposition of the IPC is used in plant A for the preparation of further CIP from iron or is fed to an associated plant B for the preparation of synthesis gas or is fed to an associated plant C for the preparation of hydrocarbons from synthesis gas, and the CIP prepared in plant A is used as catalyst or catalyst component in an associated plant C for the preparation of hydrocarbons from synthesis gas from plant B.
摘要翻译： 通过在植物A中分解纯铁五羰基（IPC）制备纯羰基铁粉（CIP）的综合方法，在植物A中使用在IPC分解中释放出的一氧化碳（CO）用于制备进一步的 将CIP从铁中加入到相关联的工厂B中用于制备合成气，或者将其进料到合成工厂C用于从合成气制备烃，并将在工厂A中制备的CIP用作催化剂或催化剂组分 联合植物C用于从植物B的合成气制备烃。
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公开(公告)号：US08293945B2
公开(公告)日：2012-10-23
申请号：US12809649
申请日：2008-12-10
IPC分类号： C07C209/16 , C07D265/30 , C07D295/03 , C07D241/04 , B01J31/00 , B01J23/76 , B01J23/835 , B01J23/843 , B01J23/883
CPC分类号： B01J23/883 , B01J23/002 , B01J23/76 , B01J23/835 , B01J23/8435 , B01J23/8437 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C213/02 , C07D295/023 , Y02P20/582 , B01J2523/44 , B01J2523/48 , B01J2523/842 , B01J2523/847 , B01J2523/68 , B01J2523/51 , B01J2523/43 , B01J2523/53 , B01J2523/54
摘要： Processes for preparing an amine, which processes comprise: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, nickel, and iron, and 0.2 to 5.5% by weight of at least one oxygen compound of tin, lead, bismuth, molybdenum, antimony or phosphorus, calculated as SnO, PbO, Bi2O3, MoO3, Sb2O3 and H3PO4 respectively; and wherein the catalytically active composition of the catalyst does not comprise any copper.
摘要翻译： 用于制备胺的方法，该方法包括：将选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆和含镍催化剂的存在下; 其中所述催化剂包含催化活性组合物，其在用氢还原之前包括锆，镍和铁的氧化合物和0.2至5.5重量％的至少一种氧化合物的锡，铅，铋，钼，锑或 磷，分别计算为SnO，PbO，Bi2O3，MoO3，Sb2O3和H3PO4; 并且其中催化剂的催化活性组合物不包含任何铜。
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公开(公告)号：US08324430B2
公开(公告)日：2012-12-04
申请号：US12809657
申请日：2008-12-10
IPC分类号： C07C209/16 , C07D241/04 , C07D265/30 , C07D295/03 , B01J23/835 , B01J23/84 , B01J23/843 , B01J23/847 , B01J23/825 , B01J37/03
CPC分类号： B01J27/1853 , B01J23/002 , B01J23/755 , B01J23/825 , B01J23/835 , B01J23/84 , B01J23/8435 , B01J23/8474 , B01J27/055 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C209/78 , C07C213/02 , C07D295/023 , Y02P20/582 , B01J2523/17 , B01J2523/48 , B01J2523/56 , B01J2523/845 , B01J2523/847 , B01J2523/44 , B01J2523/53 , C07C211/10 , C07C217/08
摘要： Processes for preparing an amine, the processes comprising: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-, copper- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, copper, and nickel, 1.5 to 4.5% by weight of an oxygen compound of cobalt, calculated as CoO, and 0.2 to 5.0% by weight of at least one oxygen compound of niobium, sulfur, phosphorus, gallium, boron, lead or antimony, calculated in each case as Nb2O5, H2SO4, H3PO4, Ga2O3, B2O3, PbO and Sb2O3 respectively, and wherein the catalytically active composition does not comprise any molybdenum.
摘要翻译： 用于制备胺的方法，所述方法包括：使选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆，含铜和镍的催化剂存在下; 其中所述催化剂包含催化活性组合物，其在用氢还原之前包括锆，铜和镍的氧化合物，1.5至4.5重量％的作为CoO计算的氧化合物钴和0.2至5.0重量％ 的铌，硫，磷，镓，硼，铅或锑的至少一种氧化合物，分别以Nb 2 O 5，H 2 SO 4，H 3 PO 4，Ga 2 O 3，B 2 O 3，PbO和Sb 2 O 3计算，其中催化活性组合物不包含 任何钼。
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公开(公告)号：US20110054167A1
公开(公告)日：2011-03-03
申请号：US12809653
申请日：2008-12-10
IPC分类号： C07D295/023 , C07C209/16 , B01J23/72
CPC分类号： B01J23/835 , B01J23/002 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C213/02 , C07D295/02 , C07D295/06 , C07C217/08
摘要： Processes for preparing an amine, which processes comprise: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-, copper- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, copper, nickel and tin, and 0.5 to 8.0% by weight of an oxygen compound of cobalt, calculated as CoO, and wherein the catalytically active composition does not comprise any ruthenium.
摘要翻译： 用于制备胺的方法，该方法包括：将选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆，含铜和镍的催化剂存在下; 其中所述催化剂包含催化活性组合物，所述催化活性组合物在用氢还原之前包括锆，铜，镍和锡的氧化合物和0.5至8.0重量％的作为CoO计算的钴的氧化合物，并且其中催化活性 组合物不包含任何钌。
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公开(公告)号：US20100274011A1
公开(公告)日：2010-10-28
申请号：US12809657
申请日：2008-12-10
IPC分类号： C07D265/30 , C07C209/68 , C07C209/78 , C07D241/04 , B01J23/72
CPC分类号： B01J27/1853 , B01J23/002 , B01J23/755 , B01J23/825 , B01J23/835 , B01J23/84 , B01J23/8435 , B01J23/8474 , B01J27/055 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C209/78 , C07C213/02 , C07D295/023 , Y02P20/582 , B01J2523/17 , B01J2523/48 , B01J2523/56 , B01J2523/845 , B01J2523/847 , B01J2523/44 , B01J2523/53 , C07C211/10 , C07C217/08
摘要： Processes for preparing an amine, the processes comprising: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-, copper- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, copper, and nickel, 1.5 to 4.5% by weight of an oxygen compound of cobalt, calculated as CoO, and 0.2 to 5.0% by weight of at least one oxygen compound of niobium, sulfur, phosphorus, gallium, boron, lead or antimony, calculated in each case as Nb2O5, H2SO4, H3PO4, Ga2O3, B2O3, PbO and Sb2O3 respectively, and wherein the catalytically active composition does not comprise any molybdenum.
摘要翻译： 用于制备胺的方法，所述方法包括：使选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆，含铜和镍的催化剂存在下; 其中所述催化剂包含催化活性组合物，其在用氢还原之前包括锆，铜和镍的氧化合物，1.5至4.5重量％的作为CoO计算的氧化合物钴和0.2至5.0重量％ 的铌，硫，磷，镓，硼，铅或锑的至少一种氧化合物，分别以Nb 2 O 5，H 2 SO 4，H 3 PO 4，Ga 2 O 3，B 2 O 3，PbO和Sb 2 O 3计算，其中催化活性组合物不包含 任何钼。
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公开(公告)号：US08268995B2
公开(公告)日：2012-09-18
申请号：US12809645
申请日：2008-12-10
IPC分类号： C07D265/30 , B01J21/06 , C07C209/16 , C07C209/26
CPC分类号： B01J23/835 , B01J23/002 , B01J23/8435 , B01J23/8437 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C213/02 , C07D295/023 , Y02P20/582 , B01J2523/17 , B01J2523/44 , B01J2523/48 , B01J2523/842 , B01J2523/845 , B01J2523/847 , B01J2523/53 , B01J2523/43 , C07C217/08
摘要： Processes for preparing an amine, which processes comprise: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-, copper- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, copper, and nickel, and 0.2 to 40% by weight of an oxygen compound of cobalt, calculated as CoO, 0.1 to 5% by weight of an oxygen compound of iron, calculated as Fe2O3, and 0.1 to 5% by weight of at least one oxygen compound of lead, tin, bismuth or antimony, calculated as PbO, SnO, Bi2O3 and Sb2O3 respectively.
摘要翻译： 用于制备胺的方法，该方法包括：将选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆，含铜和镍的催化剂存在下; 其中所述催化剂包含催化活性组合物，其在用氢还原之前包括锆，铜和镍的氧化合物和0.2至40重量％的以COO计为0.1至5重量％的钴氧化合物 的铁氧化合物，以Fe 2 O 3计，和0.1〜5重量％的至少一种铅，锡，铋或锑的氧化合物分别以PbO，SnO，Bi 2 O 3和Sb 2 O计算。
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公开(公告)号：US20100274055A1
公开(公告)日：2010-10-28
申请号：US12809649
申请日：2008-12-10
IPC分类号： C07C209/44 , B01J27/185 , B01J23/883 , B01J23/755 , B01J23/835 , B01J23/745
CPC分类号： B01J23/883 , B01J23/002 , B01J23/76 , B01J23/835 , B01J23/8435 , B01J23/8437 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C213/02 , C07D295/023 , Y02P20/582 , B01J2523/44 , B01J2523/48 , B01J2523/842 , B01J2523/847 , B01J2523/68 , B01J2523/51 , B01J2523/43 , B01J2523/53 , B01J2523/54
摘要： Processes for preparing an amine, which processes comprise: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, nickel, and iron, and 0.2 to 5.5% by weight of at least one oxygen compound of tin, lead, bismuth, molybdenum, antimony or phosphorus, calculated as SnO, PbO, Bi2O3, MoO3, Sb2O3 and H3PO4 respectively; and wherein the catalytically active composition of the catalyst does not comprise any copper.
摘要翻译： 用于制备胺的方法，该方法包括：将选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆和含镍催化剂存在下; 其中所述催化剂包含催化活性组合物，其在用氢还原之前包括锆，镍和铁的氧化合物和0.2至5.5重量％的至少一种氧化合物的锡，铅，铋，钼，锑或 磷，分别计算为SnO，PbO，Bi2O3，MoO3，Sb2O3和H3PO4; 并且其中催化剂的催化活性组合物不包含任何铜。
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公开(公告)号：US08278489B2
公开(公告)日：2012-10-02
申请号：US12809653
申请日：2008-12-10
IPC分类号： C07C209/16 , C07D265/30 , C07D295/03 , C07D241/04 , B01J23/835 , B01J37/03 , B01J37/18
CPC分类号： B01J23/835 , B01J23/002 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C213/02 , C07D295/02 , C07D295/06 , C07C217/08
摘要： Processes for preparing an amine, which processes comprise: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-, copper- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, copper, nickel and tin, and 0.5 to 8.0% by weight of an oxygen compound of cobalt, calculated as CoO, and wherein the catalytically active composition does not comprise any ruthenium.
摘要翻译： 用于制备胺的方法，该方法包括：将选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆，含铜和镍的催化剂存在下; 其中所述催化剂包含催化活性组合物，所述催化活性组合物在用氢还原之前包括锆，铜，镍和锡的氧化合物和0.5至8.0重量％的作为CoO计算的钴的氧化合物，并且其中催化活性 组合物不包含任何钌。
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公开(公告)号：US20100274009A1
公开(公告)日：2010-10-28
申请号：US12809665
申请日：2008-12-10
IPC分类号： C07D265/30 , C07D211/00 , C07C209/00 , B01J27/185 , B01J23/72
CPC分类号： B01J23/825 , B01J23/002 , B01J23/8474 , B01J23/888 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C213/02 , C07C213/06 , C07D295/02 , C07D295/08 , B01J2523/17 , B01J2523/48 , B01J2523/51 , B01J2523/847 , B01J2523/69 , B01J2523/68 , B01J2523/32 , B01J2523/56 , C07C211/10 , C07C215/10 , C07C217/08 , C07C217/28
摘要： Processes for preparing an amine, the processes comprising: reacting a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones, and mixtures thereof, with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a zirconium dioxide-, copper- and nickel-containing catalyst; wherein the catalyst comprises a catalytically active composition which comprises, before reduction with hydrogen, oxygen compounds of zirconium, copper, nickel, no oxygen compounds of cobalt, and 0.2 to 5.0% by weight of at least one oxygen compound of phosphorus or gallium, calculated as H3PO4 and Ga2O3 respectively.
摘要翻译： 用于制备胺的方法，所述方法包括：将选自伯醇，仲醇，醛，酮及其混合物的反应物与氢和选自以下的氮化合物反应：氨，伯胺， 仲胺及其混合物，在二氧化锆，含铜和镍的催化剂存在下; 其中所述催化剂包含催化活性组合物，其在用氢还原之前包括锆，铜，镍的氧化合物，不含钴的氧化合物和0.2至5.0重量％的至少一种磷或镓的氧化合物，计算 分别为H3PO4和Ga2O3。
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