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    Michael reaction
    4.
    发明授权
    Michael reaction 失效
    迈克尔反应

    公开(公告)号：US5350875A

    公开(公告)日：1994-09-27

    申请号：US156755

    申请日：1993-11-23

    Applicant: Govindarajulu Kumar ,  Mahmood Sabahi

    Inventor： Govindarajulu Kumar ,  Mahmood Sabahi

    IPC: C07C67/347 ,  C07C69/34

    CPC classification number: C07C67/347

    Abstract: Compounds varying from liquids to solids can be prepared via a reaction in which at least one Michael donor is reacted with one or more Michael acceptors in the presence of an undissolved basic compound as the catalyst.

    Abstract translation: 从液体到固体的化合物可以通过其中至少一种迈克尔供体在未溶解的碱性化合物作为催化剂的存在下与一种或多种迈克尔受体反应的反应来制备。

    Process for preparing Michael addition products
    5.
    发明授权
    Process for preparing Michael addition products 失效
    迈克尔加成产物的制备方法

    公开(公告)号：US5347043A

    公开(公告)日：1994-09-13

    申请号：US169261

    申请日：1993-12-20

    Applicant: Mahmood Sabahi ,  Robert G. Irwin

    Inventor： Mahmood Sabahi ,  Robert G. Irwin

    IPC: C07C67/343 ,  C07C69/34 ,  C07C67/00 ,  C07C67/465 ,  C07C69/38

    CPC classification number: C07C67/343

    Abstract: Dialkyl malonate/alkyl acrylate Michael addition product mixtures having at least three acceptor moieties in a substantial number of the molecules can be consistently prepared without the need for long reaction times or the use of a large excess of the acceptor when the reaction is effected by gradually adding one molar proportion of a dialkyl malonate to at least three molar proportions of an alkyl acrylate which has been preheated to 60.degree.-80.degree. C. in admixture with an initiator and a phase transfer catalyst. In a preferred embodiment, the preheated mixture is maintained at 60.degree.-80.degree. C. for at least one hour before the dialkyl malonate is added in order to increase the percentage of product composed of the heavier components.

    Abstract translation: 丙二酸二烷基酯/丙烯酸烷基酯在相当数量的分子中具有至少三个受体部分的迈克尔加成产物混合物可以一致地制备，而不需要长的反应时间或当反应通过逐渐地进行反应时使用大量过量的受体 将1摩尔比例的丙二酸二烷基酯加入到至少三摩尔比例的丙烯酸烷基酯中，该丙烯酸烷基酯与引发剂和相转移催化剂混合预热至60-80℃。 在优选的实施方案中，将预热的混合物在加入丙二酸二烷基酯之前保持在60-80℃至少1小时以增加由较重组分组成的产物的百分比。

    Diimines and secondary diamines
    7.
    发明授权
    Diimines and secondary diamines 有权
    二亚胺和仲胺

    公开(公告)号：US08212078B2

    公开(公告)日：2012-07-03

    申请号：US11909824

    申请日：2005-12-30

    Applicant: John Y. Lee ,  Paul L. Wiggins ,  Judit Orgad ,  Mahmood Sabahi ,  Vernon O. Brandt ,  David W. Owens

    Inventor： John Y. Lee ,  Paul L. Wiggins ,  Judit Orgad ,  Mahmood Sabahi ,  Vernon O. Brandt ,  David W. Owens

    IPC: C07C211/00

    CPC classification number: C07C211/12 ,  C07C211/51 ,  C08G18/10 ,  C08G18/3234 ,  C08G18/324 ,  C08G18/325 ,  C08G18/5024 ,  C08G18/6685 ,  C08G18/7671 ,  Y02P20/582

    Abstract: This invention provides aromatic diimines where the diimines have imino groups with at least two carbon atoms, and either are in the form of one benzene ring having two imino groups on the ring, which imino groups are meta or para relative to each other, and in which each position ortho to an imino group bears a hydrocarbyl group, or are in the form of two benzene rings connected by an alkylene bridge and having one imino group on each ring, and in which each position ortho to an imino group bears a hydrocarbyl group. This invention also provides aromatic secondary diamines where the diamines have amino hydrocarbyl groups with at least two carbon atoms, and either are in the form of one benzene ring having two amino groups on the ring, which amino groups are meta or para relative to each other, and in which each position ortho to an amino group bears a hydrocarbyl group, or are in the form of two benzene rings connected by an alkylene bridge and having one amino group on each ring, and in which each position ortho to an amino group bears a hydrocarbyl group. Also provided are processes for forming diimines and secondary diamines from primary diamines, including the aromatic diimines and aromatic secondary diamines of the invention.

    Abstract translation: 本发明提供芳族二亚胺，其中二亚胺具有至少两个碳原子的亚氨基，并且是环上具有两个亚氨基的一个苯环的形式，该亚氨基相对于彼此是间位或对位的，并且在 其中每个位于亚氨基的邻位具有烃基，或者是由亚烷基桥连接并在每个环上具有一个亚氨基的两个苯环的形式，并且其中亚氨基的邻位各有一个烃基 。 本发明还提供芳族仲二胺，其中二胺具有至少两个碳原子的氨基烃基，并且是环上具有两个氨基的一个苯环的形式，该氨基相对于彼此是间位或对位的 并且其中氨基的每个位置具有烃基，或者为两个苯环的形式，其通过亚烷基桥连接并且在每个环上具有一个氨基，并且其中氨基的邻位各自承载 烃基。 还提供了由伯二胺形成二亚胺和仲二胺的方法，包括本发明的芳族二亚胺和芳族仲二胺。

    DIIMINES AND SECONDARY DIAMINES
    9.
    发明申请
    DIIMINES AND SECONDARY DIAMINES 失效
    DIIMINES和次级DIAMINES

    公开(公告)号：US20080033210A1

    公开(公告)日：2008-02-07

    申请号：US11855839

    申请日：2007-09-14

    Applicant: John Lee ,  Paul Wiggins ,  Judith Orgad ,  Mahmood Sabahi

    Inventor： John Lee ,  Paul Wiggins ,  Judith Orgad ,  Mahmood Sabahi

    IPC: C07C211/51 ,  C07C211/35

    CPC classification number: C07C211/12 ,  C07C211/51 ,  C08G18/10 ,  C08G18/3234 ,  C08G18/324 ,  C08G18/325 ,  C08G18/5024 ,  C08G18/6685 ,  C08G18/7671 ,  Y02P20/582

    Abstract: This invention provides aromatic diimines which have imino hydrocarbylidene groups with at least two carbon atoms, and aromatic secondary diamines which have amino hydrocarbyl groups with at least two carbon atoms. Both the aromatic diimines and the aromatic secondary diamines either are in the form of one phenyl ring, or are in the form of two phenyl rings connected by an alkylene bridge; each position ortho to an imino group or an amino group bears a hydrocarbyl group. When in the form of one phenyl ring, there are two imino groups on the ring or two amino groups on the ring; the imino groups or amino groups are meta or para relative to each other. When in the form of two phenyl rings connected by an alkylene bridge, there is either one imino group or one amino group on each phenyl ring. Also provided are processes for forming diimines and secondary diamines.

    Abstract translation: 本发明提供具有至少两个碳原子的亚氨基亚烃基的芳族二亚胺和具有至少两个碳原子的氨基烃基的芳族仲二胺。 芳族二亚胺和芳族仲胺都是一个苯环的形式，或者是由亚烷基桥连接的两个苯环的形式; 亚氨基或氨基的邻位各为一个烃基。 当以一个苯环的形式，环上有两个亚氨基或环上两个氨基; 亚氨基或氨基相对于彼此是间位或对位的。 当以亚烷基桥连接的两个苯环的形式，每个苯环上有一个亚氨基或一个氨基。 还提供了形成二亚胺和仲二胺的方法。

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