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公开(公告)号：US07959828B2
公开(公告)日：2011-06-14
申请号：US12714709
申请日：2010-03-01
CPC分类号： C08J9/146 , B01F17/0085 , C03C23/0075 , C07C21/18 , C08G18/4208 , C08G18/4883 , C08G2101/0025 , C08J9/0019 , C08J9/144 , C08J2205/05 , C08J2205/052 , C08J2325/06 , C08J2375/06 , C08J2375/08 , C10M105/52 , C10M107/38 , C10M147/04 , C10M169/04 , C10M169/041 , C10M177/00 , C10M2211/022 , C10M2211/06 , C10M2213/04 , C10M2213/06 , C10N2230/06 , C10N2230/22 , C10N2240/20 , C10N2240/204 , C10N2250/121 , C10N2270/00 , C11D3/245 , C11D3/43 , C11D7/5018 , C11D11/0023 , C11D11/0029 , C11D11/0035 , C11D11/0047 , C23G5/02803 , C23G5/02825 , G11B5/71 , G11B5/725 , G11B5/8408 , G11B23/505
摘要： This invention relates to cleaning compositions comprising unsaturated fluorinated hydrocarbons. The invention further relates to use of said cleaning compositions in methods to clean, degrease, deflux, dewater, and deposit fluorolubricant. The invention further relates to novel unsaturated fluorinated hydrocarbons and their use as cleaning compositions and in the methods listed above.
摘要翻译： 本发明涉及包含不饱和氟化烃的清洁组合物。 本发明还涉及所述清洁组合物在清洗，脱脂，除油，脱水和沉积氟橄榄油的方法中的用途。 本发明还涉及新型不饱和氟化烃及其作为清洁组合物和上述方法的用途。
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2.发明授权公开(公告)号：US09174896B2
公开(公告)日：2015-11-03
申请号：US13988111
申请日：2011-11-07
CPC分类号： C07C17/25 , C07C17/206 , C07C21/18
摘要： A vapor phase process is disclosed for making internal fluorobutenes. The process involves contacting a halobutane starting material selected from the group consisting of CF2HCHClCH2CCl2H, CF2HCHClCH2CCl3, CF3CHClCH2CCl2H, CF3CHClCH2CCl3, CF3CHClCHClCCl2H, CF3CHClCHClCCl3, CF3CCl2CH2CCl2H, CF3CCl2CH2CCl3, CF3CCl2CHClCCl2H, CF3CCl2CHClCCl3, CF3CClFCHClCCl2H, CF3CClFCHClCCl3, CF3CClFCH2CCl2H, CF3CClFCH2CCl3, CF3CClFCHFCCl2H, CF3CClFCHFCCl3, CF3CClHCHFCCl2H and CF3CClHCHFCCl3, with HF in a reaction zone in the presence of a chromium oxyfluoride catalyst to produce a product mixture comprising an internal fluorobutene. Another vapor phase process is disclosed for making internal fluoropentenes. The process involves contacting a halopentane starting material selected from the group consisting of CF2HCHXCH2CX2CX3, CF3CHXCH2CX2CX3, CF3CHXCHXCX2CX3, CF3CX2CH2CX2CX3, CF3CX2CHXCX2CX3 and CF3CHXCHFCX2CX3, with HF in a reaction zone in the presence of a chromium oxyfluoride catalyst to produce a product mixture comprising an internal fluoropentene, wherein each X is independently selected from the group consisting of F, Cl and Br, provided that not all X are fluorines.
摘要翻译： 公开了一种用于制备内部氟代异丁烯的气相方法。 该方法包括接触选自CF2HCHClCH2CCl2H，CF2HCHClCH2CCl3，CF3CHClCH2CCl2H，CF3CHClCH2CCl3，CF3CHClCHClCCl2H，CF3CHClCHClCCl3，CF3CCl2CH2CCl2H，CF3CCl2CH2CCl3，CF3CCl2CHClCCl2H，CF3CCl2CHClCCl3，CF3CClFCHClCCl2H，CF3CClFCHClCCl3，CF3CClFCH2CCl2H，CF3CClFCH2CCl3，CF3CClFCHFCCl2H，CF3CClFCHFCCl3，CF3CClHCHFCCl2H和CF3CClHCHFCCl3的组中选择的halobutane起始材料 在HF反应区中，在氟氧化铬催化剂的存在下制备包含内部氟代丁烯的产物混合物。 公开了制备内部氟代戊烯的另一种气相方法。 该方法包括在氟氧化铬催化剂存在下，在反应区中将选自CF2HCHXCH2CX2CX3，CF3CHXCH2CX2CX3，CF3CHXCHXCX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CHXCX2CX3与CF3CHXCHFCX2CX3的卤代戊烷起始材料与HF接触，制备包含内部氟代戊烯的产物混合物， 其中每个X独立地选自F，Cl和Br，条件是不是全部X是氟。
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公开(公告)号：US09139498B2
公开(公告)日：2015-09-22
申请号：US13988121
申请日：2011-11-07
IPC分类号： C07C17/278 , C07C19/10 , C07C17/383
CPC分类号： C07C17/278 , C07C17/383 , C07C19/10
摘要： A process is disclosed for producing addition compound CF3CCl2CH2CClXR, wherein X═H, F, Cl or Br, and R═H or a perhalogenated alkyl group, provided that X and R are not both H. The process involves a liquid phase reaction of 1,1,1-trichlorotrifluoroethane with CH2═CXR in the presence of an addition catalyst.
摘要翻译： 公开了制备加成化合物CF 3 CCl 2 CH 2 ClClR的方法，其中X = H，F，Cl或Br，以及R = H或全卤代烷基，条件是X和R不同时为H.该方法涉及液相反应1 ，在加成催化剂存在下，使用CH 2 = C X R的1,1-三氯三氟乙烷。
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公开(公告)号：USRE45076E1
公开(公告)日：2014-08-12
申请号：US13606233
申请日：2012-09-07
CPC分类号： B01J23/72 , B01J21/18 , B01J23/58 , B01J23/628 , B01J23/755 , B01J23/78 , B01J23/868 , B01J27/12 , B01J35/023 , C07C17/23 , C07C21/18
摘要： Disclosed herein is a process for the preparation of fluorine-containing olefins comprising contacting a chlorofluoroalkene with hydrogen in the presence of a catalyst at a temperature sufficient to cause replacement of the chlorine substituents with hydrogen. Also disclosed is a catalyst composition for the hydrodechlorination of chlorofluoroalkenes comprising copper metal deposited on a support.
摘要翻译： 本文公开了一种制备含氟烯烃的方法，其包括在足以使氢取代氯取代基的温度下在催化剂存在下使氯氟烯与氢接触。 还公开了用于加氢脱氯包含沉积在载体上的铜金属的氯氟代烯烃的催化剂组合物。
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5.发明申请公开(公告)号：US20140114096A1
公开(公告)日：2014-04-24
申请号：US13988111
申请日：2011-11-07
IPC分类号： C07C17/25
CPC分类号： C07C17/25 , C07C17/206 , C07C21/18
摘要： A vapor phase process is disclosed for making internal fluorobutenes. The process involves contacting a halobutane starting material selected from the group consisting of CF2HCHClCH2CCl2H, CF2HCHClCH2CCl3, CF3CHClCH2CCl2H, CF3CHClCH2CCl3, CF3CHClCHClCCl2H, CF3CHClCHClCCl3, CF3CCl2CH2CCl2H, CF3CCl2CH2CCl3, CF3CCl2CHClCCl2H, CF3CCl2CHClCCl3, CF3CClFCHClCCl2H, CF3CClFCHClCCl3, CF3CClFCH2CCl2H, CF3CClFCH2CCl3, CF3CClFCHFCCl2H, CF3CClFCHFCCl3, CF3CClHCHFCCl2H and CF3CClHCHFCCl3, with HF in a reaction zone in the presence of a chromium oxyfluoride catalyst to produce a product mixture comprising an internal fluorobutene. Another vapor phase process is disclosed for making internal fluoropentenes. The process involves contacting a halopentane starting material selected from the group consisting of CF2HCHXCH2CX2CX3, CF3CHXCH2CX2CX3, CF3CHXCHXCX2CX3, CF3CX2CH2CX2CX3, CF3CX2CHXCX2CX3 and CF3CHXCHFCX2CX3, with HF in a reaction zone in the presence of a chromium oxyfluoride catalyst to produce a product mixture comprising an internal fluoropentene, wherein each X is independently selected from the group consisting of F, Cl and Br, provided that not all X are fluorines.
摘要翻译： 公开了一种用于制备内部氟代异丁烯的气相方法。 该方法包括接触选自CF2HCHClCH2CCl2H，CF2HCHClCH2CCl3，CF3CHClCH2CCl2H，CF3CHClCH2CCl3，CF3CHClCHClCCl2H，CF3CHClCHClCCl3，CF3CCl2CH2CCl2H，CF3CCl2CH2CCl3，CF3CCl2CHClCCl2H，CF3CCl2CHClCCl3，CF3CClFCHClCCl2H，CF3CClFCHClCCl3，CF3CClFCH2CCl2H，CF3CClFCH2CCl3，CF3CClFCHFCCl2H，CF3CClFCHFCCl3，CF3CClHCHFCCl2H和CF3CClHCHFCCl3的组中选择的halobutane起始材料 在HF反应区中，在氟氧化铬催化剂的存在下制备包含内部氟代丁烯的产物混合物。 公开了制备内部氟代戊烯的另一种气相方法。 该方法包括在氟氧化铬催化剂存在下，在反应区中将选自CF2HCHXCH2CX2CX3，CF3CHXCH2CX2CX3，CF3CHXCHXCX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CH2CX2CX3，CF3CX2CHXCX2CX3与CF3CHXCHFCX2CX3的卤代戊烷起始材料与HF接触，制备包含内部氟代戊烯的产物混合物， 其中每个X独立地选自F，Cl和Br，条件是不是全部X是氟。
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