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    Quality of isobutene polymers in reactions with maleic anhydride
    4.
    发明授权
    Quality of isobutene polymers in reactions with maleic anhydride 失效
    异丁烯聚合物与马来酸酐反应的质量

    公开(公告)号：US4587307A

    公开(公告)日：1986-05-06

    申请号：US657383

    申请日：1984-10-03

    申请人： Klaus Bronstert ,  Waldhelm Hochstein ,  Hans-Henning Vogel ,  Hans P. Rath

    发明人： Klaus Bronstert ,  Waldhelm Hochstein ,  Hans-Henning Vogel ,  Hans P. Rath

    IPC分类号： C08F6/00 ,  C08F6/06 ,  C08F8/00 ,  C08F10/00 ,  C08F10/10

    CPC分类号： C08F10/00

    摘要： The processing properties of isobutene polymers when reacted with maleic anhydride are improved by a method in which these polymers are brought into contact, for an effective period,with aluminum oxide and/or a completely or partially hydrated aluminum oxide at 50.degree.-280.degree. C., and/orwith boron oxide and/or a completely or partially hydrated boron oxide and/or with titanium dioxide and/or a partially hydrated titanium dioxide and/or with a completely or partially hydrated silicon dioxide at 0.degree.-280.degree. C.

    摘要翻译： 异丁烯聚合物与马来酐反应时的加工性能通过这样一种方法得到改善：使聚合物在50〜-280℃与氧化铝和/或完全或部分水合的氧化铝接触有效的时间 和/或与氧化硼和/或完全或部分水合的氧化硼和/或与二氧化钛和/或部分水合的二氧化钛和/或完全或部分水合的二氧化硅在0-280℃下 。

    Catalyst systems for the cationic polymerization of isobutylene
    5.
    发明授权
    Catalyst systems for the cationic polymerization of isobutylene 失效
    用于异丁烯阳离子聚合的催化剂体系

    公开(公告)号：US4663406A

    公开(公告)日：1987-05-05

    申请号：US836649

    申请日：1986-03-05

    申请人： Klaus Bronstert ,  Waldhelm Hochstein ,  Heinrich Mohr ,  Gerhard Sandrock ,  Hans-Henning Vogel ,  Hans P. Rath

    发明人： Klaus Bronstert ,  Waldhelm Hochstein ,  Heinrich Mohr ,  Gerhard Sandrock ,  Hans-Henning Vogel ,  Hans P. Rath

    IPC分类号： C08F4/00 ,  C08F4/14 ,  C08F10/10

    CPC分类号： C08F10/10

    摘要： Isobutylene polymers are prepared by polymerizing the monomers at from 0.2 to 20 bar and from -130.degree. and +60.degree. C. in the presence of from 0.01 to 20 mmol of a boron halide catalyst system which contains as cocatalyst a carboxylic anhydride or carbonyl halide, preferably an aliphatic or aromatic, unsubstituted or halogen-substituted C.sub.4 -C.sub.18 -carboxylic anhydride of C.sub.2 -C.sub.12 -carbonyl halide and where appropriate also a customary polymerization accelerant in customary amounts, in the presence or absence of an inert solvent with dissipation of the heat of reaction.

    摘要翻译： 异丁烯聚合物通过在0.01至20巴和-130℃和+ 60℃下聚合单体制备，在0.01至20mmol卤化硼催化剂体系的存在下，其含有作为助催化剂的羧酸酐或羰基卤化物 ，优选C 2 -C 12 - 羰基卤化物的脂族或芳族未取代或卤素取代的C 4 -C 18羧酸酐，并且在适当的情况下，在常规量的情况下，在惰性溶剂存在或不存在下， 反应热。

    Transparent thermoplastic molding material, its preparation and its use
    6.
    发明授权
    Transparent thermoplastic molding material, its preparation and its use 失效
    透明热塑性成型材料，其制备及其应用

    公开(公告)号：US5036130A

    公开(公告)日：1991-07-30

    申请号：US347438

    申请日：1989-05-02

    申请人： Hans-Michael Walter ,  Klaus Bronstert ,  Hermann Gausepohl ,  Juergen Pohrt

    发明人： Hans-Michael Walter ,  Klaus Bronstert ,  Hermann Gausepohl ,  Juergen Pohrt

    IPC分类号： C08F4/42 ,  C08F4/48 ,  C08F297/04 ,  C08L25/06 ,  C08L53/00 ,  C08L53/02

    CPC分类号： C08L25/06 ,  C08L53/02

    摘要： A transparent thermoplastic molding material contains, based on A+B,A: from 5 to 95% by weight of polystyrene andB; from 95 to 5% by weight of a nonelastomeric star block copolymer which is composed of, based on B, b.sub.1 from 60 to 95% by weight of styrene and b.sub.2 from 5 to 40% by weight of one or more conjugated dienes of 4 or 5 carbon atoms and is prepared in a conventional manner by sequential anionic polymerization using one or more organolithium compounds as an initiator and in the presence of a solvent with subsequent coupling.In this process, component A is produced by conventional anionic polymerization using one or more organolithium compounds in the presence of an organic solvent.The molding material is prepared by mixing the components A and B, with or without C, in a conventional manner and is used for the production of moldings.

    摘要翻译： 透明热塑性成型材料以A + B为基准，A：5〜95重量％的聚苯乙烯和B; 95至5重量％的非弹性星形嵌段共聚物，其基于B，由60至95重量％的苯乙烯b1和b1为5至40重量％的一种或多种共轭二烯的4或4 5个碳原子，并且以常规方式通过使用一种或多种有机锂化合物作为引发剂并且在溶剂存在下随后偶联的顺序阴离子聚合制备。 在该方法中，通过在有机溶剂存在下使用一种或多种有机锂化合物的常规阴离子聚合制备组分A. 成型材料通过以常规方式混合具有或不具有C的组分A和B而制备，并用于制备模制品。

    Preparation of homo- and copolymers having terminal mercapto groups and their use
    7.
    发明授权
    Preparation of homo- and copolymers having terminal mercapto groups and their use 失效
    具有末端巯基的均聚物和共聚物的制备及其用途

    公开(公告)号：US4839434A

    公开(公告)日：1989-06-13

    申请号：US205178

    申请日：1988-06-10

    申请人： Klaus Bronstert ,  Hans-Michael Walter ,  Hans-Dieter Schwaben

    发明人： Klaus Bronstert ,  Hans-Michael Walter ,  Hans-Dieter Schwaben

    IPC分类号： C08C19/44 ,  C08F8/34 ,  C08F293/00 ,  C08F297/02 ,  C08F297/04

    CPC分类号： C08F293/00 ,  C08C19/44 ,  C08F8/34 ,  C08F2810/40

    摘要： Homo- or copolymers which have terminal mercapto groups, are composed of one or more monomers from the group consisting of butadiene, isoprene and styrene and are obtained by anionic polymerization of one or more of the stated monomers in the presence of one or more organolithium compounds followed by reaction (of the living anions) with an episulfide of the general formula I ##STR1## where R is hydrogen, alkyl of 1 to 18 carbon atoms or aryl of 6 to 10 carbon atoms, with the formation of one or more primary or secondary mercapto groups at the end of the polymer chain(s) are prepared by a process in which a thiolcarboxylic acid of the general formula II ##STR2## where R.sup.1 is hydrogen, alkyl of 1 to 10 carbon atoms or --CH.sub.2 --COOH and R.sup.2 is 0 or from 1 to 10 CH.sub.2 units, is added directly to the resulting reaction mixture in an amount of from 0.5 to 2 moles of the thiolcarboxylic acid per mole of episulfide, and the reaction product is subjected to an aftertreatment

    摘要翻译： 具有末端巯基的均聚物或共聚物由一种或多种来自丁二烯，异戊二烯和苯乙烯的单体组成，并且通过一种或多种所述单体在一种或多种有机锂化合物存在下的阴离子聚合获得 然后用活性阴离子与通式I的环硫化物反应，其中R是氢，1至18个碳原子的烷基或6至10个碳原子的芳基，形成一个或多个伯 或聚合物链末端的仲巯基通过以下方法制备：其中R 1为氢的通式II的硫醇羧酸，1至10个碳原子的烷基或-CH 2 -COOH，以及 R2为0或1至10个CH2单元，每摩尔环硫化物直接加入到所得反应混合物中的量为0.5至2摩尔硫羟羧酸，并将反应产物进行后处理

    Polymers based on conjugated dienes
    8.
    发明授权
    Polymers based on conjugated dienes 失效
    基于共轭二烯的聚合物

    公开(公告)号：US5494976A

    公开(公告)日：1996-02-27

    申请号：US110223

    申请日：1993-08-23

    申请人： Dietmar Bender ,  Klaus Bronstert ,  Helmut Mach ,  Martin Fischer

    发明人： Dietmar Bender ,  Klaus Bronstert ,  Helmut Mach ,  Martin Fischer

    IPC分类号： C08F8/12 ,  C08C19/02 ,  C08C19/26 ,  C08C19/40 ,  C08C19/42 ,  C08F8/00 ,  C08F8/30 ,  C08F8/42 ,  C08F236/10

    CPC分类号： C08C19/40 ,  C08C19/02 ,  C08C19/26 ,  C08C19/42 ,  C08F8/04 ,  C08F8/32 ,  C08F8/42 ,  C08F2800/20

    摘要： Polymers Ia and Ib carrying functional groups and obtainable byA)1. hydrogenation of the olefinic double bonds of a polymer IIa comprisinga) from 20 to 100% by weight of a conjugated diene,b) from 0 to 80% by weight of an aromatic vinyl compound, andc) from 0 to 20% by weight of further comonomers,to give the hydrogenated polymer IIb,2. metallation of IIb using an organoalkali metal compound to give IIc,3. reaction of IIc with a diaziridine III to give IId, and4. hydrolysis or alcoholysis of IId to give Ia, or byB)1. partial hydrogenation of IIa to give a partially hydrogenated polymer IIb',2. epoxidation of the double bonds of IIb' to give IIe, and3. reaction of IIe with a compound IV carrying functional groups, to give Ib,are suitable as viscosity index improvers for engine oils.

    摘要翻译： 聚合物Ia和Ib携带官能团，可通过A）获得聚合物IIa的烯烃双键，其包含a）20至100重量％的共轭二烯，b）0至80重量％的 芳族乙烯基化合物，和c）0-20重量％的另外的共聚单体，得到氢化聚合物IIb，2.使用有机碱金属化合物对IIb进行金属化，得到IIc，3.IIc与二氮丙啶III的反应，得到 IId和4. IId的水解或醇解以得到Ia，或通过B）1. IIa部分氢化得到部分氢化的聚合物IIb'，2.IIb'的双键的环氧化得到IIe，和3。 IIe与携带官能团的化合物IV反应得到Ib，适用于发动机油的粘度指数改进剂。

    Polymers based on conjugated dienes
    9.
    发明授权
    Polymers based on conjugated dienes 失效
    基于共轭二烯的聚合物

    公开(公告)号：US5614595A

    公开(公告)日：1997-03-25

    申请号：US543318

    申请日：1995-10-16

    申请人： Dietmar Bender ,  Klaus Bronstert ,  Helmut Mach ,  Martin Fischer

    发明人： Dietmar Bender ,  Klaus Bronstert ,  Helmut Mach ,  Martin Fischer

    IPC分类号： C08F8/12 ,  C08C19/02 ,  C08C19/26 ,  C08C19/40 ,  C08C19/42 ,  C08F8/00 ,  C08F8/30 ,  C08F8/42 ,  C08F236/10 ,  C08F8/04

    CPC分类号： C08C19/40 ,  C08C19/02 ,  C08C19/26 ,  C08C19/42 ,  C08F8/04 ,  C08F8/32 ,  C08F8/42 ,  C08F2800/20

    摘要： Polymers Ia and Ib carrying functional groups and obtainable byA) 1. hydrogenation of the olefinic double bonds of a polymer IIa comprisinga) from 20 to 100% by weight of a conjugated diene,b) from 0 to 80% by weight of an aromatic vinyl compound, andc) from 0 to 20% by weight of further comonomers,to give the hydrogenated polymer IIb, 2. metallation of IIb using an organoalkali metal compound to give IIc, 3. reaction of IIc with a diaziridine III to give IId, and 4. hydrolysis or alcoholysis of IId to give Ia, or byB) 1. partial hydrogenation of IIa to give a partially hydrogenated polymer IIb', 2. epoxidation of the double bonds of IIb' to give IIe, and 3. reaction of IIe with a compound IV carrying functional groups, to give Ib,are suitable as viscosity index improvers for engine oils.

    摘要翻译： 聚合物Ia和Ib携带官能团，可通过A）获得聚合物IIa的烯烃双键，其包含a）20至100重量％的共轭二烯，b）0至80重量％的 芳族乙烯基化合物，和c）0-20重量％的另外的共聚单体，得到氢化聚合物IIb，2.使用有机碱金属化合物对IIb进行金属化，得到IIc，3.IIc与二氮丙啶III的反应，得到 IId和4. IId的水解或醇解以得到Ia，或通过B）1. IIa部分氢化得到部分氢化的聚合物IIb'，2.IIb'的双键的环氧化得到IIe，和3。 IIe与携带官能团的化合物IV反应得到Ib，适用于发动机油的粘度指数改进剂。

    Alkadiene/vinylaromatic copolymers containing side groups, and their use
    10.
    发明授权
    Alkadiene/vinylaromatic copolymers containing side groups, and their use 失效
    含有侧基的二烯/乙烯基芳族共聚物及其用途

    公开(公告)号：US5290874A

    公开(公告)日：1994-03-01

    申请号：US854386

    申请日：1992-03-19

    申请人： Dietmar Bender ,  Klaus Bronstert ,  Helmut Mach

    发明人： Dietmar Bender ,  Klaus Bronstert ,  Helmut Mach

    IPC分类号： C08G61/04 ,  C08C19/00 ,  C08C19/30 ,  C08C19/42 ,  C08F8/00 ,  C08G61/00 ,  C10M143/16 ,  C08F287/00 ,  C08F293/00

    CPC分类号： C10M143/16 ,  C08C19/00 ,  C08C19/30 ,  C08C19/42 ,  C08F8/00 ,  C10M2205/04 ,  C10M2205/06 ,  C10M2205/10 ,  Y10S525/94

    摘要： The novel alkadiene/vinyl-aromatic copolymers which contain side groups and have a random, block-like or star-like structure and whose polymerized alkadiene comonomer units are partially or completely selectively hydrogenated, and which contain one or more side groups having one or more radicals capable of (4+2) cycloaddition (Diels-Alder reaction) with dienophiles are suitable as such as viscosity index (VI) improvers or can be used for the preparation of dispersant VI improvers. For this purpose, they are reacted with one or more dienophiles which are capable of a Diels-Alder (4+2) cycloaddition reaction and preferably contain strongly polar functional groups. The resulting selectively hydrogenated alkadiene/vinylaromatic copolymers having one or more side groups which constitute a (4+2) cycloadduct or a Diels-Alder adduct can be modified in their performance characteristics by further reaction with ammonia, an organic amine, an alkylene oxide, a polyalkylene oxide and/or a condensate of ammonia and/or an organic amine with an alkylene oxide.

    摘要翻译： 含有侧基且具有无规，嵌段状或星形结构且其聚合的链烯二
    烯共聚单体部分或全部被选择性氢化的新型链二烯/乙烯基 - 芳族共聚物，其含有一个或多个具有一个或多个 具有双亲性的（4 + 2）环加成（Diels-Alder反应）的基团是适合的，如粘度指数（VI）改进剂或可用于制备分散剂VI改进剂。 为此，它们与一种或多种能够进行狄尔斯 - 阿尔德（4 + 2）环加成反应并且优选含有极性极性官能团的亲二烯体反应。 可以通过与氨，有机胺，环氧烷烃等进一步反应，将具有构成（4 + 2）环加成物或狄尔斯 - 阿尔德加合物的一个或多个侧基的所得选择性氢化的二烯烃/乙烯基芳族共聚物的性能特性改性， 聚氧化烯和/或氨和/或有机胺与烯化氧的缩合物。