Abstract:
The method for manufacturing a solid electrolyte using an LLZ material for a lithium-ion battery comprises the steps of: providing a starting material in which lanthanum nitrate [La(NO3)3.6H2O] and zirconium nitrate [ZrO(NO3)2.6H2O] are mixed at a mole ratio of 3:2; forming an aqueous solution by dissolving the starting material; forming a precipitate by putting ammonia, which is a complex agent, and sodium hydroxide, which adjusts the pH of a reactor, into the aqueous solution, mixing the same, and then co-precipitating the mixture; forming a primary precursor powder by cleaning, drying and pulverizing the precipitate; forming a secondary precursor powder by mixing lithium powder [LiOH.H2O] with the primary precursor powder and ball-milling the mixture so as to solidify the lithium; and forming a solid electrolyte powder by heat-treating the secondary precursor powder.
Abstract:
Disclosed is a method of preparing a solid electrolyte, which includes (a) preparing a solid electrolyte precursor slurry by subjecting a mixed solution including a metal precursor solution, containing a lanthanum precursor, a zirconium precursor and an aluminum precursor, a complexing agent, and a pH controller to coprecipitation, (b) preparing a solid electrolyte precursor by washing and drying the solid electrolyte precursor slurry, (c) preparing a mixture by mixing the solid electrolyte precursor with a lithium source, and (d) preparing an aluminum-doped lithium lanthanum zirconium oxide (LLZO) solid electrolyte by calcining the mixture, and which is also capable of adjusting the aluminum content of a starting material to thus control sintering properties and of adjusting the composition of a precursor and a lithium source to thus control the crystal structure, thereby improving the ionic conductivity of the solid electrolyte. In addition, a method of manufacturing an all-solid-state lithium secondary battery, including a solid electrolyte having improved ion conductivity, can be provided using the method of preparing the solid electrolyte.
Abstract:
An electromagnetic wave shielding sheet including a carbon composite fiber and manufactured by electrospinning, and a method of manufacturing the same are disclosed. More particularly, an electromagnetic wave shielding sheet includes a carbon composite fiber having a core-shell structure and a resin, and the core-shell structure includes an outer shell including a carbon fiber, and a core including metal nano particles arranged in a length direction of the carbon fiber in the outer shell. The electromagnetic wave shielding sheet includes metal nano particles as electromagnetic wave shielding materials in a carbon fiber, and the oxidation of a metal may be prevented, conductivity in a length direction of the carbon fiber may be secured, and the sheet may be applied to various industrial fields as an electromagnetic shielding material.
Abstract:
Disclosed is a liquid precursor delivery system that enables a thin film deposition process to be performed at a low temperature like 350° C. or lower in a process of manufacturing semiconductor devices or displays. The liquid precursor delivery system includes an aerosol generator, a vaporizer, and a vapor storage tank. The aerosol generator changes a liquid precursor into an aerosol precursor using ultrasonic vibrations. The vaporizer has a heater block in which a plurality of sloped plate-shaped heaters is arranged in a zigzag form and in which the aerosol precursor changes into a gas precursor by colliding with the heaters and thus obtaining heat energy. The vapor storage tank stores the gas precursor while maintaining a constant pressure and temperature of the gas precursor and delivers the gas precursor to a process chamber when a thin film deposition process is performed.
Abstract:
Disclosed is a simplified apparatus for purifying an organic material using an ionic liquid, including a sublimation unit for sublimating a raw organic material containing impurities for OLEDs by heating; a recrystallization unit for recrystallizing the sublimated gas of the organic material in the ionic liquid; and a control unit for controlling the operation of the sublimation unit and the recrystallization unit. Even when a very small amount of organic material is sublimated, the recrystallization thereof in the ionic liquid can be verified, thus easily checking the purification potential of the organic material using only a very small amount of organic material.
Abstract:
The present inventions relates to an organic light emitting device capable of decreasing a leakage current, and more particularly, to an organic light emitting device manufacturing method and an organic light emitting device using the same, which can decrease a leakage current, by flattening a lower electrode in order to decrease a leakage current of the lower electrode deposited through a shadow mask.