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公开(公告)号：US5605868A
公开(公告)日：1997-02-25
申请号：US365811
申请日：1994-12-29
CPC分类号： C03C14/002 , C03C2214/03 , C03C2214/20 , Y10T428/2918 , Y10T428/2949
摘要： This invention is directed to the fabrication of SiC fiber reinforced, ceramic matrix composite articles exhibiting superior high temperature oxidative stability, those articles comprising:(a) a glass-ceramic matrix wherein alkali metal and/or alkaline earth metal aluminosilicate crystals constitute the predominant crystal phase;(b) a fiber reinforcing phase comprising SiC fibers coated with an alkali metal and/or alkaline earth metal sheet silicate entrained within said glass-ceramic matrix; and(c) a borosilicate glass phase dispersed as an intergranular glass within said glass-ceramic matrix, said borosilicate glass phase generally being present in an amount sufficient to provide an intergranular glass phase therein.
摘要翻译： 本发明涉及制备表现出优异的高温氧化稳定性的SiC纤维增强陶瓷基复合材料制品，所述制品包括：（a）玻璃 - 陶瓷基体，其中碱金属和/或碱土金属硅铝酸盐晶体构成主要晶体 相; （b）纤维增强相，其包含被夹在所述玻璃 - 陶瓷基体内的碱金属和/或碱土金属片状硅酸盐涂覆的SiC纤维; 和（c）在所述玻璃 - 陶瓷基体内作为晶间玻璃分散的硼硅酸盐玻璃相，所述硼硅酸盐玻璃相通常以足以在其中提供晶间玻璃相的量存在。
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公开(公告)号：US5652188A
公开(公告)日：1997-07-29
申请号：US287224
申请日：1994-08-08
申请人： Kenneth Chyung , Steven B. Dawes
发明人： Kenneth Chyung , Steven B. Dawes
CPC分类号： C03C14/002 , C04B35/803
摘要： The invention relates to fiber reinforced composite materials, and a method for making, in which ceramic, glass-ceramic or glass matrix precursor particles are coated with a layer of sheet silicate crystals, or precursors for sheet silicate crystals, and then combined with a fiber reinforcement phase disposed within the matrix consisting of amorphous or crystalline inorganic fibers. The method results in a composite material in which a substantially continuous layer of sheet silicate is provided on the matrix particles, resulting in a substantially continuous sheet silicate interface between the inorganic fibers and the ceramic, glass or glass-ceramic matrix.
摘要翻译： 本发明涉及纤维增强复合材料及其制造方法，其中陶瓷，玻璃 - 陶瓷或玻璃基质前体颗粒涂覆有一层硅酸盐晶体或硅酸铝晶体的前体，然后与纤维 强化相设置在由无定形或结晶无机纤维构成的基体内。 该方法产生复合材料，其中在基体颗粒上提供基本上连续的层状硅酸盐层，导致无机纤维和陶瓷，玻璃或玻璃 - 陶瓷基体之间的基本上连续的硅酸盐界面。
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公开(公告)号：US4948758A
公开(公告)日：1990-08-14
申请号：US456803
申请日：1989-12-26
CPC分类号： C04B35/80 , C03C14/002 , C04B41/4584 , C04B41/81 , C03C2214/02 , C03C2214/03 , C03C2214/20
摘要： Ceramic matrix composite articles comprising a ceramic, glass-ceramic or glass matrix and a fiber reinforcement phase disposed within the matrix consisting of amorphous or crystalline inorganic fibers, wherein there is provided, on or in close proximity to the surfaces of the inorganic fibers, a layer of sheet silicate crystals constituting a sheet silicate interface between the inorganic fibers and the ceramic, glass, or glass-ceramic matrix. Optionally, the composition of the matrix may be the same as the sheet silicate interface so that the matrix provides the sheet silicate layer.
摘要翻译： 包含陶瓷，玻璃陶瓷或玻璃基质的陶瓷基质复合制品以及设置在由无定形或结晶无机纤维构成的基体内的纤维增强相，其中在无机纤维的表面上或紧邻无机纤维的表面上提供 层状硅酸盐晶体构成无机纤维与陶瓷，玻璃或玻璃 - 陶瓷基体之间的硅酸盐界面。 任选地，基质的组成可以与片状硅酸盐界面相同，使得基质提供片状硅酸盐层。
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公开(公告)号：US4935387A
公开(公告)日：1990-06-19
申请号：US261671
申请日：1988-10-24
CPC分类号： C04B41/009 , C03C14/002 , C04B35/80 , C04B41/4584 , C04B41/81 , C03C2214/02 , C03C2214/03 , C03C2214/20 , Y10S428/902
摘要： Ceramic matrix composite articles comprising a ceramic, glass-ceramic or glass matrix and a fiber reinforcement phase disposed within the matrix consisting of amorphous or cyrstalline inorganic fibers, wherein there is provided, on or in close proximity to the surfaces of the inorganic fibers, a layer of sheet silicate crystals constituting a sheet silicate interface between the inorganic fibers and the ceramic, glass, or glass-ceramic matrix. Optionally, the composition of the matrix may be the same as the sheet silicate interface so that the matrix provides the sheet silicate layer.
摘要翻译： 包含陶瓷，玻璃陶瓷或玻璃基质的陶瓷基质复合制品和设置在由无定形或无环状无机纤维构成的基质内的纤维增强相，其中在无机纤维的表面上或附近提供无机纤维的 层状硅酸盐晶体构成无机纤维与陶瓷，玻璃或玻璃 - 陶瓷基体之间的硅酸盐界面。 任选地，基质的组成可以与片状硅酸盐界面相同，使得基质提供片状硅酸盐层。
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5.发明授权Coated inorganic fiber reinforcement materials and ceramic composites comprising the same 失效涂层无机纤维增强材料和包含其的陶瓷复合材料
公开(公告)号：US5198302A
公开(公告)日：1993-03-30
申请号：US512392
申请日：1990-04-23
申请人： Kenneth Chyung , Steven B. Dawes , Dale R. Wexell
发明人： Kenneth Chyung , Steven B. Dawes , Dale R. Wexell
IPC分类号： C04B35/18 , C03C14/00 , C04B35/584 , C04B35/622 , C04B35/80 , C04B41/45 , C04B41/52 , C04B41/81 , C04B41/89
CPC分类号： C04B41/009 , C03C14/002 , C04B35/62227 , C04B35/803 , C04B41/4584 , C04B41/52 , C04B41/81 , C04B41/89 , C03C2214/02 , C03C2214/03 , C03C2214/20 , Y10T428/2933
摘要： Silicon nitride reinforcing fibers provided with a protective surface coating comprising a boron nitride base layer and, optionally, an alumina overcoating, and fiber-reinforced ceramic matrix composite products incorporating the protectively-coated fibers, are disclosed. The composites offer significantly improved high temperature strength in combination with low dielectric constant and low dielectric loss characteristics.
摘要翻译： 公开了具有包含氮化硼基底层和任选的氧化铝外涂层的保护性表面涂层的氮化硅增强纤维和掺有保护性涂覆纤维的纤维增强陶瓷基复合材料。 复合材料提供显着改善的高温强度与低介电常数和低介电损耗特性相结合。
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6.发明授权
公开(公告)号：US4808460A
公开(公告)日：1989-02-28
申请号：US57531
申请日：1987-06-02
IPC分类号： B32B3/18 , B32B17/10 , B32B18/00 , C03B11/14 , C03B19/06 , C03C27/06 , C04B35/80 , C04B38/00 , E04C2/34 , B32B3/12
CPC分类号： B32B17/10577 , B32B18/00 , B32B3/18 , C03B11/14 , C03B19/06 , C03C27/06 , C04B35/80 , C04B38/0006 , C04B38/008 , E04C2/34 , C04B2237/04 , C04B2237/10 , C04B2237/34 , C04B2237/38 , C04B2237/62 , Y10T428/24149 , Y10T428/24661 , Y10T428/24694 , Y10T428/24727 , Y10T428/249969
摘要： This invention relates to the production of laminated structures consisting essentially of a light weight interior member prepared from a glass, glass-ceramic, or ceramic, an exterior member prepared from a glass, glass-ceramic, or ceramic, and a bonding member prepared from a glass, glass-ceramic, or ceramic. The light weight interior member may be composed of a porous body, a corrugated body, or a honeycomb body. In a preferred embodiment, at least one of said members is reinforced through the entrainment of ceramic fibers and/ or whiskers. In the most preferred embodiment, each exterior and interior member is reinforced through the entrainment of ceramic fibers and/or whiskers and the bonding member is reinforced through the entrainment of ceramic whiskers.
摘要翻译： 本发明涉及层压结构的制造，其主要由玻璃，玻璃陶瓷或陶瓷制成的轻质内部构件，由玻璃，玻璃陶瓷或陶瓷制成的外部构件以及由 玻璃，玻璃陶瓷或陶瓷。 轻质内部构件可以由多孔体，波纹体或蜂窝体构成。 在一个优选实施例中，通过夹带陶瓷纤维和/或晶须来增强至少一个所述构件。 在最优选的实施例中，通过夹带陶瓷纤维和/或晶须来增强每个外部和内部构件，并且通过夹带陶瓷晶须来增强粘合构件。
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公开(公告)号：US4755489A
公开(公告)日：1988-07-05
申请号：US943072
申请日：1986-12-18
CPC分类号： C03C14/002 , C03C10/0036 , C03C2214/02 , C03C2214/06 , C03C2214/20
摘要： The present invention is directed to the production of SiC whisker- and/or fiber-reinforced, internally-nucleated glass-ceramic matrix composite articles consisting essentially of 0.5-60% by weight SiC whiskers and/or 15-70% by volume ceramic fibers substantially uniformly distributed in a glass-ceramic matrix consisting essentially, in weight percent on the oxide basis, of 16-20%, CaO, 38.5-46% Al.sub.2 O.sub.3, 35-42% SiO.sub.2, and up to 10% total of at least one nucleating agent in the indicated proportion selected from the group consisting of 0.1-3% Cr.sub.2 O.sub.3, 0.25-3% HfO.sub.2, 2-5% MoO.sub.3, 0.25-3% Nb.sub.2 O.sub.5, 0.25-3% Ta.sub.2 O.sub.5, 0.25-3% WO.sub.3, and 1-10% ZrO.sub.2, wherein Al.sub.2 O.sub.3 is present in an amount which is at least 5 mole percent and up to 50 mole percent in excess of that present in stoichiometric triclinic anorthite, and wherein the predominant crystal phases in the glass-ceramic are triclinic anorthite and mullite and/or .alpha.-Al.sub.2 O.sub.3. Up to 1.5% As.sub.2 O.sub.3 may advantageously be included in the composition.
摘要翻译： 本发明涉及生产基本上由0.5-60％（重量）SiC晶须和/或15-70％（体积）陶瓷纤维组成的SiC晶须和/或纤维增强的，内部成核的玻璃 - 陶瓷基复合材料 基本上均匀分布在基本上以氧化物为基准重量百分比为16-20％，CaO，38.5-46％Al2O3,35-42％SiO2和至多10％总共的至少一种 指定比例的成核剂选自0.1-3％Cr2O3,0.25-3％HfO2,2.5％MoO3,0.25-3％Nb2O5,0.25-3％Ta2O5,0.23％WO3和1％ -10％的ZrO 2，其中Al 2 O 3以至少5摩尔％且高达50摩尔％的量存在于化学计量的三斜钙石中存在，并且其中玻璃 - 陶瓷中的主要结晶相是三斜长岩和 莫来石和/或α-Al2O3。 高达1.5％的As2O3可以有利地包括在组合物中。
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公开(公告)号：US4719151A
公开(公告)日：1988-01-12
申请号：US861303
申请日：1986-05-09
CPC分类号： F41H5/0435 , C03C14/002 , C03C27/00 , C03C27/06 , C04B35/645 , C04B37/001 , C04B37/005 , C04B37/042 , C03C2214/02 , C03C2214/20 , C04B2235/5208 , C04B2235/5244 , C04B2235/5248 , C04B2235/6567 , C04B2235/658 , C04B2237/04 , C04B2237/10 , C04B2237/32 , C04B2237/365 , C04B2237/38 , C04B2237/704 , C04B37/045 , Y10S428/911
摘要： There is disclosed a laminated ceramic structure including a facing member and a backing member, the two members being bonded together either directly or through an intermediate layer, the facing member being formed from a very hard ceramic such as a carbide having a KHN.sub.100 value in excess of 1000 kg/mm.sup.2, the backing member being a glass or glass-ceramic matrix having an enhanced capability or absorbing impact energy, preferably being fiber reinforced and having an energy absorbing capacity in excess of 10 KJ/m.sup.2.
摘要翻译： 公开了一种层叠陶瓷结构，其包括面向构件和背衬构件，两个构件直接地或通过中间层结合在一起，面对构件由非常硬的陶瓷形成，例如具有超过KHN100值的碳化物 1000kg / mm2的背衬构件是具有增强的能力或吸收冲击能量的玻璃或玻璃 - 陶瓷基体，优选地是纤维增强并具有超过10KJ / m 2的能量吸收能力。
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公开(公告)号：US4615987A
公开(公告)日：1986-10-07
申请号：US723572
申请日：1985-04-15
CPC分类号： C03C10/0036 , C03C14/002 , C03C2214/02 , C03C2214/06 , C03C2214/20 , Y10T428/252
摘要： The present invention is directed to SiC whisker and/or fiber reinforced glass-ceramic matrix composite articles wherein an alkaline earth aluminosilicate constitutes the predominant crystal phase. More particularly the composite articles will consist essentially of 10-60% by weight SiC whiskers and/or 15-70% by volume ceramic fibers and the glass-ceramic matrix will consist essentially, by weight on the oxide basis, of______________________________________ CaO 0-25 MgO 0-15 SrO 0-30 Na.sub.2 O 0-4 CaO + SrO 10-30 K.sub.2 O 0-6 Al.sub.2 O.sub.3 25-38 TiO.sub.2 0-12 SiO.sub.2 35-60 ZrO.sub.2 0-15 BaO 0-25 As.sub.2 O.sub.3 0-3 BaO + MgO + Na.sub.2 O + K.sub.2 O + TiO.sub.2 ZrO.sub.2 + As.sub.2 O.sub.3 0-30 ______________________________________ The preferred predominant crystal phase is selected from the group of anorthite and its pseudo-binaries, with mullite, cordierite, barium osumilite, and albite solid solution.
摘要翻译： 本发明涉及SiC晶须和/或纤维增强玻璃 - 陶瓷基复合材料制品，其中碱土铝硅酸盐构成主要晶相。 更具体地，复合制品将基本上由10-60重量％的SiC晶须和/或15-70体积％的陶瓷纤维组成，并且玻璃 - 陶瓷基体将基本上由氧化物基础上由-CaO 0- 25 MgO 0-15 -SrO 0-30 Na2O 0-4 -CaO + SrO 10-30 K2O 0-6 -Al2O3 25-38 TiO2 0-12 -SiO2 35-60 ZrO2 0-15 -BaO 0-25 As2O3 0 -3BaO + MgO + Na2O + K2O + TiO2ZrO2 + As2O3 0-30 - 优选的主要结晶相选自钙长石及其伪二进制，与莫来石，堇青石，奥斯米石和钠长石固溶体相组合。
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10.发明授权公开(公告)号：US06477299B1
公开(公告)日：2002-11-05
申请号：US09531053
申请日：2000-03-20
申请人： George H. Beall , Joel P. Carberry , Kenneth Chyung , Joseph E. Pierson , Kamjula P. Reddy , James E. Webb
发明人： George H. Beall , Joel P. Carberry , Kenneth Chyung , Joseph E. Pierson , Kamjula P. Reddy , James E. Webb
IPC分类号： G02B634
CPC分类号： C03C27/06 , G02B6/0218 , G02B6/12 , G02B6/4238 , G02B6/4239
摘要： The invention includes environmentally stable athermalized optical fiber gratings and methods of making such stabilized optical waveguide fiber grating. Stable humidity-resistant athermalized fiber Bragg gratings are provided by stabilizing a negative thermal expansion substrate and utilizing a durable frit to attach the fiber Bragg grating to the substrate.
摘要翻译： 本发明包括环境稳定的非热化光纤光栅和制造这种稳定的光波导光纤光栅的方法。 通过稳定负热膨胀基板并利用耐用的玻璃料将光纤布拉格光栅连接到基板来提供稳定的耐湿无热纤维布拉格光栅。
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