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    Fenton and Fenton-Like System Hardening Agent and Usage Thereof
    9.
    发明申请
    Fenton and Fenton-Like System Hardening Agent and Usage Thereof 审中-公开
    芬顿和芬顿系统硬化剂及其用途

    公开(公告)号：US20120305497A1

    公开(公告)日：2012-12-06

    申请号：US13578244

    申请日：2010-10-18

    申请人： Jun Ma ,  Liwei Chen ,  Xuchun Li ,  Jing Zhang ,  Yinghong Guan ,  Jingyun Fang

    发明人： Jun Ma ,  Liwei Chen ,  Xuchun Li ,  Jing Zhang ,  Yinghong Guan ,  Jingyun Fang

    IPC分类号： C02F1/72 ,  C07C211/51 ,  C01B21/16 ,  C07C239/08 ,  C01B17/62 ,  C01B21/14

    CPC分类号： C02F1/72 ,  C02F1/70 ,  C02F2209/06 ,  C02F2305/026

    摘要： Fenton and Fenton-like system enhancing agent and the usage thereof are provided. It relates to a water treatment enhancer (enhancing agent) and the usage thereof. It widens water pH range of Fenton and Fenton-like system reaction. It reduces amount of Fe2+ required for Fenton reaction. It increases rate of Fenton-like reaction. The enhancing agent is selected from sodium sulfite, lithium sulfite, potassium sulfite, magnesium sulfite, calcium sulfite, hydroxylamine hydrochloride, hydroxylamine perchlorate, hydroxylamine sulfate, hydrazine, N,N-diethylhydroxylamine, amino ethanolamine, hydroxylamine solution or N,N,N′,N′-tetrasubstituted p-phenylenediamine. The method of use of enhancing agent comprises the steps of: adding Fenton or Fenton-like system enhancing agent, an agent for enhancement and hydrogen peroxide into water subject to treatment; and mixing and allowing reaction. The enhancing agent can increase the rate of reaction for the water treatment and reduce the dosage of the agent for enhancement.

    摘要翻译： 提供芬顿和芬顿类系统增强剂及其用途。 它涉及一种水处理增强剂（增强剂）及其用途。 它扩大了Fenton和Fenton样系统反应的水pH范围。 减少芬顿反应所需的Fe2 +量。 它增加芬顿样反应的速率。 增强剂选自亚硫酸钠，亚硫酸锂，亚硫酸钾，亚硫酸镁，亚硫酸钙，盐酸羟胺，高氯酸羟胺，硫酸羟胺，肼，N，N-二乙基羟胺，氨基乙醇胺，羟胺溶液或N，N，N' ，N'-四取代对苯二胺。 使用增强剂的方法包括以下步骤：将Fenton或Fenton样系统增强剂，增强剂和过氧​​化氢加入待处理的水中; 并混合并使反应。 增强剂可以增加水处理的反应速率，并减少增加剂的用量。

    PROCESS FOR THE PRODUCTION OF METHYLENE-BRIDGED POLYPHENYL POLYAMINES
    10.
    发明申请
    PROCESS FOR THE PRODUCTION OF METHYLENE-BRIDGED POLYPHENYL POLYAMINES 有权
    制备亚甲基桥联聚苯胺的方法

    公开(公告)号：US20110282099A1

    公开(公告)日：2011-11-17

    申请号：US13133410

    申请日：2009-11-26

    申请人： Christopher John Mitchell ,  Avelino Corma Canos ,  Robert Henry Carr ,  Pablo Botella Asuncion

    发明人： Christopher John Mitchell ,  Avelino Corma Canos ,  Robert Henry Carr ,  Pablo Botella Asuncion

    IPC分类号： C07C211/51

    CPC分类号： C07C209/60 ,  C07C209/78 ,  C07C211/50

    摘要： A process for providing methylene-bridged polyphenyl polyamines from aniline and formaldehyde according to the invention comprises the subsequent steps ofa) condensing aniline and formaldehyde, providing a condensate, the molar ratio of aniline to formaldehyde being chosen in the range of 2 to 3.5;b) reacting, in a first catalytic reaction step, at a reaction temperature within the range of about 30° C. to about 100° C., said condensate over a solid catalyst being chosen from the group consisting of clays, silicates, silica-aluminas and ion exchange resins, whereby an intermediate mixture is provided, the intermediate mixture comprising amino benzyl amines;c) converting, in a subsequent catalytic reaction step, at a temperature within the range of about 70° C. to about 250° C., the reaction temperature in said subsequent catalytic reaction step is higher than the reaction temperature in said first catalytic reaction step, said intermediate mixture into methylene-bridged polyphenyl polyamines in presence of a subsequent solid catalyst being chosen from the group consisting of zeolites, delaminated zeolites and ordered mesoporous materials, thereby providing said methylene-bridged polyphenyl polyamines.

    摘要翻译： 根据本发明的由苯胺和甲醛提供亚甲基桥接的聚苯胺的方法包括以下步骤：a）使苯胺和甲醛缩合，提供缩合物，苯胺与甲醛的摩尔比选择在2至3.5的范围内; b）在第一催化反应步骤中，在约30℃至约100℃范围内的反应温度下使所述缩合物在固体催化剂上选自粘土，硅酸盐，二氧化硅 - 氧化铝和离子交换树脂，由此提供中间体混合物，所述中间体混合物包含氨基苄基胺; c）在随后的催化反应步骤中，在约70℃至约250℃的温度范围内转化，所述后续催化反应步骤中的反应温度高于所述第一催化反应中的反应温度 在随后的固体催化剂存在下将所述中间体混合物形成亚甲基桥连的聚苯胺，所述固体催化剂选自沸石，分层沸石和有序介孔材料，从而提供所述亚甲基桥连的聚苯基多胺。