利索-全球专利检索

  1. 登录
  2. 注册

搜索结果

152 条记录 (耗时 0.021 秒)

    Manufacturing method of hexafluorophosphate
    1.
    发明授权
    Manufacturing method of hexafluorophosphate 有权
    六氟磷酸盐的制造方法

    公开(公告)号：US08383075B2

    公开(公告)日：2013-02-26

    申请号：US12525900

    申请日：2008-02-05

    申请人： Masahide Waki ,  Kazuhiro Miyamoto ,  Kenji Aoki

    发明人： Masahide Waki ,  Kazuhiro Miyamoto ,  Kenji Aoki

    IPC分类号： C01B25/10 ,  H01M6/04 ,  B01J27/24 ,  B01J27/00

    CPC分类号： C01D15/005 ,  C01B25/455 ,  C01D13/00

    摘要： In the manufacturing method of hexafluorophosphate (MPF6: M=Li, Na, K, Rb, Cs, NH4, and Ag) of the present invention, at least a HxPOyFz aqueous solution, a hydrofluoric acid aqueous solution, and MF.r (HF) are used as raw materials (wherein, r≧0, 0≦x≦3, 0≦y≦4, and 0≦z≦6). According to the above description, a manufacturing method of hexafluorophosphate can be provided which is capable of manufacturing hexafluorophosphate (GPF6: G=Li, Na, K, Rb, Cs, NH4, and Ag) at a low cost in which the raw materials can be easily obtained, the control of the reaction is possible, and the workability is excellent.

    摘要翻译： 在本发明的六氟磷酸盐（MPF6：M = Li，Na，K，Rb，Cs，NH4和Ag）的制造方法中，至少含有H x PO y F z水溶液，氢氟酸水溶液和MF.r（HF ）作为原料（其中，r≥0,0，nlE; x＆nlE; 3,0＆nlE; y＆nlE; 4和0＆amp; nlE; z＆nlE; 6）。 根据上述说明，可以以低成本制造能够制造六氟磷酸盐（GPF6：G = Li，Na，K，Rb，Cs，NH4和Ag）的六氟磷酸盐的制造方法，其中原料可以 可以容易地获得，反应的控制是可能的，并且可加工性是优异的。

    METHOD OF MANUFACTURING PHOSPHOROUS PENTAFLUORIDE AND HEXAFLUOROPHOSPHATE
    2.
    发明申请
    METHOD OF MANUFACTURING PHOSPHOROUS PENTAFLUORIDE AND HEXAFLUOROPHOSPHATE 审中-公开
    磷酸二氢钠和十六烷基磷酸盐的制备方法

    公开(公告)号：US20100322838A1

    公开(公告)日：2010-12-23

    申请号：US12525907

    申请日：2008-02-05

    申请人： Masahide Waki ,  Kazuhiro Miyamoto ,  Kenji Aoki

    发明人： Masahide Waki ,  Kazuhiro Miyamoto ,  Kenji Aoki

    IPC分类号： C01B25/10

    CPC分类号： C01B25/10 ,  C01B25/455 ,  C01D15/005

    摘要： A process for phosphorus pentafluoride production by which high-purity phosphorus pentafluoride can be produced by a simple and economical procedure without the need of a large-scale purification apparatus or high-pressure apparatus and without generating a large amount of a by-product gas requiring a special discharge-gas treatment. The process for phosphorus pentafluoride production is characterized by introducing hydrogen fluoride and a hexafluorophosphate (MPF6) into a vessel and reacting them according to the reaction shown by the scheme (1) to yield phosphorus pentafluoride. MPF6+uHF→PF5+MF r(HF) (Scheme 1) In the scheme, M is at least any one of Li, Na, K, Rb, Cs, NH4, and Ag; 0≦r≦u; and the HF is used in an amount not smaller than the stoichiometric amount.

    摘要翻译： 一种五氟化磷生产方法，其中可以通过简单和经济的方法制备高纯度五氟化磷，而不需要大规模的净化装置或高压装置，并且不产生大量的副产物气体需要 特殊放电气体处理。 五氟化磷生产方法的特征在于将氟化氢和六氟磷酸盐（MPF6）引入容器中，并根据方案（1）所示的反应进行反应，得到五氟化磷。 MPF6 + uHF→PF5 + MFr（HF）（方案1）在该方案中，M是Li，Na，K，Rb，Cs，NH 4和Ag中的至少任一种; 0＆nlE; r＆nlE; u; HF的使用量不小于化学计量量。

    MANUFACTURING METHOD OF HEXAFLUOROPHOSPHATE
    3.
    发明申请
    MANUFACTURING METHOD OF HEXAFLUOROPHOSPHATE 有权
    十六烷基磷酸盐的制备方法

    公开(公告)号：US20100317511A1

    公开(公告)日：2010-12-16

    申请号：US12525900

    申请日：2008-02-05

    申请人： Masahide Waki ,  Kazuhiro Miyamoto ,  Kenji Aoki

    发明人： Masahide Waki ,  Kazuhiro Miyamoto ,  Kenji Aoki

    IPC分类号： B01J27/14 ,  H01M6/04 ,  B01J27/24

    CPC分类号： C01D15/005 ,  C01B25/455 ,  C01D13/00

    摘要： In the manufacturing method of hexafluorophosphate (MPF6: M=Li, Na, K, Rb, Cs, NH4, and Ag) of the present invention, at least a HxPOyFz aqueous solution, a hydrofluoric acid aqueous solution, and MF.r (HF) are used as raw materials (wherein, r≧0, 0≦x≦3, 0≦y≦4, and 0≦z≦6). According to the above description, a manufacturing method of hexafluorophosphate can be provided which is capable of manufacturing hexafluorophosphate (GPF6: G=Li, Na, K, Rb, Cs, NH4, and Ag) at a low cost in which the raw materials can be easily obtained, the control of the reaction is possible, and the workability is excellent.

    摘要翻译： 在本发明的六氟磷酸盐（MPF6：M = Li，Na，K，Rb，Cs，NH4和Ag）的制造方法中，至少含有H x PO y F z水溶液，氢氟酸水溶液和MF.r（HF ）作为原料（其中，r≥0,0，nlE; x＆nlE; 3,0＆nlE; y＆nlE; 4和0＆amp; nlE; z＆nlE; 6）。 根据上述说明，可以以低成本制造能够制造六氟磷酸盐（GPF6：G = Li，Na，K，Rb，Cs，NH4和Ag）的六氟磷酸盐的制造方法，其中原料可以 可以容易地获得，反应的控制是可能的，并且可加工性是优异的。

    Tantalum oxide and/or niobium oxide and method for preparation thereof
    5.
    发明申请
    Tantalum oxide and/or niobium oxide and method for preparation thereof 审中-公开
    氧化钽和/或氧化铌及其制备方法

    公开(公告)号：US20070178040A1

    公开(公告)日：2007-08-02

    申请号：US10592360

    申请日：2005-03-11

    申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Kenji Aoki

    发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Kenji Aoki

    IPC分类号： C01G31/02

    CPC分类号： C01G33/00 ,  C01G35/00 ,  C01P2004/03 ,  C01P2004/10

    摘要： A method for preparing tantalum oxide and/or niobium oxide, characterized in that it comprises adding a basic aqueous solution to an aqueous solution of tantalum fluoride salt and/or niobium fluoride salt, to form tantalum hydroxide and/or niobium hydroxide, and then firing said tantalum hydroxide and/or niobium hydroxide. The above method allows the preparation of the tantalum oxide and/or niobium oxide in the state of a needle crystal or columnar crystal, not of a spherical crystal or an assemblage form.

    摘要翻译： 一种氧化钽和/或氧化铌的制备方法，其特征在于，包括向氟化钽盐和/或氟化铌盐水溶液中添加碱性水溶液，形成氢氧化钽和/或氢氧化铌，然后进行烧成 所述氢氧化钽和/或氢氧化铌。 上述方法允许以针状晶体或柱状晶体的状态制备氧化钽和/或氧化铌，而不是球形晶体或组合形式。

    Method for producing tantalum oxide and/or niobium oxide in form of hollow particle
    9.
    发明申请
    Method for producing tantalum oxide and/or niobium oxide in form of hollow particle 审中-公开
    用于制造中空颗粒形式的氧化钽和/或氧化铌的方法

    公开(公告)号：US20070189957A1

    公开(公告)日：2007-08-16

    申请号：US10592372

    申请日：2005-03-11

    申请人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Kenji Aoki

    发明人： Hirohisa Kikuyama ,  Masahide Waki ,  Shinji Hashiguchi ,  Kenji Aoki

    IPC分类号： C01G31/02 ,  C01G33/00

    CPC分类号： C01G33/00 ,  C01G35/00

    摘要： The object of the invention is to provide tantalum oxide and/or niobium oxide in the form of hollow particles. Disclosed is a method comprising adding hydrazine or an aqueous solution of hydrazine to (1) an aqueous solution of a tantalum compound and/or a niobium compound, to (2) an aqueous solution of fluorotantalic acid and/or fluoroniobic acid, or to (3) a solution obtained by dissolving crystallized fluorotantalic acid and/or crystallized fluoroniobic acid in water, to produce tantalum hydroxide and/or niobium hydroxide, and firing the tantalum hydroxide and/or niobium hydroxide.

    摘要翻译： 本发明的目的是提供中空颗粒形式的氧化钽和/或氧化铌。 公开了一种方法，其包括向（1）钽化合物和/或铌化合物的水溶液中加入肼或肼的水溶液，加入（2）氟代花青酸和/或氟铌酸的水溶液或（ 3）通过将结晶的氟代花青酸和/或结晶的氟铌酸溶解在水中而制得的氢氧化钽和/或氢氧化铌获得的溶液，以及氢氧化钽和/或氢氧化铌的烧制。