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    PREPARATION OF HIGH-QUALITY OXO PROCESS ALCOHOLS FROM INCONSTANT RAW MATERIAL SOURCES
    4.
    发明申请
    PREPARATION OF HIGH-QUALITY OXO PROCESS ALCOHOLS FROM INCONSTANT RAW MATERIAL SOURCES 有权
    从不合理原料来源制备高品质氧气工艺酒精

    公开(公告)号：US20150336861A1

    公开(公告)日：2015-11-26

    申请号：US14717183

    申请日：2015-05-20

    申请人： Frank GEILEN ,  Katrin Marie DYBALLA ,  Dieter HESS ,  Stephan PEITZ ,  Robert FRANKE ,  Dirk FRIDAG ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Guido STOCHNIOL

    发明人： Frank GEILEN ,  Katrin Marie DYBALLA ,  Dieter HESS ,  Stephan PEITZ ,  Robert FRANKE ,  Dirk FRIDAG ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Guido STOCHNIOL

    IPC分类号： C07C29/14 ,  C07C69/80 ,  C08K5/12 ,  C07C67/08

    CPC分类号： C07C29/14 ,  B01J31/185 ,  B01J31/1885 ,  C07C2/24 ,  C07C29/141 ,  C07C45/50 ,  C07C67/08 ,  C07C69/80 ,  C07C2523/755 ,  C08K5/12 ,  C07C11/02 ,  C07C47/02 ,  C07C31/125

    摘要： The preparation of high-quality oxo process alcohols from inconstant raw material sources is the technically demanding problem which is addressed by a process for continuously preparing an alcohol mixture, in which an input mixture which contains an olefin and has a composition that changes over time is subjected to an oligomerization to obtain an oligomerizate and at least a portion of the olefin oligomers present in the oligomerizate are hydroformylated with carbon monoxide and hydrogen in a hydroformylation in the presence of a homogeneous catalyst system to give aldehydes, at least some of which are converted to the alcohol mixture by subsequent hydrogenation. The process provides a constant plasticizer quality to be produced over a long production period and, optionally, a higher throughput with the same product quality. This is achieved a) by control of the temperature and/or the conversion of the oligomerization as a function of the current composition of the oligomerizate; and b) by control of the composition of the catalyst system and/or of the pressure of the hydroformylation as a function of the current composition of the aldehydes.

    摘要翻译： 从不定原料来源制备高品质氧化工艺醇是技术上要求苛刻的问题，其通过连续制备醇混合物的方法来解决，其中含有烯烃并且具有随时间变化的组成的输入混合物是 进行低聚以获得低聚物，并且在均相催化剂体系的存在下，在加氢甲酰化中，将低聚物中存在的烯烃低聚物的至少一部分与一氧化碳和氢气加氢甲酰化，得到醛，其中至少一些转化为 通过随后的氢化到醇混合物。 该方法提供了在长的生产周期内生产的恒定的增塑剂质量，并且可选地具有相同产品质量的较高产量。 这是通过控制低聚物的温度和/或转化作为当前低聚物组成的函数来实现的; 和b）通过控制催化剂体系的组成和/或加氢甲酰基化的压力作为醛的当前组成的函数。

    OPTIMIZED SEPARATION TECHNIQUE FOR WORK-UP OF HOMOGENEOUSLY CATALYSED HYDROFORMYLATION MIXTURES
    5.
    发明申请
    OPTIMIZED SEPARATION TECHNIQUE FOR WORK-UP OF HOMOGENEOUSLY CATALYSED HYDROFORMYLATION MIXTURES 有权
    用于均相催化水解混合物的优化分离技术

    公开(公告)号：US20160002136A1

    公开(公告)日：2016-01-07

    申请号：US14770525

    申请日：2014-02-13

    申请人： Hans-Gerd LUEKEN ,  Bart HAMERS ,  Dirk FRIDAG ,  Robert FRANKE ,  Markus PRISKE ,  Dieter HESS ,  Marc BECKER ,  Markus RUDEK

    发明人： Hans-Gerd LUEKEN ,  Bart HAMERS ,  Dirk FRIDAG ,  Robert FRANKE ,  Markus PRISKE ,  Dieter HESS ,  Marc BECKER ,  Markus RUDEK

    IPC分类号： C07C45/78 ,  C07C29/16 ,  C07C45/81 ,  B01J19/00 ,  C07C45/50

    CPC分类号： C07C45/786 ,  B01D61/02 ,  B01D2311/25 ,  B01D2317/025 ,  B01D2325/30 ,  B01D2325/38 ,  B01J19/00 ,  B01J31/185 ,  B01J2231/321 ,  B01J2531/822 ,  C07C29/16 ,  C07C45/50 ,  C07C45/81 ,  C07C45/82 ,  C07C31/02 ,  C07C31/125 ,  C07C47/02

    摘要： The invention relates to a method for producing alcohols by homogeneously catalysed hydroformylation of olefins to aldehydes and subsequent hydration of the aldehydes. The invention further relates to a system for carrying out the method. The main focus is on the separation technique for work-up of the hydroformylation mixture. The problem addressed by the invention is that specifying a work-up method for hydroformylation mixtures that utilises the specific advantages of known separation technologies but at the same time largely avoids the specific disadvantages of said separation technologies. The most important objective is to create a catalyst separation system that is as complete and at the same time conservative as possible and that operates in a technically reliable manner and entails low investment and operating costs. The method should be unrestrictedly suitable for processing the reaction output from oxo systems in “world scale” format. The problem is solved by combining membrane separation units and a thermal separation unit, the thermal separation unit being operated in such a manner that 80% to 98% of the mass introduced with the product stream into the thermal separation unit exits the thermal separation unit again as a head product.

    摘要翻译： 本发明涉及通过将烯烃均匀催化加氢甲酰化成醛并随后醛的水合生产醇的方法。 本发明还涉及一种用于执行该方法的系统。 主要关注加氢甲酰化混合物后处理的分离技术。 本发明解决的问题是指定利用已知分离技术的具体优点但同时大大地避免了所述分离技术的具体缺点的加氢甲酰化混合物的后处理方法。 最重要的目标是创建一个尽可能完整且同时保守的催化剂分离系统，并以技术上可靠的方式运行，并且需要低投资和运营成本。 该方法不受限制地适用于以“世界规模”格式处理氧代系统的反应输出。 通过组合膜分离单元和热分离单元来解决问题，热分离单元以使得进入热分离单元的产物流引入的质量的80％至98％再次离开热分离单元的方式操作 作为头饰产品。