Abstract:
Apparatus for measuring gas comprising a gas sensing unit having a gas inlet membrane and being evacuated by a sputter ion pump via a restrictive conductance. Said conductance has a very low value relative to the pumping speed of the pump, whereby a change in the pumping speed of the pump causes substantially no change in the pumping speed with which the gas sensing unit is evacuated, so that the output signal of said gas sensing unit is a true reflection of the gas entering said inlet, without distortion which would otherwise be caused by changes in pumping speed of said pump.
Abstract:
A cryogenic apparatus comprises refrigeration means utilizing a two-stage expansion of compressed helium gas that circulates in a closed loop, whereby a first pumping stage can be maintained at a temperature in the range from 50.degree. K. to 80.degree. K. and a second pumping stage can be maintained at a colder temperature in the range from 10.degree. K. to 20.degree. K. The first pumping stage comprises an array of louvers of chevron configuration. These louvers enclose the second pumping stage, and serve as baffles to shield the pumping surfaces of the second stage from thermal radiation that would reduce the usable refrigeration capacity of the second stage for removing gases from a chamber to be evacuated. The chevroned baffles also protect a cryosorbent coating on the interior surfaces of the second stage from becoming iced or plugged by gas species that cryocondense at the higher temperature of the first stage. The assembly comprising the first-stage array of chevroned baffles surrounding the second-stage pumping surfaces may be disposed directly in the chamber to be evacuated, or may be mounted in a housing structure coupled to the chamber. The housing structure preferably has a radially bulging cylindrical configuration that permits substantially unimpeded conductance of gases from the chamber to the first-stage chevroned baffles.
Abstract:
In an apparatus for removing a selected first gas from a chamber at a controllably variable pumping speed while maintaining a substantially constant pumping speed for removing a second gas from the same chamber, a flow restricting device is disposed between the chamber and a device that pumps the first gas. The flow restricting device comprises a stationary member having an apertured portion through which the first gas can flow from the chamber to the pumping device. Restriction of the flow of the first gas to the pumping device is accomplished by covering the apertured portion of the stationary member with a movable member to the extent necessary to provide the desired pumping speed for the first gas. The stationary member is maintained at a cryogenic temperature higher than the condensation temperature of the first gas, but at a value at which the second gas condenses. In one embodiment, the stationary member is maintained at the desired cryogenic temperature by being mounted in intimate thermal contact with a cryogenic fluid reservoir. In an alternative embodiment, the stationary member is mounted in intimate thermal contact with the warmer stage of a two-stage cryogenic pump.
Abstract:
Two stage cryogenic pump having axially spaced baffle members for shielding the second stage from external thermal radiation while permitting substantially unimpeded gas flow from the inlet opening to the second stage.
Abstract:
Applying a thin film coating to the surface of a workpiece, in particular, applying a coating of titanium nitride to a klystron window by means of a crossed-field diode sputtering array. The array is comprised of a cohesive group of numerous small hollow electrically conducting cylinders and is mounted so that the open ends of the cylinders on one side of the group are adjacent a titanium cathode plate. The workpiece is mounted so as to face the open ends of the other side of the group. A magnetic field is applied to the array so as to be coaxial with the cylinders and a potential is applied across the cylinders and the cathode plate, the cylinders as an anode being positive with respect to the cathode plate. The cylinders, the cathode plate and the workpiece are situated in an atmosphere of nitrogen which becomes ionized such as by field emission because of the electric field between the cylinders and cathode plate, thereby establishing an anode-cathode discharge that results in sputtering of the titanium plate. The sputtered titanium coats the workpiece and chemically combines with the nitrogen to form a titanium nitride coating on the workpiece. Gas pressure, gas mixtures, cathode material composition, voltages applied to the cathode and anode, the magnetic field, cathode, anode and workpiece spacing, and the aspect ratio (ratio of length to inner diameter) of the anode cylinders, all may be controlled to provide consistent optimum thin film coatings of various compositions and thicknesses. Another facet of the disclosure is the coating of microwave components per se with titanium nitride to reduce multipactoring under operating conditions of the components.
Abstract:
Two-stage cryogenic pumping apparatus having individual plate members with cryosorbent coatings secured by removable fasteners to permit easy assembly and replacement of the plate members. The plate members are spaced apart to provide relatively unrestricted access to the cryosorbent material for the gases to be adsorbed thereon.
Abstract:
Applying a thin film coating to the surface of a workpiece, in particular, applying a coating of titanium nitride to a klystron window by means of a crossed-field diode sputtering array. The array is comprised of a cohesive group of numerous small hollow electrically conducting cylinders and is mounted so that the open ends of the cylinders on one side of the group are adjacent a titanium cathode plate. The workpiece is mounted so as to face the open ends of the other side of the group. A magnetic field is applied to the array so as to be coaxial with the cylinders and a potential is applied across the cylinders and the cathode plate, the cylinders as an anode being positive with respect to the cathode plate. The cylinders, the cathode plate and the workpiece are situated in an atmosphere of nitrogen which becomes ionized such as by field emission because of the electric field between the cylinders and cathode plate, thereby establishing an anode-cathode discharge that results in sputtering of the titanium plate. The sputtered titanium coats the workpiece and chemically combines with the nitrogen to form a titanium nitride coating on the workpiece. Gas pressure, gas mixtures, cathode material composition, voltages applied to the cathode and anode, the magnetic field, cathode, anode and workpiece spacing, and the aspect ratio (ratio of length to inner diameter) of the anode cylinders, all may be controlled to provide consistent optimum thin film coatings of various compositions and thicknesses. Another facet of the disclosure is the coating of microwave components per se with titanium nitride to reduce multipactoring under operating conditions of the components.
Abstract:
Applying a thin film coating to the surface of a workpiece, in particular, applying a coating of titanium nitride to a klystron window by means of a crossed-field diode sputtering array. The array is comprised of a cohesive group of numerous small hollow electrically conducting cylinders and is mounted so that the open ends of the cylinders on one side of the group are adjacent a titanium cathode plate. The workpiece is mounted so as to face the open ends of the other side of the group. A magnetic field is applied to the array so as to be coaxial with the cylinders and a potential is applied across the cylinders and the cathode plate, the cylinders as an anode being positive with respect to the cathode plate. The cylinders, the cathode plate and the workpiece are situated in an atmosphere of nitrogen which becomes ionized such as by field emission because of the electric field between the cylinders and cathode plate, thereby establishing an anode-cathode discharge that results in sputtering of the titanium plate. The sputtered titanium coats the workpiece and chemically combines with the nitrogen to form a titanium nitride coating on the workpiece. Gas pressure, gas mixtures, cathode material composition, voltages applied to the cathode and anode, the magnetic field, cathode, anode and workpiece spacing, and the aspect ratio (ratio of length to inner diameter) of the anode cylinders, all may be controlled to provide consistent optimum thin film coatings of various compositions and thicknesses. Another facet of the disclosure is the coating of microwave components per se with titanium nitride to reduce multipactoring under operating conditions of the components.
Abstract:
In a magnetically confined sputter-ion vacuum pump a multi-apertured anode electrode is interposed between a pair of reactive cathode electrode plates. An evacuable envelope encloses the anode and cathode electrodes and a magnetic circuit surrounds the vacuum envelope for producing a glow discharge confining magnetic field extending axially of the apertures in the anode. The reactive cathode plates include peripheral sealing flanges for compressing a sealing gasket into sealing engagement with a pair of sealing surfaces at opposite ends of a tubular main body portion of the envelope. A clamping ring structure, having a bolt circle formed therein, serves to clamp the two reactive cathode plates to the main body and also serves as an integral part of the magnetic circuit. Water coolant channels are brazed to the outer surfaces of the cathode plates for cooling same in use. The magnetic circuit includes a pair of ferrite magnets disposed outside the envelope on opposite sides of the cathodes and enclosed by a magnetic yoke to minimize the size and weight of the magnet and to reduce unwanted stray magnetic fields.