公开(公告)号：US09176406B2

公开(公告)日：2015-11-03

申请号：US13958745

申请日：2013-08-05

申请人： Satoyuki Sekiguchi ,  Hiroshi Yamashita ,  Minoru Masuda ,  Susumu Chiba ,  Tatsuya Morita ,  Atsushi Yamamoto ,  Shinya Nakayama ,  Masahide Yamada ,  Kohsuke Nagata ,  Keiji Makabe ,  Toyoshi Sawada

发明人： Satoyuki Sekiguchi ,  Hiroshi Yamashita ,  Minoru Masuda ,  Susumu Chiba ,  Tatsuya Morita ,  Atsushi Yamamoto ,  Shinya Nakayama ,  Masahide Yamada ,  Kohsuke Nagata ,  Keiji Makabe ,  Toyoshi Sawada

IPC分类号： G03G9/00 ,  G03G9/087 ,  G03G9/13 ,  G03G9/08

CPC分类号： G03G9/08764 ,  G03G9/0804 ,  G03G9/08755 ,  G03G9/08795 ,  G03G9/08797

摘要： Toner contains a binder resin containing a crystalline resin having a urethane and/or urea bonding; and a colorant, wherein in a diffraction spectrum of the toner as measured by an X-ray diffraction instrument, a ratio {C/(C+A)} of an integral intensity C of the spectrum derived from the crystalline structure to an integral intensity A of the spectrum derived from the non-crystalline structure is 0.12 or greater, wherein the toner satisfies the following relation 1: T1−T2≦30° C. (Relation 1), where T1 represents the maximum endothermic peak in the first temperature rising from 0° C. to 100° C. at the temperature rising rate of 10° C./min and T2 represents the maximum exothermic peak in the first temperature falling from 100° C. to 0° C. at the temperature falling rate of 10° C./min as T1 and T2 are measured by diffraction scanning calorimetry (DSC).

摘要翻译： 调色剂含有含有具有氨基甲酸酯和/或脲键合的结晶性树脂的粘合剂树脂; 和着色剂，其中在通过X射线衍射仪测量的调色剂的衍射光谱中，从晶体结构衍生的光谱的积分强度C与积分强度之比{C /（C + A）} 衍生自非晶体结构的光谱的A为0.12或更大，其中调色剂满足以下关系1：T1-T2＆nlE; 30℃（关系1），其中T1表示第一升温中的最大吸热峰 0℃至100℃，升温速率为10℃/分钟，T2表示在100℃至0℃的第一温度下的最大放热峰，温度下降速率为 10℃/ min，通过衍射扫描量热法（DSC）测量T1和T2。

公开(公告)号：US20140272698A1

公开(公告)日：2014-09-18

申请号：US14210993

申请日：2014-03-14

申请人： Masahide YAMADA ,  Atsushi Yamamoto ,  Satoyuki Sekiguchi ,  Keiji Makabe ,  Kohsuke Nagata ,  Toyoshi Sawada

发明人： Masahide YAMADA ,  Atsushi Yamamoto ,  Satoyuki Sekiguchi ,  Keiji Makabe ,  Kohsuke Nagata ,  Toyoshi Sawada

IPC分类号： G03G9/087

CPC分类号： G03G9/08753 ,  G03G9/0821 ,  G03G9/08702 ,  G03G9/08755 ,  G03G9/08764 ,  G03G9/08788 ,  G03G9/08797

摘要： Toner contains a binder resin containing two or more kinds of crystalline resins; and a coloring agent, wherein the two or more kinds of crystalline resins have at least two endothermic peak temperatures in a set of endothermic peak temperatures of the two or more kinds of crystalline resins as measured by differential scanning calorimetry (DSC).

摘要翻译： 调色剂含有含有两种或更多种结晶树脂的粘合剂树脂; 和着色剂，其中两种或更多种结晶树脂在通过差示扫描量热法（DSC）测量的两种或更多种结晶树脂的吸热峰温度的集合中具有至少两个吸热峰温度。

公开(公告)号：US20140051019A1

公开(公告)日：2014-02-20

申请号：US13958745

申请日：2013-08-05

申请人： Satoyuki Sekiguchi ,  Hiroshi Yamashita ,  Minoru Masuda ,  Susumu Chiba ,  Tatsuya Morita ,  Atsushi Yamamoto ,  Shinya Nakayama ,  Masahide Yamada ,  Kohsuke Nagata ,  Keiji Makabe ,  Toyoshi Sawada

发明人： Satoyuki Sekiguchi ,  Hiroshi Yamashita ,  Minoru Masuda ,  Susumu Chiba ,  Tatsuya Morita ,  Atsushi Yamamoto ,  Shinya Nakayama ,  Masahide Yamada ,  Kohsuke Nagata ,  Keiji Makabe ,  Toyoshi Sawada

IPC分类号： G03G9/00 ,  G03G15/08

CPC分类号： G03G9/08764 ,  G03G9/0804 ,  G03G9/08755 ,  G03G9/08795 ,  G03G9/08797

摘要： Toner contains a binder resin containing a crystalline resin having a urethane and/or urea bonding; and a colorant, wherein in a diffraction spectrum of the toner as measured by an X-ray diffraction instrument, a ratio {C/(C+A)} of an integral intensity C of the spectrum derived from the crystalline structure to an integral intensity A of the spectrum derived from the non-crystalline structure is 0.12 or greater, wherein the toner satisfies the following relation 1: T1−T2≦30° C. (Relation 1), where T1 represents the maximum endothermic peak in the first temperature rising from 0° C. to 100° C. at the temperature rising rate of 10° C./min and T2 represents the maximum exothermic peak in the first temperature falling from 100° C. to 0° C. at the temperature falling rate of 10° C./min as T1 and T2 are measured by diffraction scanning calorimetry (DSC).

摘要翻译： 调色剂含有含有具有氨基甲酸酯和/或脲键合的结晶性树脂的粘合剂树脂; 和着色剂，其中在通过X射线衍射仪测量的调色剂的衍射光谱中，从晶体结构衍生的光谱的积分强度C与积分强度之比{C /（C + A）} 衍生自非晶体结构的光谱的A为0.12或更大，其中调色剂满足以下关系1：T1-T2 @ 30℃（关系1），其中T1表示第一升温中的最大吸热峰 0℃至100℃，升温速率为10℃/分钟，T2表示在100℃至0℃的第一温度下的最大放热峰，温度下降速率为 10℃/ min，通过衍射扫描量热法（DSC）测量T1和T2。

公开(公告)号：US09851649B2

公开(公告)日：2017-12-26

申请号：US14891032

申请日：2013-11-27

申请人： Keiji Makabe ,  Tsuyoshi Sugimoto ,  Akinori Saito ,  Suzuka Amemori ,  Toyoshi Sawada ,  Hiroshi Yamashita ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Daisuke Asahina ,  Satoyuki Sekiguchi

发明人： Keiji Makabe ,  Tsuyoshi Sugimoto ,  Akinori Saito ,  Suzuka Amemori ,  Toyoshi Sawada ,  Hiroshi Yamashita ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Daisuke Asahina ,  Satoyuki Sekiguchi

IPC分类号： G03G9/00 ,  G03G9/087 ,  G03G15/01

CPC分类号： G03G9/08788 ,  G03G9/08755 ,  G03G9/08791 ,  G03G9/08793 ,  G03G9/08795 ,  G03G9/08797 ,  G03G15/0126

摘要： A toner includes a binder resin including a copolymer resin containing structural units derived from crystalline and non-crystalline resins, respectively. Spin-spin relaxation time (t50) of the toner at 50° C. measured by pulse NMR is ≦0.05 msec., spin-spin relaxation time (t130) at 130° C. when warmed from 50° C. to 130° C. is >15 msec., and spin-spin relaxation time (t′70) at 70° C. when cooled from 130° C. to 70° C. is ≦1.00 msec. A binarized image obtained by binarizing a phase image of the toner observed by a tapping mode AFM based on intermediate value between maximum and minimum phase difference values in the phase image includes first phase difference images constituted by large phase-difference portions and a second phase difference image constituted by a small phase-difference portion. The first phase difference images are dispersed in the second phase difference image. The dispersion diameter of the first phase difference images is 150 nm or less.

公开(公告)号：US08859179B2

公开(公告)日：2014-10-14

申请号：US13679057

申请日：2012-11-16

申请人： Hideyuki Santo ,  Masahide Yamada ,  Kazumi Suzuki ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Tatsuya Morita ,  Shingo Sakashita ,  Yukiko Nakajima ,  Keiji Makabe ,  Daiki Yamashita

发明人： Hideyuki Santo ,  Masahide Yamada ,  Kazumi Suzuki ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Tatsuya Morita ,  Shingo Sakashita ,  Yukiko Nakajima ,  Keiji Makabe ,  Daiki Yamashita

IPC分类号： G03G9/107 ,  G03G9/113 ,  G03G9/087 ,  G03G9/083

CPC分类号： G03G9/0832 ,  G03G9/08797 ,  G03G9/107 ,  G03G9/1131

摘要： A developer, including a toner including a binder resin comprising a crystalline resin; and a colorant, and a resin carrier comprising a resin; a magnetic particulate material having a magnetic anisotropy, dispersed in the resin, and having a saturated magnetization of from 16 to 30 emu/g, a coercive force of from 15 to 40 kA/m and an average particle diameter not less than 15 μm and less than 100 μm.

摘要翻译： 一种显影剂，包括包含结晶树脂的粘合剂树脂的调色剂; 和着色剂，以及包含树脂的树脂载体; 具有磁各向异性的磁性颗粒材料，分散在树脂中，并且具有16至30emu / g的饱和磁化强度，15至40kA / m的矫顽力和不小于15μm的平均粒径， 小于100μm。

公开(公告)号：US20130236826A1

公开(公告)日：2013-09-12

申请号：US13709185

申请日：2012-12-10

申请人： Keiji MAKABE ,  Masahide Yamada ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Hideyuki Santo ,  Yukiko Nakajima ,  Daiki Yamashita ,  Kazumi Suzuki ,  Tatsuya Morita ,  Shingo Sakashita

发明人： Keiji MAKABE ,  Masahide Yamada ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Hideyuki Santo ,  Yukiko Nakajima ,  Daiki Yamashita ,  Kazumi Suzuki ,  Tatsuya Morita ,  Shingo Sakashita

IPC分类号： G03G9/087

CPC分类号： G03G9/08728 ,  G03G9/0804 ,  G03G9/0827 ,  G03G9/08755 ,  G03G9/08764 ,  G03G9/08788 ,  G03G9/08797 ,  G03G9/09716

摘要： A toner for electrophotography, which is prepared by a method including dissolving or dispersing a toner composition including at least a binder resin, or binder resin and a binder resin precursor as a resin component; and a colorant in an organic solvent to form an oil phase; emulsifying or dispersing the oil phase in an aqueous medium to form an emulsion dispersion comprising emulsified particles; converging the emulsified particles to granulate mother toner particles, including controlling a temperature of the emulsion dispersion to control a circularity of the mother toner particles; and removing the organic solvent, wherein the resin component includes a crystalline resin in an amount not less than 50% by weight, and the mother toner particles have an average circularity of from 0.940 to 0.980.

摘要翻译： 一种用于电子照相的调色剂，其通过包括溶解或分散至少包含粘合剂树脂或粘合剂树脂和粘合剂树脂前体的调色剂组合物作为树脂组分的方法制备; 和有机溶剂中的着色剂以形成油相; 将油相乳化或分散在水性介质中以形成包含乳化颗粒的乳液分散体; 将乳化颗粒收敛成颗粒母体调色剂颗粒，包括控制乳液分散体的温度以控制母体调色剂颗粒的圆形度; 并除去有机溶剂，其中树脂组分包括不小于50重量％的结晶树脂，母体调色剂颗粒的平均圆形度为0.940-0.980。

公开(公告)号：US20130157183A1

公开(公告)日：2013-06-20

申请号：US13679057

申请日：2012-11-16

申请人： Hideyuki Santo ,  Masahide Yamada ,  Kazumi Suzuki ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Tatsuya Morita ,  Shingo Sakashita ,  Yukiko Nakajima ,  Keiji Makabe ,  Daiki Yamashita

发明人： Hideyuki Santo ,  Masahide Yamada ,  Kazumi Suzuki ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Tatsuya Morita ,  Shingo Sakashita ,  Yukiko Nakajima ,  Keiji Makabe ,  Daiki Yamashita

IPC分类号： G03G9/00 ,  G03G15/08

CPC分类号： G03G9/0832 ,  G03G9/08797 ,  G03G9/107 ,  G03G9/1131

摘要： A developer, including a toner including a binder resin comprising a crystalline resin; and a colorant, and a resin carrier comprising a resin; a magnetic particulate material having a magnetic anisotropy, dispersed in the resin, and having a saturated magnetization of from 16 to 30 emu/g, a coercive force of from 15 to 40 kA/m and an average particle diameter not less than 15 μm and less than 100 μm.

摘要翻译： 一种显影剂，包括包含结晶树脂的粘合剂树脂的调色剂; 和着色剂，以及包含树脂的树脂载体; 具有磁各向异性的磁性颗粒材料，分散在树脂中，饱和磁化强度为16-30emu / g，矫顽力为15至40kA / m，平均粒径不小于15μm， 少于100个妈妈。

公开(公告)号：US09127118B2

公开(公告)日：2015-09-08

申请号：US13413980

申请日：2012-03-07

申请人： Hideyuki Santo ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Yoshihiro Moriya ,  Akiyoshi Sabu ,  Daisuke Asahina ,  Yoshitaka Yamauchi ,  Taichi Nemoto ,  Yukiko Nakajima ,  Daiki Yamashita ,  Masahide Yamada ,  Keiji Makabe

发明人： Hideyuki Santo ,  Shinya Nakayama ,  Atsushi Yamamoto ,  Yoshihiro Moriya ,  Akiyoshi Sabu ,  Daisuke Asahina ,  Yoshitaka Yamauchi ,  Taichi Nemoto ,  Yukiko Nakajima ,  Daiki Yamashita ,  Masahide Yamada ,  Keiji Makabe

IPC分类号： G03G9/087 ,  C08G63/08

CPC分类号： C08G63/08 ,  G03G9/08755 ,  G03G9/08757 ,  G03G9/08764 ,  G03G9/08791 ,  G03G9/08797

摘要： A resin for toner contains a polyhydroxycarboxylic acid skeleton and a rigid skeleton.

摘要翻译： 用于调色剂的树脂含有聚羟基羧酸骨架和刚性骨架。

公开(公告)号：US20150248073A1

公开(公告)日：2015-09-03

申请号：US14433770

申请日：2013-10-11

申请人： Shinya Nakayama ,  Atsushi Yamamoto ,  Minoru Masuda ,  Susumu Chiba ,  Toyoshi Sawada ,  Hiroshi Yamashita

发明人： Shinya Nakayama ,  Atsushi Yamamoto ,  Minoru Masuda ,  Susumu Chiba ,  Toyoshi Sawada ,  Hiroshi Yamashita

IPC分类号： G03G9/00

CPC分类号： G03G9/08764 ,  G03G9/0821 ,  G03G9/08755 ,  G03G9/08788 ,  G03G9/08795 ,  G03G9/08797

摘要： Provided is a toner containing a binder resin. The binder resin contains a crystalline resin. The toner has a maximum endothermic peak temperature (P1) of from 50° C. to 80° C. and a total endothermic amount (Q) of from 35 J/g to 90 J/g at a first temperature elevation of differential scanning calorimetry. A ratio (Qp/Q) of a total endothermic amount (Qp) of the toner in a temperature range of from 20° C. to the maximum endothermic peak temperature (P1) to the total endothermic amount (Q) of the toner is from 0.65 to 0.83.

摘要翻译： 提供含有粘合剂树脂的调色剂。 粘合剂树脂含有结晶性树脂。 在差示扫描量热法的第一温度升高下，调色剂具有50℃至80℃的最大吸热峰温度（P1）和35J / g至90J / g的总吸热量（Q） 。 调色剂在20℃至最大吸热峰温度（P1）的温度范围内的总吸热量（Qp）与总吸热量（Q）之间的比例（Qp / Q）来自 0.65〜0.83。

公开(公告)号：US09366982B2

公开(公告)日：2016-06-14

申请号：US14274875

申请日：2014-05-12

申请人： Atsushi Yamamoto ,  Hiroshi Yamada ,  Takamasa Hase ,  Kohsuke Nagata

发明人： Atsushi Yamamoto ,  Hiroshi Yamada ,  Takamasa Hase ,  Kohsuke Nagata

IPC分类号： G03G9/087 ,  G03G15/08 ,  G03G9/08

CPC分类号： G03G9/08764 ,  G03G9/0819 ,  G03G9/0825 ,  G03G9/08755 ,  G03G9/08797 ,  G03G15/0865

摘要： To provide a toner for developing an electrostatic image, the toner including toner particles, wherein the toner particles contain: a non-crystalline resin A; and a crystalline resin, wherein the crystalline resin contains a crystalline resin C containing a urethane bond, or a urea bond, or both thereof, and wherein the toner particles each have a sea-island structure, where the resin C is dispersed in the non-crystalline resin on a cross-section of the toner particle.

摘要翻译： 为了提供用于显影静电图像的调色剂，调色剂包括调色剂颗粒，其中调色剂颗粒包含：非结晶树脂A; 和结晶性树脂，其中所述结晶性树脂含有含有氨基甲酸酯键或脲键的结晶性树脂C或其二者，并且其中所述调色剂颗粒各自具有海岛结构，其中树脂C分散在非 - 在调色剂颗粒的横截面上的结晶树脂。