摘要:
Their is disclosed a process for producing a monoalkenyl aromatic hydrocarbon compound (e.g. 5-(o-tolyl)-2-pentene) which comprises the steps of alkenylating a side chain of an aromatic hydrocarbon compound having at lease one hydrogen atom bonded to .alpha.-position of the side chain (e.g. alkylbenzene) by the use of a conjugated diene having 4 to 5 carbon atoms (e.g. 1-3 butadiene) in the presence an alkali metal-based catalyst supported on a carrier; removing at least part of the catalyst from the resultant reaction product by separating the same; inactivating and optionally removing the catalyst contained in the reaction product; and thereafter distilling the reaction produce in liquid form to separate and recover the objective monoalkenyl aromatic hydrocarbon compound. By virtue of using the above specific method, the process can prevent the change in quality and properly of the objective product even during atmospheric distillation, produce the objective product with high purity in high recovery race and operate a distillation column during a long stable period of time.
摘要:
A process for producing a high-purity naphthalenedicarboxylic acid having an improved hue or an excellent hue from a crude naphthalenedicarboxylic acid obtained by the oxidation of dialkyl naphthalene, industrially advantageously at high yields, which comprises dissolving a crude naphthalenedicarboxylic acid obtained by the oxidation of dialkyl naphthalene in an aqueous solution containing an aliphatic amine, an alicyclic amine or acetonitrile, removing heavy metal components contained as impurities until the content of the heavy metal components based on the crude naphthalenedicarboxylic acid is 100 ppm or less, and heating the aqueous solution containing a naphthalenedicarboxylic acid amine salt to distill off the amine.
摘要:
A process for the production of a pyridinecarboxylic acid by the air-oxidation of an alkylpyridine in a liquid phase, in which the conversion of the alkylpyridine is high, the yield of the pyridinecarboxylic acid is therefore high, the content of impurities in the product is decreased, and unreacted raw material and an oxidation intermediate can be recycled without the adverse effect of accumulation of the catalyst and bromine component, the process comprising oxidizing an alkylpyridine with an oxygen-containing gas in a solvent in the presence of a catalyst formed of a heavy metal salt and a bromine compound, the solvent being a lower aliphatic monocarboxylic acid having a water content of 2 to 15% by weight, or the process comprising the step of catalytically hydrogenating an oxidation reaction mixture or an isolated pyridinecarboxylic acid in the presence of a catalyst of a metal belonging to the group VIII of the periodic table.
摘要:
Provided is a process for producing alkylbenzoyl chloride which comprises reacting alkylbenzaldehyde with chlorine at a temperature of -10.degree. to 80.degree. C. under a pressure of 5 kg/cm.sup.2 or below in a liquid phase, whereby alkylbenzoyl chloride can be produced in a high yield and at a low price.
摘要翻译:本发明提供烷基苯甲酰氯的制造方法,其特征在于,在液相中,在压力为5kg / cm 2以下的压力下,在-10℃〜80℃的温度下使烷基苯甲醛与氯反应,由此能够高效地生成烷基苯甲酰氯 收益率低廉。
摘要:
A shock absorber includes: at least one cylinder apparatus including a cylinder sealingly containing operating fluid, a piston slidably fittedly inserted in the cylinder to divide an interior of the cylinder into two chambers, and a piston rod coupled to the piston and extending to an outside of the cylinder; and at least one damping force generation mechanism connected to the cylinder apparatus, and capable of generating a damping force to be applied to a flow of the operating fluid caused by a movement of the piston and adjusting the damping force from the outside. The damping force generation mechanism includes a damping valve for generating the damping force, a pilot chamber for applying a pilot pressure by the operating fluid to the damping valve, and a pump for at least supplying or discharging the operating fluid to or from the pilot chamber.
摘要:
An aspect of the present invention relates to a magnetic recording medium comprising on one surface of a nonmagnetic support a nonmagnetic layer containing a nonmagnetic powder and a binder and a magnetic layer containing a ferromagnetic powder and a binder in this order, as well as comprising a backcoat layer on the other surface of the nonmagnetic support. The nonmagnetic layer is a radiation-cured layer formed by curing with radiation a given radiation-curable composition, and the backcoat layer comprises filler particles with an average primary particle diameter, D50, ranging from 0.05 to 1.0 μm, the filler particles being selected from the group consisting of organic polymer particles and inorganic colloidal particles.
摘要:
A capacitor is connected between direct current voltage terminals, and inductance means is connected between one end of the capacitor and one of load terminals. In a case in which the direct current voltage exceeds a set value, voltage at both ends of the capacitor is shared by the first and second switching elements that are not electrically conductive; in a case in which the direct current voltage is below the set value, the first and second switching elements are electrically conductive on a periodic basis or as needed to output reversed-polarity voltage between load terminals; and in a case in which the first and second switching elements are turned off, voltage at both ends of the capacitor restricts voltage applied to both ends of the first and second switching elements, during a period in which the first and second feedback rectifier elements are electrically conductive.
摘要:
Disclosed is a technique for providing a transmission data processing method and the like capable of estimating a communicable band in a heterogeneous multi-radio network at a higher speed and minimizing the deterioration of the video quality even if an unavoidable fluctuation occurs in a band available for transmission. According to the technique, there is provided a transmission data processing method at a stage prior to data transmission by a transmission device 100 for providing the data transmission to a reception device 200 as a communication partner, including: a priority giving step of giving priority to each data of multiple pieces of data, to be transmitted to the reception device, based on a predetermined criterion; a feedback receiving step of receiving, from the reception device, feedback information on data transmitted from the transmission device to the reception device; and a distribution step of distributing, based on the priority and the feedback information received, the multiple pieces of data into a first interface and a second interface used for communication with the reception device.
摘要:
Regarding contents of C, Si, Mn and Cr, a value of parameter P represented by the following (equation 1) is 1000 or more. A metallic structure contains wire-drawn pearlite in an area ratio of 98% or more, a diameter is 0.05 mm to 0.18 mm, a tensile strength is 4000 MPa or more, and a twist number in a twist test in which a grip-to-grip distance is 100 mm, and a tension equal to a tensile strength×a cross-sectional area of wire×0.5 is applied, is 5 or more. P=1098×[C]+98×[Si]−20×[Mn]+167×[Cr] (equation 1) (in the (equation 1), [C], [Si], [Mn] and [Cr] indicate contents (mass %) of C, Si, Mn and Cr, respectively.)
摘要:
Certain embodiments provide an ADC includes a comparator, a binary counter and a control circuit. The comparator compares a first analog signal voltage with a first reference voltage, and compares a second analog signal voltage with a second reference voltage. The binary counter counts up the clock signal for a first period until the first reference voltage becomes equal to the first analog signal after the comparator starts to compare the first reference voltage with the first analog signal voltage, and inverts a logic level of the count output having a plurality of bits after the first period elapses. The binary counter counts up the clock signal for a second period until the second reference voltage becomes equal to a second analog signal after the comparator starts to compare the second reference voltage with the second analog signal voltage.