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公开(公告)号：US07049466B2
公开(公告)日：2006-05-23
申请号：US09962998
申请日：2001-09-25
申请人： Leonard Edward Bogan, Jr. , Daniel A. Bors , Fernando Antonio Pessoa Cavalcanti , Scott Han , Bradley Anson Jacobs , Frederick William Kaiser , Peter David Klugherz , Manhua Lin , Donald Lee Zolotorofe
发明人： Leonard Edward Bogan, Jr. , Daniel A. Bors , Fernando Antonio Pessoa Cavalcanti , Scott Han , Bradley Anson Jacobs , Frederick William Kaiser , Peter David Klugherz , Manhua Lin , Donald Lee Zolotorofe
IPC分类号： C07C51/16
CPC分类号： C07C253/24 , B01J2523/00 , C07C51/215 , C07C51/252 , C07C2523/28 , Y02P20/52 , C07C57/04 , C07C255/08 , B01J2523/55 , B01J2523/56 , B01J2523/64 , B01J2523/68
摘要： A method for producing an unsaturated carboxylic acid comprises: (a) contacting, in a reaction zone, an alkane with a catalyst containing a mixed metal oxide, under conditions which produce a product gas comprising the unsaturated carboxylic acid, unreacted alkane and a product alkene; (b) recovering unreacted alkane and product alkene from the product gas; and (c) recycling the recovered unreacted alkane and product alkene to the reaction zone; wherein the mixed metal oxide consists of a material having the formula AaMmNnXxOo wherein A is at least one element selected from the group consisting of molybdenum and tungsten, wherein M is at least one element selected from the group consisting of vanadium, cerium and chromium, wherein N is at least one element selected from the group consisting of tellurium, bismuth and selenium, wherein X is at least one element selected from the group consisting of niobium, tantalum, titanium, aluminum, zirconium, chromium, manganese, iron, ruthenium, cobalt, rhodium, nickel, platinum, bismuth, boron, indium, arsenic, germanium, tin, lithium, sodium, potassium, rubidium, cesium, francium, beryllium, magnesium, calcium, strontium, barium, hafnium, lead, phosphorus, promethium, europium, gadolinium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, gold, silver, palladium, gallium, zinc, praseodymium, rhenium, iridium, neodymium, yttrium, samarium and terbium, wherein 0.25
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2.发明授权公开(公告)号：US06710207B2
公开(公告)日：2004-03-23
申请号：US09962487
申请日：2001-09-25
申请人： Leonard Edward Bogan, Jr. , Scott Han , Bradley Anson Jacobs , Frederick William Kaiser , Peter David Klugherz , Manhua Lin , Richard David Link, III. , Michael William Linsen
发明人： Leonard Edward Bogan, Jr. , Scott Han , Bradley Anson Jacobs , Frederick William Kaiser , Peter David Klugherz , Manhua Lin , Richard David Link, III. , Michael William Linsen
IPC分类号： C07C5116
CPC分类号： C07C253/24 , B01J2523/00 , C07C51/215 , C07C51/252 , Y02P20/52 , Y02P20/582 , C07C57/04 , C07C255/08 , B01J2523/55 , B01J2523/56 , B01J2523/64 , B01J2523/68
摘要： Unsaturated carboxylic acids are produced by the vapor phase catalytic oxidation of mixtures of alkenes and alkanes in the presence of a catalyst containing a mixed metal oxide. Similarly, unsaturated nitrites are produced by the vapor phase catalytic oxidation of alkenes or mixtures of alkenes and alkanes and ammonia in the presence of a catalyst containing a mixed metal oxide.
摘要翻译： 在含有混合金属氧化物的催化剂存在下，通过气相催化氧化烯烃和烷烃的混合物来生产不饱和羧酸。 类似地，在含有混合金属氧化物的催化剂的存在下，通过烯烃或烯烃和烷烃和氨的混合物的气相催化氧化产生不饱和亚硝酸盐。
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3.发明授权公开(公告)号：US06989460B2
公开(公告)日：2006-01-24
申请号：US10722281
申请日：2003-11-25
申请人： Leonard Edward Bogan, Jr. , Scott Han , Bradley Anson Jacobs , Frederick William Kaiser , Peter David Klugherz , Manhua Lin , Richard David Link, III , Michael William Linsen
发明人： Leonard Edward Bogan, Jr. , Scott Han , Bradley Anson Jacobs , Frederick William Kaiser , Peter David Klugherz , Manhua Lin , Richard David Link, III , Michael William Linsen
IPC分类号： C07C253/24
CPC分类号： C07C253/24 , B01J2523/00 , C07C51/215 , C07C51/252 , Y02P20/52 , Y02P20/582 , C07C57/04 , C07C255/08 , B01J2523/55 , B01J2523/56 , B01J2523/64 , B01J2523/68
摘要： Unsaturated carboxylic acids are produced by the vapor phase catalytic oxidation of mixtures of alkenes and alkanes in the presence of a catalyst containing a mixed metal oxide. Similarly, unsaturated nitriles are produced by the vapor phase catalytic oxidation of alkenes or mixtures of alkenes and alkanes and ammonia in the presence of a catalyst containing a mixed metal oxide.
摘要翻译： 在含有混合金属氧化物的催化剂存在下，通过气相催化氧化烯烃和烷烃的混合物来生产不饱和羧酸。 类似地，在含有混合金属氧化物的催化剂的存在下，通过烯烃或烯烃和烷烃和氨的混合物的气相催化氧化制备不饱和腈。
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公开(公告)号：US06180242B2
公开(公告)日：2001-01-30
申请号：US09549846
申请日：2000-04-14
IPC分类号： B32B3106
CPC分类号： B32B7/12 , B32B21/042 , B32B21/06 , B32B21/08 , B32B27/08 , B32B27/10 , B32B29/005 , B32B38/164 , C08L31/02 , C08L2666/28 , C09J5/06 , C09J131/02 , C09J2431/00 , Y10T428/277 , Y10T428/28 , Y10T428/2835 , Y10T428/2848 , Y10T428/2852 , Y10T428/2891 , Y10T428/31536 , Y10T428/31576 , Y10T428/31895
摘要： An aqueous adhesive composition for wet lamination of substrate layers to form a laminated article includes from about 40 weight percent to about 65 weight percent solids dispersed in an aqueous medium, wherein the solids include a polymer having repeating units derived from a vinyl ester monomer and having a glass transition temperature of about −15° C. to about +15° C.; and from about 0.1 parts by weight to about 40 parts by weight of a plasticizer compound per 100 parts by weight of the polymer. A method for making a laminated article includes applying a wet layer of the aqueous laminating adhesive composition of the to a first substrate layer; covering the wet layer of adhesive composition with a second substrate layer; and drying the layer of adhesive composition to form the laminated article. A laminated article includes two substrate layers bonded together by an interposed layer of the dried adhesive composition.
摘要翻译： 用于湿法层压基底层以形成层压制品的水性粘合剂组合物包含分散在水性介质中的约40重量％至约65重量％的固体，其中固体包括具有衍生自乙烯基酯单体的重复单元的聚合物，并且具有 约-15℃至约+ 15℃的玻璃化转变温度。 和每100重量份聚合物约0.1重量份至约40重量份的增塑剂化合物。 制造层压制品的方法包括将第一衬底层的水性层压粘合剂组合物的湿层施加到第一衬底层; 用第二基底层覆盖粘合剂组合物的湿层; 并干燥粘合剂组合物层以形成层压制品。 层压制品包括通过干燥的粘合剂组合物的中间层粘合在一起的两个基材层。
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公开(公告)号：US6087425A
公开(公告)日：2000-07-11
申请号：US198336
申请日：1994-02-18
CPC分类号： C09J5/06 , B32B7/12 , C09J131/02 , C08L31/02 , C09J2431/00 , Y10T428/277 , Y10T428/28 , Y10T428/2835 , Y10T428/2848 , Y10T428/2852 , Y10T428/2891 , Y10T428/31536 , Y10T428/31576 , Y10T428/31895
摘要： An aqueous adhesive composition for wet lamination of substrate layers to form a laminated article includes from about 40 weight percent to about 65 weight percent solids dispersed in an aqueous medium, wherein the solids include a polymer having repeating units derived from a vinyl ester monomer and having a glass transition temperature of about -15.degree. C. to about +15.degree. C.; and from about 0.1 parts by weight to about 40 parts by weight of a plasticizer compound per 100 parts by weight of the polymer. A method for making a laminated article includes applying a wet layer of the aqueous laminating adhesive composition of the to a first substrate layer; covering the wet layer of adhesive composition with a second substrate layer; and drying the layer of adhesive composition to form the laminated article. A laminated article includes two substrate layers bonded together by an interposed layer of the dried adhesive composition.
摘要翻译： 用于湿法层压基底层以形成层压制品的水性粘合剂组合物包含分散在水性介质中的约40重量％至约65重量％的固体，其中固体包括具有衍生自乙烯基酯单体的重复单元的聚合物，并且具有 约-15℃至约+15℃的玻璃化转变温度。 和每100重量份聚合物约0.1重量份至约40重量份的增塑剂化合物。 制造层压制品的方法包括将第一衬底层的水性层压粘合剂组合物的湿层施加到第一衬底层; 用第二基底层覆盖粘合剂组合物的湿层; 并干燥粘合剂组合物层以形成层压制品。 层压制品包括通过干燥的粘合剂组合物的中间层粘合在一起的两个基材层。
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公开(公告)号：US06203916B1
公开(公告)日：2001-03-20
申请号：US09549847
申请日：2000-04-14
IPC分类号： B32B712
CPC分类号： B32B7/12 , B32B21/042 , B32B21/06 , B32B21/08 , B32B27/08 , B32B27/10 , B32B29/005 , B32B38/164 , C08L31/02 , C08L2666/28 , C09J5/06 , C09J131/02 , C09J2431/00 , Y10T428/277 , Y10T428/28 , Y10T428/2835 , Y10T428/2848 , Y10T428/2852 , Y10T428/2891 , Y10T428/31536 , Y10T428/31576 , Y10T428/31895
摘要： An aqueous adhesive composition for wet lamination of substrate layers to form a laminated article includes from about 40 weight percent to about 65 weight percent solids dispersed in an aqueous medium, wherein the solids include a polymer having repeating units derived from a vinyl ester monomer and having a glass transition temperature of about −15° C. to about +15° C.; and from about 0.1 parts by weight to about 40 parts by weight of a plasticizer compound per 100 parts by weight of the polymer. A method for making a laminated article includes applying a wet layer of the aqueous laminating adhesive composition of the to a first substrate layer; covering the wet layer of adhesive composition with a second substrate layer; and drying the layer of adhesive composition to form the laminated article. A laminated article includes two substrate layers bonded together by an interposed layer of the dried adhesive composition.
摘要翻译： 用于湿法层压基底层以形成层压制品的水性粘合剂组合物包含分散在水性介质中的约40重量％至约65重量％的固体，其中固体包括具有衍生自乙烯基酯单体的重复单元的聚合物，并且具有 约-15℃至约+ 15℃的玻璃化转变温度。 和每100重量份聚合物约0.1重量份至约40重量份的增塑剂化合物。 制造层压制品的方法包括将第一衬底层的水性层压粘合剂组合物的湿层施加到第一衬底层; 用第二基底层覆盖粘合剂组合物的湿层; 并干燥粘合剂组合物层以形成层压制品。 层压制品包括通过干燥的粘合剂组合物的中间层粘合在一起的两个基材层。
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公开(公告)号：US5652289A
公开(公告)日：1997-07-29
申请号：US540682
申请日：1995-10-11
IPC分类号： C08F2/08 , C08F218/04 , C08F220/12 , C08K5/06
CPC分类号： C08F220/12 , C08F218/04
摘要： A method for making a polymer, includes the step of polymerizing a mixture of a vinyl ester monomer, a (C.sub.1 -C.sub.12)alkyl (meth)acrylate monomer and a mono ethylenically unsaturated polar monomer by free radical initiated polymerization in an aqueous medium and in free presence of a colloidal stabilizer, a first poly(alkoxylated) alkyl phenol having less than or equal to 12 alkoxyl units per molecule and a second poly(alkoxylated) alkyl phenol having greater than 12 alkoxyl units per molecule, to form an emulsion of the polymer in the aqueous medium.
摘要翻译： 制备聚合物的方法包括通过自由基引发聚合在水性介质中聚合乙烯基酯单体，（甲基）丙烯酸（C 1 -C 12）烷基酯（甲基）丙烯酸烷基酯单体和单烯属不饱和极性单体的混合物的步骤 胶体稳定剂的自由存在，每分子具有小于或等于12个烷氧基单元的第一聚（烷氧基化）烷基苯酚和每分子具有大于12个烷氧基单元的第二聚（烷氧基化）烷基苯酚，以形成 聚合物在水性介质中。
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8.发明授权Dispersible, high speed book casing-in vinyl ester/(meth)acrylate adhesive 失效分散，高速书套管乙烯基酯/（甲基）丙烯酸酯粘合剂
公开(公告)号：US6120638A
公开(公告)日：2000-09-19
申请号：US931842
申请日：1997-09-17
IPC分类号： B42C9/00 , C09J151/00 , C09J7/00
CPC分类号： B42C9/0006 , C09J151/003
摘要： An improved method for forming book casing is provided through an adhesive composition. The adhesive provides surprising adhesion to both paper and plastic films with also allowing higher processing rates. Book casings produced with the adhesives are also claimed.
摘要翻译： 通过粘合剂组合物提供了一种用于形成书套的改进方法。 粘合剂对纸张和塑料膜都提供惊人的粘合力，同时也允许更高的处理速度。 还要求使用粘合剂生产的预订外壳。
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公开(公告)号：US5652293A
公开(公告)日：1997-07-29
申请号：US551703
申请日：1995-10-25
IPC分类号： C08F2/22 , C08F218/04 , C08F2/16
CPC分类号： C08F218/04
摘要： A method for making a polymer includes adding a first portion of a colloidal stabilizer to an aqueous medium, adding a monomer mixture, said monomer mixture including a monomer charge and a second portion of colloidal stabilizer and said monomer charge including from about 40 parts by weight to about 70 parts by weight of a vinyl ester monomer per 100 parts by weight monomer charge and from about 30 parts by weight to about 60 parts by weight of a (C.sub.1 -C.sub.12)alkyl (meth)acrylate monomer per 100 parts by weight monomer charge, to the aqueous medium and polymerizing the monomers to form an emulsion of the polymer in the aqueous medium.
摘要翻译： 制备聚合物的方法包括将第一部分胶体稳定剂加入水性介质中，加入单体混合物，所述单体混合物包括单体进料和第二部分胶体稳定剂，所述单体进料包含约40重量份 至约70重量份的乙烯基酯单体/ 100重量份单体电荷和约30重量份至约60重量份的（甲基）丙烯酸（C 1 -C 12）烷基酯单体/ 100重量份单体 向水介质中加入并聚合单体以在水性介质中形成聚合物的乳液。
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