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    Hydrophobically modified polyethylenimines and polyvinylamines for wrinkle-resistant finishing of textiles containing cellulose
    1.
    发明授权
    Hydrophobically modified polyethylenimines and polyvinylamines for wrinkle-resistant finishing of textiles containing cellulose 有权
    疏水改性的聚乙烯亚胺和聚乙烯胺用于含纤维素的织物的抗皱整理

    公开(公告)号：US07141077B2

    公开(公告)日：2006-11-28

    申请号：US10477208

    申请日：2002-05-16

    申请人： Juergen Detering ,  Guenther Grimm ,  Torsten Freund

    发明人： Juergen Detering ,  Guenther Grimm ,  Torsten Freund

    IPC分类号： D06M15/61

    CPC分类号： C11D3/3723 ,  D06M15/3562 ,  D06M15/61 ,  D06M15/6436 ,  D06M15/647 ,  D06M23/06 ,  D06M2101/06 ,  D06M2200/20

    摘要： A process for wrinkleproofing cellulosic textiles comprises treating the textiles with a finish and drying the treated textiles, wherein the finish comprises one or more water-soluble or water-dispersible hydrophobically modified polyethyleneimines and/or polyvinylamines.Suitable hydrophobically modified polyethyleneimines are hydrophobically modified homopolymers of ethyleneimine, hydrophobically modified graft polymers of polyamidoamines or of polyvinylamines. Suitable hydrophobically modified polyvinylamines are hydrophobically modified at least partially hydrolyzed homo- or copolymers of N-vinylcarboxamides. The polyethyleneimines and polyvinylamines can be crosslinked by polyfunctional crosslinking compounds, quaternized and/or modified by reaction with alkylene oxides, dialkyl carbonates, alkylene carbonates and/or C1–C4-carboxylic acids.Suitable hydrophobicizing reagents are selected from the group consisting of long-chain linear or branched linear carboxylic acids, linear or branched alkyl halides, alkyl epoxides, alkylketene dimers, cyclic dicarboxylic anhydrides, alkyl isocyanates and chloroformic esters of fatty alcohols.

    摘要翻译： 纤维素纺织品的防皱方法包括用精加工处理织物并干燥经处理的纺织品，其中整理剂包含一种或多种水溶性或水分散性疏水改性的聚乙烯亚胺和/或聚乙烯胺。 合适的疏水改性聚乙烯亚胺是乙烯亚胺，聚酰胺胺或聚乙烯胺的疏水改性接枝聚合物的疏水改性均聚物。 合适的疏水改性聚乙烯胺是至少部分水解的N-乙烯基甲酰胺的均聚物或共聚物进行疏水改性的。 聚乙烯亚胺和聚乙烯胺可以通过多官能交联化合物交联，季铵化和/或通过与环氧烷，碳酸二烷基酯，碳酸亚烷基酯和/或C 1 -C 4 - - 羧酸。 合适的疏水化试剂选自长链直链或支链直链羧酸，直链或支链烷基卤，烷基环氧化物，烷基乙烯酮二聚体，环二羧酸酐，烷基异氰酸酯和脂肪醇的氯甲酸酯。

    Use of vinylpyrrolidone and vinylimidazole copolymers as detergent additives, novel polymers of vinylpyrrolidone and of vinylimidazole, and preparation thereof
    2.
    发明授权
    Use of vinylpyrrolidone and vinylimidazole copolymers as detergent additives, novel polymers of vinylpyrrolidone and of vinylimidazole, and preparation thereof 失效
    使用乙烯基吡咯烷酮和乙烯基咪唑共聚物作为洗涤剂添加剂，乙烯基吡咯烷酮和乙烯基咪唑的新型聚合物及其制备

    公开(公告)号：US5846924A

    公开(公告)日：1998-12-08

    申请号：US694023

    申请日：1996-08-08

    申请人： Juergen Detering ,  Christian Schade ,  Wolfgang Trieselt ,  Juergen Tropsch

    发明人： Juergen Detering ,  Christian Schade ,  Wolfgang Trieselt ,  Juergen Tropsch

    IPC分类号： C08F2/10 ,  C08F26/00 ,  C08F26/10 ,  C08F226/06 ,  C08F226/10 ,  C08F289/00 ,  C11D3/00 ,  C11D3/37 ,  C11D3/28

    CPC分类号： C11D3/3776 ,  C08F289/00 ,  C11D3/0021 ,  C11D3/3788

    摘要： There are described the use of copolymers obtainable by free-radically initiated copolymerization of monomer mixtures comprising (a) 60-99% by weight of 1-vinylpyrrolidone, 1-vinyl-imidazole or mixtures thereof, (b) 1-40% by weight of nitrogen-containing, basic ethylenically unsaturated monomers in the form of the free bases, in the form of salts or in quaternized form, and optionally (c) up to 20% by weight of other monoethylenically unsaturated monomers, as detergent additives for inhibiting dye transfer during the wash, detergents which contain such polymers, and polymers which are obtainable by free-radically initiated polymerization of (a) 1-vinylpyrrolidone, 1-vinylimidazole, 1-vinylimidazolium compounds, or mixtures thereof, and optionally (b) other nitrogen-containing, basic ethylenically unsaturated monomers in the form of the free bases, in the form of the salts or in quaternized form, and/or (c) other monoethylenically unsaturated monomers, in an aqueous medium in the presence of water-soluble proteins and a process for the preparation of the polymers by polymerising the monomers (a) and optionally (b) and/or (c) in an aqueous medium in the presence of water-soluble proteins using from 0.5 to 400 parts by weight of protein per 100 parts by weight of monomer used in the polymerization.

    摘要翻译： 描述了通过自由基引发的单体混合物共聚获得的共聚物的用途，所述单体混合物包含（a）60-99重量％的1-乙烯基吡咯烷酮，1-乙烯基 - 咪唑或其混合物，（b）1-40重量％ 的游离碱形式的含氮碱性烯键式不饱和单体，以盐形式或季铵化形式，以及任选地（c）至多20重量％的其它单烯属不饱和单体作为抑制染料的洗涤剂添加剂 在洗涤期间的转移，含有这种聚合物的洗涤剂，以及可通过（a）1-乙烯基吡咯烷酮，1-乙烯基咪唑，1-乙烯基咪唑鎓化合物或其混合物和任选的（b）其他氮气的自由引发聚合而获得的聚合物 含有游离碱形式的碱性烯属不饱和单体，以盐形式或季铵化形式，和/或（c）其它单烯键式不饱和单体，在预混物的水性介质中 ce的水溶性蛋白质的制备方法和通过在水溶性蛋白质的存在下在水溶液中使单体（a）和任选地（b）和/或（c）聚合而制备聚合物的方法，使用0.5至400 每100重量份聚合中使用的单体重量份蛋白质。

    Preparation of polyvinylpyridine N-oxides
    3.
    发明授权
    Preparation of polyvinylpyridine N-oxides 失效
    聚乙烯吡啶N-氧化物的制备

    公开(公告)号：US5578684A

    公开(公告)日：1996-11-26

    申请号：US507237

    申请日：1995-08-24

    申请人： Christian Schade ,  Dieter Boeckh ,  Juergen Detering

    发明人： Christian Schade ,  Dieter Boeckh ,  Juergen Detering

    IPC分类号： C08F8/06 ,  C08F26/08 ,  C08F8/42

    CPC分类号： C08F8/06

    摘要： Polyvinylpyridine N-oxides are prepared by oxidizing polyvinyl-pyridines with aqueous solutions of hydrogen peroxide in the presence of acids and oxides or acids of elements of Groups 5b, 6b, 7b and 8 of the Periodic Table or of salts of these acids as catalyst, it also being possible for the oxidation to take place in the absence of the catalysts when from 40 to 80% strength aqueous solutions of at least dibasic carboxylic acids or of polymers of monoethylenically unsaturated carboxylic acids are used as solvent.

    摘要翻译： PCT No.PCT / EP94 / 00490 Sec。 371日期1995年8月24日 102（e）日期1995年8月24日PCT 1995年2月21日提交PCT公布。 出版物WO94 / 20549 日期1994年9月15日聚乙烯基吡啶N-氧化物是通过在酸和氧化物的存在下用水过氧化氢水溶液氧化聚乙烯吡啶而制备的，其中元素周期表第5b，6b，7b和8族的元素，或 这些酸作为催化剂，当使用40-80％强度的至少二元羧酸的水溶液或单烯属不饱和羧酸的聚合物作为溶剂时，也可以在不存在催化剂的情况下进行氧化。

    Preparation of ultrapure N-vinylpyrrolidone polymers
    4.
    发明授权
    Preparation of ultrapure N-vinylpyrrolidone polymers 失效
    超纯N-乙烯基吡咯烷酮聚合物的制备

    公开(公告)号：US5354945A

    公开(公告)日：1994-10-11

    申请号：US982885

    申请日：1992-11-30

    申请人： Juergen Detering ,  Hartwig Voss

    发明人： Juergen Detering ,  Hartwig Voss

    IPC分类号： C08F6/06 ,  C08F2/04 ,  C08F6/00 ,  C08F26/10 ,  C08J3/07 ,  B01D61/14

    CPC分类号： C08F6/003 ,  Y10S210/908

    摘要： A process for preparing ultrapure polymers (or solutions thereof) which contain at least 20% by weight of N-vinylpyrrolidone as copolymerized units and have a Fikentscher K value of from 10 to 45 by customary free-radical polymerization in solution and subsequent purification of the solution with or without drying comprises purifying the solutions of the polymers by separating off the low molecular weight impurities by means of ultrafiltration at from 20.degree. to 100.degree. C. and from 1 to 80 bar.

    摘要翻译： 一种制备超纯聚合物（或其溶液）的方法，其含有至少20重量％的N-乙烯基吡咯烷酮作为共聚单元，并且通过溶液中的常规自由基聚合将Fikentscher K值设定为10至45，随后纯化 有或没有干燥的溶液包括通过在20℃至100℃和1至80巴下的超滤分离低分子量杂质来纯化聚合物溶液。

    Removal of heavy metal ions from wine and wine-like beverages
    6.
    发明授权
    Removal of heavy metal ions from wine and wine-like beverages 失效
    从葡萄酒和葡萄酒饮料中去除重金属离子

    公开(公告)号：US5094867A

    公开(公告)日：1992-03-10

    申请号：US639098

    申请日：1991-01-09

    申请人： Juergen Detering ,  Axel Sanner ,  Bernhard Fussnegger

    发明人： Juergen Detering ,  Axel Sanner ,  Bernhard Fussnegger

    IPC分类号： C02F1/28 ,  C02F1/62 ,  C12H1/04 ,  C12H1/056

    CPC分类号： C12H1/0424

    摘要： A process for removing heavy metal ions from wine and wine-like beverages, which entails treating each 100 l of the beverage with from 5 to 250 g of a polymer which contains, as copolymerized units, from 50 to 99.5% by weight of at least one basic vinylheterocycle with a pK.sub.a of not less than 3.8 and from 0 to 49.5% by weight of another copolymerizable monomer, and which has been prepared with the exclusion of oxygen and of polymerization initiators and in the presence of from 0.5 to 10% by weight, based on the monomers, of a crosslinker.

    摘要翻译： 从葡萄酒和酒样饮料中除去重金属离子的方法，其需要用5至250g聚合物处理每100升饮料，所述聚合物含有作为共聚单元的至少50至99.5重量％ 一种碱性乙烯基杂环，其中pKa不低于3.8，0-49.5重量％的另一种可共聚单体，并且其被排除氧和聚合引发剂制备，并且在0.5至10重量％ ，基于单体，交联剂。

    Branched polyesters with sulfonate groups
    7.
    发明授权
    Branched polyesters with sulfonate groups 有权
    具有磺酸基团的支化聚酯

    公开(公告)号：US08901066B2

    公开(公告)日：2014-12-02

    申请号：US13495512

    申请日：2012-06-13

    申请人： Monika Haberecht ,  Juergen Detering ,  Bernd Bruchmann ,  Helmut Witteler ,  Heike Weber ,  Karl Kolter

    发明人： Monika Haberecht ,  Juergen Detering ,  Bernd Bruchmann ,  Helmut Witteler ,  Heike Weber ,  Karl Kolter

    IPC分类号： C11D3/37 ,  C11D1/00 ,  B08B3/04 ,  C08G63/91 ,  C02F5/10 ,  C08G63/688

    CPC分类号： C02F5/10 ,  C08G63/6884 ,  C08G63/918 ,  C11D3/378

    摘要： Branched polyesters with sulfonate groups can be obtained by reacting components A, B, optionally C, and optionally D to yield branched polyesters, then reacting these branched polyesters with hydrogen sulfite. Component A is at least one α,β-olefinically unsaturated dicarboxylic acid, component B is at least one di- or higher-functional alcohol, optional component C is at least one di- or higher-functional carboxylic acid or hydroxycarboxylic acid without an α,β-olefinically unsaturated bond, and optional component D is at least one compound of formula CH3(—O—CH2—CH2)n—OH. In reacting the branched polyesters with hydrogen sulfite, a molar amount of hydrogen sulfite is at most 95 mol %, based on an amount of α,β-olefinically unsaturated dicarboxylic acid.

    摘要翻译： 具有磺酸盐基团的支链聚酯可以通过使组分A，B，任选地C和任选的D反应得到支链聚酯，然后使这些支化聚酯与亚硫酸氢钠反应而获得。 组分A是至少一种α，β-烯属不饱和二羧酸，组分B是至少一种二官能或更高官能的醇，任选的组分C是至少一种二官能或更高官能的羧酸或羟基羧酸，没有 α，β-烯属不饱和键，任选的组分D是至少一种式CH3（-O-CH2-CH2）n-OH的化合物。 在使支化聚酯与亚硫酸氢钠反应时，基于α，α-烯属不饱和二羧酸的量，亚硫酸氢的摩尔量为至多95摩尔％。

    Copolymers comprising polyalkylene oxide groups and quaternary nitrogen atoms
    9.
    发明申请
    Copolymers comprising polyalkylene oxide groups and quaternary nitrogen atoms 审中-公开
    包含聚环氧烷基团和季氮原子的共聚物

    公开(公告)号：US20070129516A1

    公开(公告)日：2007-06-07

    申请号：US10579547

    申请日：2004-11-17

    申请人： Juergen Detering ,  Thomas Pfeiffer ,  Parmod Reddy ,  Xinbei Song

    发明人： Juergen Detering ,  Thomas Pfeiffer ,  Parmod Reddy ,  Xinbei Song

    IPC分类号： C08F26/06

    CPC分类号： C11D3/3776 ,  C08F220/06 ,  C08F220/26 ,  C08F220/28 ,  C08F220/58 ,  C08F228/02 ,  C08F290/062 ,  C11D3/1253 ,  C11D3/3757 ,  C11D3/3769

    摘要： Copolymers which comprise in copolymerized form, (A) 60 to 99% by weight of at least one monoethylenically unsaturated polyalkylene oxide monomer of the formula I H2C═CR1—X—Y—R2—O—n—R3  I  in which the variables have the following meanings: X is —CH2— or —CO—, if Y is —O—; is —CO—, if Y is —NH—; Y is —O— or —NH—; R1 is hydrogen or methyl; R2 are identical or different C2-C6-alkylene radicals, which may be linear or branched and may be arranged blockwise or randomly; R3 is hydrogen or C1-C4-alkyl; n is an integer from 3 to 50, (B) 1 to 40% by weight of at least one quaternized nitrogen-containing monoethylenically unsaturated monomer, (C) 0 to 39% by weight of anionic monoethylenically unsaturated monomers and (D) 0 to 30% by weight of other nonionic monoethylenically unsaturated monomers and have an average molecular weight Mw of from 2000 to 100 000, and use of these copolymers as dispersants for clay minerals.

    摘要翻译： 包含共聚形式的共聚物（A）60至99重量％的至少一种式I的单烯键式不饱和聚环氧烷单体<？in-line-formula description =“In-line Formulas”end =“lead”？ “H”2 C-CR 1 -XY - R＆lt; 2＆lt;＆lt; img id = “PRIVATE-USE-CHARACTER-00002”he =“7.20mm”wi =“8.47mm”file =“US20070129516A1-20070607-Parenclosest.TIF”alt =“私人使用字符Parenclosest”img-content =“character”img-format =“tif”/> 3 I <？in-line-formula description =“In-line Formulas”end =“tail”？>其中 变量具有以下含义：X是-CH 2 - 或-CO-，如果Y是-O-; 是-CO-，如果Y是-NH-; Y是-O-或-NH-; R 1是氢或甲基; R 2是相同或不同的C 2 -C 6 - 亚烷基，其可以是直链或支链的并且可以以块状或随机排列; R 3是氢或C 1 -C 4 - 烷基; n为3〜50的整数，（B）1〜40重量％的至少一种季铵化含氮单烯属不饱和单体，（C）0〜39重量％的阴离子单烯属不饱和单体和（D）0〜 30重量％的其它非离子单烯键式不饱和单体，其平均分子量M w 2为2000至100 000，并且使用这些共聚物作为粘土矿物的分散剂。