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    Process for producing 2,4-dichloro-3-alkyl-6-nitrophenol
    1.
    发明授权
    Process for producing 2,4-dichloro-3-alkyl-6-nitrophenol 失效
    2,4-二氯-3-烷基-6-硝基苯酚的制备方法

    公开(公告)号：US5012015A

    公开(公告)日：1991-04-30

    申请号：US319718

    申请日：1989-03-07

    申请人： Masanobu Terao ,  Yuzo Maegawa ,  Yasuyoshi Ueda ,  Kiyoyasu Hashimoto ,  Takashi Omura

    发明人： Masanobu Terao ,  Yuzo Maegawa ,  Yasuyoshi Ueda ,  Kiyoyasu Hashimoto ,  Takashi Omura

    IPC分类号： C07C201/10 ,  C07C205/12 ,  C07C205/26 ,  C07C309/39

    CPC分类号： C07C201/10

    摘要： 2,4-Dichloro-3-alkyl-6-nitrophenol, which is a precursor of 2,4-dichloro-3-alkyl-6-aminophenol useful for the production of a cyan coupler to be used with a sensitive material in the field of a photography in color, is industrially advantageously produced by (a) nitration of 2,4,5-trichloro-3-alkylbenzene, followed by hydrolysis of the resulting 2,4,5-trichloro-3-alkyl-6-nitrobenzene, or (b) hydrolysis of 2,4,5-trichloro-3-alkylbenzene-6-sulfonic acid or a salt thereof, followed by nitration of the resulting 2,4-dichloro-3-alkylphenol-6-sulfonic acid or a salt thereof, the starting material usable for these processes being 4-alkylbenzenesulfonic acid or a salt thereof, which is easily available.

    摘要翻译： 2,4-二氯-3-烷基-6-硝基苯酚，它是2,4-二氯-3-烷基-6-氨基苯酚的前体，可用于生产与现场敏感材料一起使用的青色成色剂 在工业上有利地通过（a）2,4-二氯-3-烷基苯的硝化，然后水解所得的2,4,5-三氯-3-烷基-6-硝基苯， 或（b）2,4,5-三氯-3-烷基苯-6-磺酸或其盐的水解，然后硝化得到的2,4-二氯-3-烷基苯酚-6-磺酸或盐 可用于这些方法的原料是4-烷基苯磺酸或其盐，其容易获得。

    2,6-dicyano-4'-morpholinoazobenzene compounds useful for dyeing hydrophobic materials
    2.
    发明授权
    2,6-dicyano-4'-morpholinoazobenzene compounds useful for dyeing hydrophobic materials 失效
    可用于染色疏水性材料的2,6-二氰基-4'-吗啉代偶氮苯化合物

    公开(公告)号：US4923974A

    公开(公告)日：1990-05-08

    申请号：US221223

    申请日：1988-07-19

    申请人： Yasuyoshi Ueda ,  Hideo Hattori ,  Jun Yamamoto ,  Kiyoyasu Hashimoto

    发明人： Yasuyoshi Ueda ,  Hideo Hattori ,  Jun Yamamoto ,  Kiyoyasu Hashimoto

    IPC分类号： C09B29/34 ,  C09B29/08 ,  C09B29/085 ,  D06P1/18

    CPC分类号： C09B29/083

    摘要： A monoazo compound of the following formula, ##STR1## wherein X is a hydrogen or halogen atom, or a C.sub.1-4 alkyl, C.sub.1-4 alkoxy, C.sub.1-4 alkylsulfonyl, C.sub.1-4 alkylcarbonyl, C.sub.1-4 alkoxycarbonyl, nitro, cyano or trifluoromethyl group, Y is a hydrogen or chlorine atom or a methyl or acylamino group, and Z is a hydrogen or chlorine atom or a methyl, methoxy or ethoxy group, which is useful for dyeing or printing hydrophobic fibers with superior level dyeing and build-up properties to give dyed products of a brilliant color superior in fastness properties.

    摘要翻译： 下式的单偶氮化合物，其中X为氢或卤素原子，或C 1-4烷基，C 1-4烷氧基，C 1-4烷基磺酰基，C 1-4烷基羰基，C 1-4烷氧基羰基，硝基，氰基 或三氟甲基，Y是氢或氯原子或甲基或酰基氨基，Z是氢或氯原子或甲基，甲氧基或乙氧基，其可用于染色或印刷具有优异染色和构建的疏水性纤维 - 赋予染色产品的色牢度优于色牢度的特性。

    Benzodifuranone compounds useful for dyeing or printing hydrophobic fiber materials and process for their production
    3.
    发明授权
    Benzodifuranone compounds useful for dyeing or printing hydrophobic fiber materials and process for their production 失效
    用于染色或印刷疏水性纤维材料的苯并二酮化合物及其生产方法

    公开(公告)号：US5077416A

    公开(公告)日：1991-12-31

    申请号：US408064

    申请日：1989-09-15

    申请人： Yasuyoshi Ueda ,  Jun Yamamoto ,  Takashi Omura ,  Hideo Hattori ,  Shinei Ikeou ,  Yosuke Yamamoto

    发明人： Yasuyoshi Ueda ,  Jun Yamamoto ,  Takashi Omura ,  Hideo Hattori ,  Shinei Ikeou ,  Yosuke Yamamoto

    IPC分类号： C07D493/04 ,  C09B57/00

    CPC分类号： C07D493/04 ,  C09B57/00

    摘要： A heterocyclic compound of the formula, ##STR1## wherein A and B are each hydrogen, alkyl or alkoxy, Y is hydrogen, alkyl, alkoxy or --O--R.sup.2 --X--R.sup.1, or Y and B are taken together with each other to form methylenedioxy, R.sup.1 is alkyl, phenyl or alkenyl, R.sup.2 is unsubstituted or substituted alkylene, and X is --O--, --S--, --SO--, --SO.sub.2 -- or ##STR2## in which R.sup.3 is hydrogen or alkyl, with the proviso that R.sup.1 is C.sub.3 or C.sub.4 alkyl or alkenyl, or C.sub.1 -C.sub.4 alkyl when R.sup.2 is unsubstituted ethylene or propylene, respectively, X is --O-- or --S--, and Y and B don't form methylenedioxy, which is useful for dyeing or printing hydrophobic fiber materials with superior dyeability to give a dyed or printed product of a red color excellent in fastness properties, particularly those such as washing fastness.

    摘要翻译： 下式的杂环化合物，其中A和B各自为氢，烷基或烷氧基，Y为氢，烷基，烷氧基或-O-R2-X-R1，或Y和B为 一起彼此形成亚甲二氧基，R1是烷基，苯基或烯基，R2是未取代或取代的亚烷基，X是-O - ， - S - ， - SO-，-SO2-或者其中R3是氢 或烷基，条件是当R 2为未取代的乙烯或丙烯时，R 1为C 3或C 4烷基或链烯基或C 1 -C 4烷基，X为-O-或-S-，并且Y和B不形成亚甲二氧基 可用于染色或印刷具有优异染色性的疏水性纤维材料，得到耐光性优异的红色染色或印刷品，特别是耐洗牢度。

    Disperse dye composition useful for dyeing of printing hydrophobic fiber materials: mixture of pyridone mono-azo dyes and optionally a quino-phthalone
    5.
    发明授权
    Disperse dye composition useful for dyeing of printing hydrophobic fiber materials: mixture of pyridone mono-azo dyes and optionally a quino-phthalone 失效
    用于印染疏水纤维材料染色的分散染料组合物：吡啶酮单偶氮染料和任选的喹喔啉酮混合物

    公开(公告)号：US5038415A

    公开(公告)日：1991-08-13

    申请号：US462738

    申请日：1990-01-09

    申请人： Yasuyoshi Ueda ,  Junichi Sekihachi ,  Takashi Omura ,  Hideo Hattori ,  Kiyoharu Nakatsuka

    发明人： Yasuyoshi Ueda ,  Junichi Sekihachi ,  Takashi Omura ,  Hideo Hattori ,  Kiyoharu Nakatsuka

    IPC分类号： C09B29/42 ,  C09B67/22

    CPC分类号： C09B67/0051 ,  C09B29/363 ,  Y10S8/921 ,  Y10S8/922 ,  Y10S8/924

    摘要： A disperse dye composition comprising (a) a pyridone monoazo compound of the formula (I), ##STR1## wherein X.sup.1 and X.sup.2 are each hydrogen, halogen, alkyl, alkoxy or others, and R.sup.1 is alkyl, alkenyl, cycloalkyl, phenyl or anilino, and (b) a pyridone monoazo compound of the formula (II). ##STR2## wherein X.sup.3 and X.sup.4 are each hydrogen, halogen, alkyl, alkoxy or others, and R.sup.2 is alkyl, alkenyl, cycloalkyl, phenyl or anilino, optionally together with (c) a quinophthalone compound of the formula (III), ##STR3## wherein Y is hydrogen or bromine, and the ring A is unsubstituted or substituted benzene or naphthalene ring, which is useful as a yellow dye component for dyeing or printing hydrophobic fiber materials with superior dye bath stability and level dyeing property.

    摘要翻译： 一种分散染料组合物，其包含（a）式（I）的吡啶酮单偶氮化合物，其中X 1和X 2各自为氢，卤素，烷基，烷氧基等，R 1为烷基，烯基，环烷基， 苯基或苯胺基，和（b）式（II）的吡啶酮单偶氮化合物。 （II）其中X 3和X 4各自为氢，卤素，烷基，烷氧基或其它，并且R 2为烷基，烯基，环烷基，苯基或苯胺基，任选与（c）式（III）的喹酞酮化合物 ，其中Y是氢或溴，环A是未取代或取代的苯环或萘环，其可用作用于染色或印刷具有优异的染液浴稳定性和水平染色性能的疏水性纤维材料的黄色染料组分。

    Monoazo compounds and dyeing or printing methods using the same
    6.
    发明授权
    Monoazo compounds and dyeing or printing methods using the same 失效
    单偶氮化合物和染色或印刷方法使用相同

    公开(公告)号：US5770707A

    公开(公告)日：1998-06-23

    申请号：US605432

    申请日：1996-02-22

    申请人： Yoshimi Ebiike ,  Takeshi Washimi ,  Yasuyoshi Ueda ,  Takashi Omura

    发明人： Yoshimi Ebiike ,  Takeshi Washimi ,  Yasuyoshi Ueda ,  Takashi Omura

    IPC分类号： C09B62/51

    CPC分类号： C09B62/51

    摘要： A monoazo compound represented by the general formula (I): ##STR1## wherein D is an optionally substituted phenyl or an optionally substituted naphthyl; R and R.sup.1 are hydrogen or an optionally substituted lower alkyl; A is a naphthylene represented by the general formula (A1): ##STR2## m.sub.1 and m.sub.2 are 0 or 1; Y is an aliphatic connecting group Z is --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 Z.sup.1 in which Z.sup.1 is a group removable by the action of an alkali; X is an aliphatic, aromatic, alicyclic, cyclic amino group, etc; and a method for dyeing or printing fiber materials using the monoazo compound.

    摘要翻译： 由通式（I）表示的单偶氮化合物：其中D是任选取代的苯基或任选取代的萘基; R和R 1是氢或任选取代的低级烷基; A是由通式（A1）表示的亚萘基：（IMA）（A1）m1和m2是0或1; Y是脂族连接基团Z是-CH = CH 2或-CH 2 CH 2 Z 1，其中Z 1是可以通过碱的作用除去的基团; X是脂肪族，芳香族，脂环族，环状氨基等; 以及使用单偶氮化合物染色或印刷纤维材料的方法。

    Monoazo compounds and method for dyeing or printing fiber materials using the same
    8.
    发明授权
    Monoazo compounds and method for dyeing or printing fiber materials using the same 失效
    单偶氮化合物和使用其的纤维材料的染色或印花方法

    公开(公告)号：US5596083A

    公开(公告)日：1997-01-21

    申请号：US579603

    申请日：1995-12-26

    申请人： Nobutaka Kunimi ,  Yasuyoshi Ueda ,  Takashi Omura

    发明人： Nobutaka Kunimi ,  Yasuyoshi Ueda ,  Takashi Omura

    IPC分类号： C09B62/51 ,  D06P1/384

    CPC分类号： C09B62/51

    摘要： A monoazo compound suitable for dyeing or printing materials having a hydroxy group and/or amide group represented by the following general formula (I): ##STR1## wherein D represents a phenyl or naphthyl group; A represents a group represented by the following formula: ##STR2## or A represents a group represented by the following formula: ##STR3## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7, R.sub.8, R.sub.9, n and Y have the meaning given in the specification; and salts thereof.

    摘要翻译： 适用于具有下列通式（I）表示的羟基和/或酰胺基的染色或印刷材料的单偶氮化合物：其中D表示苯基或萘基; A表示由下式表示的基团：或A表示由下式表示的基团：其中R1，R2，R3，R4，R5，R6，R7，R8，R9，n和Y具有 说明书中给出的含义; 及其盐。

    Heterocyclic compounds for making red disperse dyes
    9.
    发明授权
    Heterocyclic compounds for making red disperse dyes 失效
    用于制备红色分散染料的杂环化合物

    公开(公告)号：US5424455A

    公开(公告)日：1995-06-13

    申请号：US104474

    申请日：1993-07-28

    申请人： Jun Yamamoto ,  Yasuyoshi Ueda ,  Junichi Sekihachi ,  Yosuke Yamamoto ,  Takashi Omura

    发明人： Jun Yamamoto ,  Yasuyoshi Ueda ,  Junichi Sekihachi ,  Yosuke Yamamoto ,  Takashi Omura

    IPC分类号： C07D493/04 ,  C09B57/00 ,  D06P1/16 ,  D06P3/54

    CPC分类号： C07D493/04 ,  C09B57/00 ,  Y10S8/922

    摘要： A heterocyclic compound of the formula, ##STR1## wherein A and B are each hydrogen, halogen, alkyl or alkoxy, R.sup.1 is alkylene having upto 6 carbon atoms, X is direct linkage or divalent group such as --O--, --S--and the like, T and U are each hydrogen or alkyl, l is 0 or 1 to 3, Q is 5-, 6- or 7- membered saturated or unsaturated heterocyclic residue, and Y is hydrogen, halogen, alkyl, alkoxy or ##STR2## and B are taken together with each other to form methylene-dioxy, which is useful for dyeing or printing hydrophobic fiber materials with superior dyeability to give a dyed or printed product of a red color excellent in fastness properties, particularly those such as washing fastness.

    摘要翻译： 式中的杂环化合物，其中A和B各自为氢，卤素，烷基或烷氧基，R 1为具有至多6个碳原子的亚烷基，X为直链或二价基团，例如-O - ， - S-和 T和U各自为氢或烷基，l为0或1至3，Q为5-，6-或7-元饱和或不饱和杂环残基，Y为氢，卤素，烷基，烷氧基或和B相互结合以形成亚甲基二氧基，其可用于染色或印刷具有优异染色性的疏水性纤维材料，以得到耐晒性优异的红色染色或印刷产品，特别是耐洗牢度 。

    Reduced coenzyme Q10 crystal having excellent stability
    10.
    发明授权
    Reduced coenzyme Q10 crystal having excellent stability 有权
    还原型辅酶Q10晶体具有优异的稳定性

    公开(公告)号：US09388109B2

    公开(公告)日：2016-07-12

    申请号：US14129003

    申请日：2012-06-21

    申请人： Hideo Kawachi ,  Shiro Kitamura ,  Yasuyoshi Ueda

    发明人： Hideo Kawachi ,  Shiro Kitamura ,  Yasuyoshi Ueda

    IPC分类号： A61K31/12 ,  C07C49/577 ,  A23L2/52 ,  A23K1/16 ,  A23L1/30 ,  A61K8/34 ,  A61Q19/00 ,  C07C45/81 ,  C07C41/40 ,  C07C41/46 ,  C07C43/23

    CPC分类号： C07C49/577 ,  A23K20/111 ,  A23L2/52 ,  A23L33/10 ,  A23V2002/00 ,  A61K8/347 ,  A61K9/28 ,  A61K31/122 ,  A61Q19/00 ,  C07C41/40 ,  C07C41/46 ,  C07C43/23 ,  C07C45/81

    摘要： With respect to reduced coenzyme Q10, there has been no report about the presence of crystal polymorphism, and it has been considered that a conventionally obtained crystal form is only one form. The present invention relates to a reduced coenzyme Q10 crystal having an endothermic peak indicating melting at 54±2° C. during temperature rise at a rate of 5° C./min by differential scanning calorimetry (DSC), and/or to a reduced coenzyme Q10 crystal showing characteristic peaks at diffraction angles (2θ±0.2°) of 11.5°, 18.2°, 19.3°, 22.3°, 23.0° and 33.3° by powder X-ray (Cu—Kα) diffraction. The crystal form is a novel reduced coenzyme Q10 crystal which has a higher melting point and a lower solubility in a solvent, and is more excellent in stability than the conventionally known reduced coenzyme Q10 crystal.

    摘要翻译： 关于还原型辅酶Q10，没有关于晶体多晶型的存在的报道，已经认为常规获得的晶体形式仅是一种形式。 本发明涉及在通过差示扫描量热法（DSC）以5℃/ min的速率升温的温度升高期间具有指示在54±2℃熔化的吸热峰的还原型辅酶Q10晶体和/或还原型辅酶Q10晶体 通过粉末X射线（Cu-Kα）衍射，辅助Q10晶体在衍射角（2θ;±0.2°）为11.5°，18.2°，19.3°，22.3°，23.0°和33.3°处显示出特征峰。 晶体形式是在溶剂中具有较高熔点和较低溶解度的新型还原型辅酶Q10晶体，其稳定性优于常规已知的还原型辅酶Q10晶体。