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    Process for making organic compounds and the organic compounds made therefrom
    1.
    发明授权
    Process for making organic compounds and the organic compounds made therefrom 有权
    制备有机化合物的方法和由其制备的有机化合物

    公开(公告)号：US08178682B2

    公开(公告)日：2012-05-15

    申请号：US12492716

    申请日：2009-06-26

    申请人： Yangang Liang ,  Shengxia Liu ,  Rui Wang ,  Jie Liu ,  Kelly Scott Chichak

    发明人： Yangang Liang ,  Shengxia Liu ,  Rui Wang ,  Jie Liu ,  Kelly Scott Chichak

    IPC分类号： C07D213/127

    CPC分类号： H01L51/0067 ,  C07D213/127 ,  C07D213/26 ,  C07D213/30

    摘要： An organic compound of formula E is made from a process comprising: reacting a compound of formula A and a compound of formula B to form a compound of formula C; and reacting one of the compound of formula C and the compound of formula D with a first boron esterification reagent to generate a boronic acid or a boronic ester to react with another of the compound of formula C and the compound of formula D to form a compound of formula E; wherein R1, R2, and R3 are, independently at each occurrence, a C1-C20 aliphatic radical, a C3-C20 aromatic radical, or a C3-C20 cycloaliphatic radical.

    摘要翻译： 式E的有机化合物由以下方法制得，该方法包括：使式A化合物与式B化合物反应以形成式C化合物; 并使式C化合物与式D化合物之一与第一硼酯化试剂反应，生成硼酸或硼酸酯与另一种式C化合物与式D化合物反应，形成化合物 的式E; 其中R1，R2和R3在每次出现时独立地为C 1 -C 20脂族基团，C 3 -C 20芳族基团或C 3 -C 20脂环族基团。

    ELECTRON-TRANSPORTING MATERIALS
    3.
    发明申请
    ELECTRON-TRANSPORTING MATERIALS 有权
    电子传输材料

    公开(公告)号：US20110155955A1

    公开(公告)日：2011-06-30

    申请号：US13060855

    申请日：2009-08-19

    申请人： Qing Ye ,  Jie Liu ,  Kelly Scott Chichak ,  Yanggang Liang

    发明人： Qing Ye ,  Jie Liu ,  Kelly Scott Chichak ,  Yanggang Liang

    IPC分类号： C07D401/10 ,  C09K11/06

    CPC分类号： C09K11/06 ,  C07D213/53 ,  C09K2211/1007 ,  C09K2211/1029 ,  H01L51/0067 ,  H01L51/5048 ,  H05B33/14 ,  Y10S428/917

    摘要： Compounds of formula I may be used in optoelectronic devices wherein R1, R2 and R4 are, independently at each occurrence, H, a C1-C20 aliphatic radical, a C3-C20 aromatic radical, or a C3-C20 cycloaliphatic radical; R3 is H or a is, independently at each occurrence, 1 or 2; b is, independently at each occurrence, an integer ranging from 0-3; c is, independently at each occurrence, an integer ranging from 0-4; Ar is independently at each occurrence, H, or heteroaryl; and at least two of Ar are heteroaryl.

    摘要翻译： 式I化合物可用于光电子器件，其中R 1，R 2和R 4在每次出现时独立地为H，C 1 -C 20脂族基，C 3 -C 20芳族基或C 3 -C 20环脂族基; R3是H或a是在每次出现时独立地为1或2; b在每次出现时独立地为0-3的整数; c在每次出现时独立地为0-4的整数; Ar在每次出现时独立地为H或杂芳基; 并且Ar中的至少两个是杂芳基。

    EMISSIVE POLYMERIC MATERIALS FOR OPTOELECTRONIC DEVICES
    6.
    发明申请
    EMISSIVE POLYMERIC MATERIALS FOR OPTOELECTRONIC DEVICES 有权
    用于光电器件的EMISSIVE聚合材料

    公开(公告)号：US20090156783A1

    公开(公告)日：2009-06-18

    申请号：US11957579

    申请日：2007-12-17

    申请人： Joseph John Shiang ,  Kelly Scott Chichak ,  James Anthony Cella ,  Larry Neil Lewis ,  Kevin Henry Janora

    发明人： Joseph John Shiang ,  Kelly Scott Chichak ,  James Anthony Cella ,  Larry Neil Lewis ,  Kevin Henry Janora

    IPC分类号： C08G73/00

    CPC分类号： C08G61/12 ,  C08G2261/142 ,  C08G2261/1526 ,  C08G2261/3142 ,  C08G2261/3162 ,  H01L51/0039 ,  H01L51/5012 ,  Y10S428/917

    摘要： Polymers including at least one structural unit derived from a compound of formula I or including at least one pendant group of formula II may be used in optoelectronic devices wherein R1, R3, R4 and R6 are independently hydrogen, alkyl, alkoxy, oxaalkyl, alkylaryl, aryl, arylalkyl, heteroaryl, substituted alkyl; substituted alkoxy, substituted oxaalkyl, substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted heteroaryl; R1a is hydrogen or alkyl; R2 is alkylene, substituted alkylene, oxaalkylene, CO, or CO2; R2a is alkylene; R5 is independently at each occurrence hydrogen, alkyl, alkylaryl, aryl, arylalkyl, alkoxy, carboxy, substituted alkyl; substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted alkoxy, X is halo, triflate, —B(OR1a)2, or  located at the 2, 5- or 2, 7-positions; and L is derived from phenylpyridine, tolylpyridine, benzothienylpyridine, phenylisoquinoline, dibenzoquinozaline, fluorenylpyridine, ketopyrrole, 2-(1-naphthyl)benzoxazole)), 2-phenylbenzoxazole, 2-phenylbenzothiazole, coumarin, thienylpyridine, phenylpyridine, benzothienylpyridine, 3-methoxy-2-phenylpyridine, thienylpyridine, phenylimine, vinylpyridine, pyridylnaphthalene, pyridylpyrrole, pyridylimidazole, phenylindole, derivatives thereof or combinations thereof.

    摘要翻译： 包括至少一种衍生自式I化合物或包含至少一个式II侧基的结构单元的聚合物可用于其中R 1，R 3，R 4和R 6独立地为氢，烷基，烷氧基，氧杂烷基，烷芳基， 芳基，芳基烷基，杂芳基，取代的烷基; 取代的烷氧基，取代的氧杂烷基，取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的杂芳基; R1a是氢或烷基; R2是亚烷基，取代的亚烷基，氧杂亚烷基，CO或CO 2; R2a是亚烷基; R5各自独立地为氢，烷基，烷基芳基，芳基，芳基烷基，烷氧基，羧基，取代的烷基; 取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的烷氧基，X是卤素，三氟甲磺酸酯，-B（OR1a）2，或位于2,5-或2,7-位; 苯基吡啶，苯并噻吩并吡啶，二苯并喹嗪，芴基吡啶，酮吡咯，2-（1-萘基）苯并恶唑）），2-苯基苯并恶唑，2-苯基苯并噻唑，香豆素，噻吩基吡啶，苯基吡啶，苯并噻吩基吡啶，3-甲氧基 - 2-苯基吡啶，噻吩基吡啶，苯基亚胺，乙烯基吡啶，吡啶基萘，吡啶基吡咯，吡啶基咪唑，苯基吲哚，其衍生物或其组合。

    Ketopyrroles useful as ligands in organic iridium compositions
    7.
    发明申请
    Ketopyrroles useful as ligands in organic iridium compositions 有权
    可用作有机铱组合物中配体的酮塔吡咯

    公开(公告)号：US20080027028A1

    公开(公告)日：2008-01-31

    申请号：US11504084

    申请日：2006-08-14

    申请人： Kelly Scott Chichak

    发明人： Kelly Scott Chichak

    IPC分类号： A61K31/695 ,  C07F7/02

    CPC分类号： H01L51/0085 ,  A61K31/695 ,  C07F7/1804 ,  H01L51/0035 ,  H01L51/42 ,  H01L51/5012 ,  Y02E10/549

    摘要： The present invention provides novel ketopyrroles having structure XXIV wherein R2 is independently at each occurrence a deuterium atom, a halogen, a nitro group, an amino group, a C3-C40 aromatic radical, a C1-C50 aliphatic radical, or a C3-C40 cyclcoaliphatic radical; “a” is an integer from 0 to 3; and X1 and X2 are independently at each occurrence a bromine atom, a hydroxy group, or the group OR10, and wherein the group R10 is independently at each occurrence a deuterium atom, a halogen, a nitro group, an amino group, a C3-C40 aromatic radical, a C1-C50 aliphatic radical, or a C3-C40 cyclcoaliphatic radical. Ketopyrroles XXIV are useful ligands for the preparation of Type (1) and Type (2) organic iridium compositions. In one aspect, the present invention provides deuterated analogs of XXIV. Organic iridium compositions are useful in the preparation optoelectronic devices, such as OLED devices and photovoltaic devices exhibiting enhanced performance characteristics.

    摘要翻译： 本发明提供具有结构ⅩⅩⅣ的新型酮吡咯，其中R 2 2在每次出现时独立地为氘原子，卤素，硝基，氨基，C 3 - C 40芳族基团，C 1 -C 50脂族基团或C 3 -C 30亚烷基 > 40脂环族基团; “a”是从0到3的整数; 并且X 1和X 2各自在每次出现时独立地为溴原子，羟基或OR 10，并且其中基团 R 10在每次出现时独立地为氘原子，卤素，硝基，氨基，C 3 -C 40芳族 自由基，C 1 -C 50脂肪族基团或C 3 -C 40脂环族基团。 酮基吡咯二酮XXIV是制备类型（1）和类型（2）有机铱组合物的有用配体。 一方面，本发明提供了XXIV的氘代类似物。 有机铱组合物可用于制备光电子器件，例如具有增强的性能特征的OLED器件和光伏器件。

    Method of making organic light emitting devices
    8.
    发明申请
    Method of making organic light emitting devices 有权
    制造有机发光装置的方法

    公开(公告)号：US20080026496A1

    公开(公告)日：2008-01-31

    申请号：US11637582

    申请日：2006-12-12

    申请人： Joseph John Shiang ,  Kevin Henry Janora ,  Gautam Parthasarathy ,  James Anthony Cella ,  Kelly Scott Chichak

    发明人： Joseph John Shiang ,  Kevin Henry Janora ,  Gautam Parthasarathy ,  James Anthony Cella ,  Kelly Scott Chichak

    IPC分类号： H01L21/00 ,  H01L29/08

    CPC分类号： H01L51/0043 ,  H01L51/0003 ,  H01L51/0035 ,  H01L51/0039 ,  H01L51/005 ,  H01L51/0085 ,  H01L51/56 ,  Y10T428/31511

    摘要： The present invention provides a method for the preparation of organic light-emitting devices comprising a bilayer structure made by forming a first film layer comprising an electroactive material and an INP precursor material, and exposing the first film layer to a radiation source under an inert atmosphere to generate an interpenetrating network polymer composition comprising the electroactive material. At least one additional layer is disposed on the reacted first film layer to complete the bilayer structure. The bilayer structure is comprised within an organic light-emitting device comprising standard features such as electrodes and optionally one or more additional layers serving as a bipolar emission layer, a hole injection layer, an electron injection layer, an electron transport layer, a hole transport layer, exciton-hole transporting layer, exciton-electron transporting layer, a hole transporting emission layer, or an electron transporting emission layer.

    摘要翻译： 本发明提供一种制备有机发光器件的方法，其包括通过形成包含电活性材料和INP前体材料的第一膜层制备的双层结构，并在惰性气氛下将第一膜层暴露于辐射源 以产生包含电活性材料的互穿网络聚合物组合物。 在反应的第一膜层上设置至少一个附加层以完成双层结构。 双层结构包括在包括标准特征的有机发光器件中，例如电极和可选地用作双极型​​发射层的一个或多个附加层，空穴注入层，电子注入层，电子传输层，空穴传输 层，激子 - 空穴传输层，激子 - 电子传输层，空穴传输发射层或电子传输发射层。

    Polymer for optoelectronic device
    9.
    发明授权
    Polymer for optoelectronic device 有权
    聚合物用于光电器件

    公开(公告)号：US08512879B2

    公开(公告)日：2013-08-20

    申请号：US12615748

    申请日：2009-11-10

    申请人： Qing Ye ,  Jie Lu ,  Kelly Scott Chichak

    发明人： Qing Ye ,  Jie Lu ,  Kelly Scott Chichak

    IPC分类号： H01L51/54 ,  C09K11/06

    CPC分类号： H01L51/0035 ,  C08G61/12 ,  C08G73/026 ,  C08G2261/1424 ,  C08G2261/148 ,  C08G2261/149 ,  C08G2261/1526 ,  C08G2261/3142 ,  C08G2261/3162 ,  C08G2261/411 ,  C09K11/06 ,  C09K2211/1416 ,  C09K2211/1425 ,  C09K2211/1433 ,  C09K2211/1466 ,  C09K2211/185 ,  H01L51/5012 ,  H05B33/14

    摘要： A polymer useful in an optoelectronic device comprises structural unit of formula I: wherein R1 is, independently at each occurrence, a C1-C20 aliphatic radical, a C3-C20 aromatic radical, or a C3-C20 cycloaliphatic radical; a is, independently at each occurrence, an integer ranging from 0-4; Ar1 is aryl or heteroaryl; Ar2 is fluorene; R2 is alkylene, substituted alkylene, oxaalkylene, CO, or CO2; R3, R4 and R5 are independently hydrogen, alkyl, alkoxy, alkylaryl, aryl, arylalkyl, heteroaryl, substituted alkyl; substituted alkoxy, substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted heteroaryl; and L is derived from phenylpyridine, tolylpyridine, benzothienylpyridine, phenylisoquinoline, dibenzoquinozaline, fluorenylpyridine, ketopyrrole, 2-(1-naphthyl)benzoxazole)), 2-phenylbenzoxazole, 2 phenylbenzothiazole, coumarin, thienylpyridine, phenylpyridine, benzothienylpyridine, 3 methoxy-2-phenylpyridine, thienylpyridine, phenylimine, vinylpyridine, pyridylnaphthalene, pyridylpyrrole, pyridylimidazole, phenylindole, derivatives thereof or combinations thereof.

    摘要翻译： 可用于光电子器件的聚合物包括式I的结构单元：其中R 1在每次出现时独立地为C 1 -C 20脂族基团，C 3 -C 20芳族基团或C 3 -C 20脂环族基团; a在每次出现时独立地为0-4的整数; Ar 1是芳基或杂芳基; Ar2是芴; R2是亚烷基，取代的亚烷基，氧杂亚烷基，CO或CO 2; R3，R4和R5独立地是氢，烷基，烷氧基，烷基芳基，芳基，芳基烷基，杂芳基，取代的烷基; 取代的烷氧基，取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的杂芳基; 苯基吡啶，苯并异喹啉，二苯并喹啉，芴基吡啶，酮吡咯，2-（1-萘基）苯并恶唑，2-苯基苯并恶唑，苯基苯并噻唑，香豆素，噻吩并吡啶，苯基吡啶，苯并噻吩基吡啶，3-甲氧基-2-苯基吡啶， 噻吩基吡啶，苯基亚胺，乙烯基吡啶，吡啶基萘，吡啶基吡咯，吡啶基咪唑，苯基吲哚，其衍生物或其组合。

    Functionalized polyfluorenes for use in optoelectronic devices
    10.
    发明授权
    Functionalized polyfluorenes for use in optoelectronic devices 有权
    用于光电器件的功能化聚芴

    公开(公告)号：US08053536B2

    公开(公告)日：2011-11-08

    申请号：US12328805

    申请日：2008-12-05

    申请人： Kelly Scott Chichak ,  Larry Neil Lewis ,  James Anthony Cella ,  Joseph John Shiang

    发明人： Kelly Scott Chichak ,  Larry Neil Lewis ,  James Anthony Cella ,  Joseph John Shiang

    IPC分类号： C08G61/00 ,  C08L65/00 ,  H01L33/00

    CPC分类号： C08G61/02 ,  C08G2261/1412 ,  C08G2261/1424 ,  C08G2261/143 ,  C08G2261/148 ,  C08G2261/1526 ,  C08G2261/5242 ,  C08G2261/95 ,  C09K11/06 ,  C09K2211/185 ,  H01L51/0039 ,  H01L51/0085 ,  H05B33/14

    摘要： The present invention relates to process comprising reacting a polyfluorenes comprising at least one structural group of formula I with an iridium (III) compound of formula II wherein R1 and R2 are independently alkyl, substituted alkyl, aryl, substituted aryl or a combination thereof; R5is H or CHO; R3 and R4 are independently hydrogen, alkyl, substituted alkyl, aryl, substituted aryl or a combination thereof; R11 and R12 taken together form a substituted or unsubstituted monocyclic or bicyclic heteroaromatic ring; R13 is independently at each occurrence halo, nitro, hydroxy, amino, alkyl, aryl, arylalkyl, alkoxy, substituted alkoxy, substituted alkyl, substituted aryl, or substituted arylalkyl; Ar is aryl, heteroaryl, substituted aryl, substituted heteroaryl, or a combination thereof; X is selected from a direct bond, alky, substituted alkyl, and combinations thereof; Y is CHO or NH2; Z is CHO or NH2 where Z does not equal Y; and p is 0, 1 or 2. The invention also relates to the polyfluorenes, which are products of the reaction, and the use of the polyfluorenes in optoelectronic devices.

    摘要翻译： 本发明涉及包括使包含至少一个式I结构基团的聚芴与式II的铱（III）化合物反应的方法，其中R 1和R 2独立地为烷基，取代的烷基，芳基，取代的芳基或其组合; R5is H或CHO; R3和R4独立地是氢，烷基，取代的烷基，芳基，取代的芳基或其组合; R11和R12一起形成取代或未取代的单环或双环杂芳环; R13各自独立地为卤素，硝基，羟基，氨基，烷基，芳基，芳基烷基，烷氧基，取代的烷氧基，取代的烷基，取代的芳基或取代的芳基烷基; Ar是芳基，杂芳基，取代的芳基，取代的杂芳基或其组合; X选自直接键，烷基，取代的烷基及其组合; Y为CHO或NH2; Z是CHO或NH2，其中Z不等于Y; 并且p为0,1或2.本发明还涉及作为反应产物的聚芴以及聚芴在光电器件中的应用。