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1.发明申请Multilayer heat-shrinkable film of high transparency, low haze, and high semi-crystalline polyamide content 审中-公开多层热收缩膜，透明度高，雾度低，半结晶聚酰胺含量高公开(公告)号：US20080182052A1
公开(公告)日：2008-07-31
申请号：US11699154
申请日：2007-01-29
申请人： Michael E. Broadus , Richard M. Dayrit , Bryan E. Freeman , Frank M. Hofmeister , Brian P. Rivers , Christopher K. Robinson , Matthew D. Dawe , Nathanael R. Miranda
发明人： Michael E. Broadus , Richard M. Dayrit , Bryan E. Freeman , Frank M. Hofmeister , Brian P. Rivers , Christopher K. Robinson , Matthew D. Dawe , Nathanael R. Miranda
CPC分类号： B32B27/32 , B32B7/02 , B32B27/34 , Y10T428/1328 , Y10T428/2495 , Y10T428/24992 , Y10T428/3175
摘要： A multilayer, heat-shrinkable film has a first layer that is an outer film layer and that serves as a heat seal layer, and a second layer comprising at least one semi-crystalline polyamide. The first layer contains at least one member selected from the group consisting of (i) polyolefin having a density of from 0.88 g/cm3 to 0.917 g/cm3, and (ii) ionomer resin. The second layer contains at least one semi-crystalline polyamide selected from the group consisting of polyamide 6, polyamide 66, polyamide 6/66, and polyamide 6/12, with the semi-crystalline polyamide making up at least 50 weight percent of the second layer. The film has a total free shrink at 185° F. of at least 35 percent. The film has a total semi-crystalline polyamide content of at least 35 volume percent. The multilayer, heat-shrinkable film exhibits a percent haze as measured using ASTM D 1003-00, and a percent transparency as measured using ASTM D 1746-97, in accordance with the following equation: % Transparency≧5.33 (% Haze)−31.5 The multilayer, heat-shrinkable film can be used to make a packaging article.
摘要翻译： 多层热收缩膜具有作为外膜层的第一层，用作热封层，以及包含至少一种半结晶聚酰胺的第二层。 第一层含有选自（i）密度为0.88g / cm 3至0.917g / cm 3的聚烯烃中的至少一种，和 （ii）离聚物树脂。 第二层包含至少一种选自聚酰胺6，聚酰胺66，聚酰胺6/66和聚酰胺6/12的半结晶聚酰胺，半结晶聚酰胺占第二层的至少50重量％ 层。 该膜在185°F下的总自由收缩率至少为35％。 该膜具有至少35体积％的总半结晶聚酰胺含量。 使用ASTM D 1003-00测量的多层热收缩膜表现出雾度百分比，并且使用ASTM D 1746-97测量的透明度百分比根据下列等式：％透明度= 5.33（％雾度） - 31.5多层热收缩膜可用于制作包装制品。
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2.发明授权公开(公告)号：US07687123B2
公开(公告)日：2010-03-30
申请号：US11801902
申请日：2007-05-11
申请人： Michael E. Broadus , Richard M. Dayrit , Brian P. Rivers , Roger D. Vrooman , Marvin R. Havens , Emmet Austin , Frank M. Hofmeister , Matthew D. Dawe , Nathanael R. Miranda , Christopher K. Robinson , Bryan E. Freeman , Josh E. Johnston
发明人： Michael E. Broadus , Richard M. Dayrit , Brian P. Rivers , Roger D. Vrooman , Marvin R. Havens , Emmet Austin , Frank M. Hofmeister , Matthew D. Dawe , Nathanael R. Miranda , Christopher K. Robinson , Bryan E. Freeman , Josh E. Johnston
CPC分类号： B32B27/34 , Y10T428/1328 , Y10T428/1379 , Y10T428/1383 , Y10T428/31725 , Y10T428/31739
摘要： A multilayer, heat-shrinkable film contains at least one semi-crystalline polyamide selected from the group consisting of polyamide 6, polyamide 66, polyamide 6/66, and polyamide 6/12. The film may have a total semi-crystalline polyamide content of at least 35 volume percent, based on total film volume, and a total free shrink at 185° F. of at least 35 percent. The film may have an FTIR Transmission Absorbance A1199/A1170 ratio of up to 1.65. The film may be a retortable film, capable of being used in a process for preparing a retorted packaged product. A process for making a heat-shrinkable annular film containing the semi-crystalline polyamide comprises extruding an annular extrudate downward from an annular die, quenching the annular extrudate by applying a quenching liquid to the annular extrudate, reheating the extrudate to an orientation temperature, and orienting the reheated annular extrudate while the reheated annular extrudate is in the solid state, the orientation being carried out with a total orientation factor of at least 2, to produce a film having a total free shrink at 185° F. of at least 10 percent.
摘要翻译： 多层热收缩膜含有至少一种选自聚酰胺6，聚酰胺66，聚酰胺6/66和聚酰胺6/12的半结晶聚酰胺。 基于总膜体积，膜可以具有至少35体积％的总半结晶聚酰胺含量，并且在185°F下的总自由收缩率至少为35％。 该片可能具有高达1.65的FTIR透射率吸收比A1199 / A1170。 该膜可以是能够用于制备蒸煮包装产品的方法中的可蒸煮膜。 制造含有半结晶聚酰胺的热收缩性环状膜的方法包括从环形模具向下挤出环形挤出物，通过向环形挤出物施加淬火液淬火环状挤出物，将挤出物再加热至取向温度，以及 在重新加热的环状挤出物处于固态的同时，对再加热的环状挤出物进行定向，所述取向以总取向因子至少为2进行，以产生在185°F下的总自由收缩率为至少10％ 。
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3.发明申请公开(公告)号：US20080182053A1
公开(公告)日：2008-07-31
申请号：US11801902
申请日：2007-05-11
申请人： Michael E. Broadus , Richard M. Dayrit , Brian P. Rivers , Roger D. Vrooman , Marvin R. Havens , Emmet Austin , Frank M. Hofmeister , Matthew D. Dawe , Nathanael R. Miranda , Christopher K. Robinson , Bryan B. Freeman , Josh E. Johnston
发明人： Michael E. Broadus , Richard M. Dayrit , Brian P. Rivers , Roger D. Vrooman , Marvin R. Havens , Emmet Austin , Frank M. Hofmeister , Matthew D. Dawe , Nathanael R. Miranda , Christopher K. Robinson , Bryan B. Freeman , Josh E. Johnston
IPC分类号： B65B53/02
CPC分类号： B32B27/34 , Y10T428/1328 , Y10T428/1379 , Y10T428/1383 , Y10T428/31725 , Y10T428/31739
摘要： A multilayer, heat-shrinkable film contains at least one semi-crystalline polyamide selected from the group consisting of polyamide 6, polyamide 66, polyamide 6/66, and polyamide 6/12. The film may have a total semi-crystalline polyamide content of at least 35 volume percent, based on total film volume, and a total free shrink at 185° F. of at least 35 percent. The film may have an FTIR Transmission Absorbance A1199/A1170 ratio of up to 1.65. The film may be a retortable film, capable of being used in a process for preparing a retorted packaged product. A process for making a heat-shrinkable annular film containing the semi-crystalline polyamide comprises extruding an annular extrudate downward from an annular die, quenching the annular extrudate by applying a quenching liquid to the annular extrudate, reheating the extrudate to an orientation temperature, and orienting the reheated annular extrudate while the reheated annular extrudate is in the solid state, the orientation being carried out with a total orientation factor of at least 2, to produce a film having a total free shrink at 185° F. of at least 10 percent.
摘要翻译： 多层热收缩膜含有至少一种选自聚酰胺6，聚酰胺66，聚酰胺6/66和聚酰胺6/12的半结晶聚酰胺。 基于总膜体积，膜可以具有至少35体积％的总半结晶聚酰胺含量，并且在185°F下的总自由收缩率至少为35％。 该胶片可以具有高达1.65的FTIR透射率吸收率1199 / A 1170比。 该膜可以是能够用于制备蒸煮包装产品的方法中的可蒸煮膜。 制造含有半结晶聚酰胺的热收缩性环状膜的方法包括从环形模具向下挤出环形挤出物，通过向环形挤出物施加淬火液淬火环状挤出物，将挤出物再加热至取向温度，以及 在重新加热的环状挤出物处于固态的同时，对再加热的环状挤出物进行定向，所述取向以总取向因子至少为2进行，以产生在185°F下的总自由收缩率为至少10％ 。
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4.发明授权Process for making shrink film comprising rapidly-quenched semi-crystalline polyamide 有权用于制造包含快速淬火的半结晶聚酰胺的收缩膜的方法公开(公告)号：US07744806B2
公开(公告)日：2010-06-29
申请号：US11699532
申请日：2007-01-29
申请人： Michael E. Broadus , Richard M. Dayrit , Bryan E. Freeman , Frank M. Hofmeister , Brian P. Rivers , Roger D. Vrooman , Christopher K. Robinson , George D. Bolden , Robert W. Campbell , Nathanael R. Miranda
发明人： Michael E. Broadus , Richard M. Dayrit , Bryan E. Freeman , Frank M. Hofmeister , Brian P. Rivers , Roger D. Vrooman , Christopher K. Robinson , George D. Bolden , Robert W. Campbell , Nathanael R. Miranda
IPC分类号： B29C45/16
CPC分类号： B29C55/28 , B29C47/0021 , B29C47/0026 , B29C47/003 , B29C47/0057 , B29C47/0059 , B29C47/065 , B29C47/8805 , B29C47/883 , B29C47/8835 , B29C47/8845 , B29C47/8895 , B29C61/003 , B29K2077/00
摘要： As a first aspect, the present invention is directed to a process for making a heat-shrinkable annular film, comprising: (A) extruding an annular extrudate downward from an annular die; (B) quenching the annular extrudate by applying a quenching liquid to the annular extrudate; (C) reheating the extrudate to an orientation temperature of from 130° F. to 210° F., resulting in a reheated annular extrudate; and (D) orienting the reheated annular extrudate while the reheated annular extrudate is in the solid state, the orientation being carried out with a total orientation factor of at least 2, so that the resulting oriented, heat-shrinkable film has a total free shrink at 185° F. of at least 10 percent. The extrudate comprises at least one semi-crystalline polyamide selected from the group consisting of: (i) polyamide 6, (ii) polyamide 66, (iii) polyamide 6/66, and (iv) polyamide 6/12. The semi-crystalline polyamide makes up at least 5 volume percent of the annular extrudate. At least 50% of the quenching liquid cascades down the annular extrudate for a distance of at least 2 inches. The quenching liquid makes initial contact with the annular extrudate within 0.1 to 8 inches of the annular die.
摘要翻译： 作为第一方面，本发明涉及一种制造热收缩性环状膜的方法，包括：（A）从环形模具向下挤出环形挤出物; （B）通过向环形挤出物施加淬火液淬火环形挤出物; （C）将挤出物再加热至取向温度为130°F至210°F，得到再加热的环状挤出物; 和（D）在重新加热的环状挤出物处于固态的同时使再加热的环状挤出物定向，所述取向以总取向因子至少为2进行，使得得到的取向的热收缩膜具有总自由收缩 在185°F下至少10％。 挤出物包含至少一种选自以下的半结晶聚酰胺：（i）聚酰胺6，（ii）聚酰胺66，（iii）聚酰胺6/66和（iv）聚酰胺6/12。 半结晶聚酰胺占环形挤出物的至少5体积％。 至少50％的淬火液体将环形挤出物向下延伸至少2英寸的距离。 淬火液体与环形挤出物初始接触在环形模具的0.1至8英寸内。
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5.发明申请Process for making shrink film comprising rapidly-quenched semi-crystalline polyamide 有权用于制造包含快速淬火的半结晶聚酰胺的收缩膜的方法公开(公告)号：US20080179780A1
公开(公告)日：2008-07-31
申请号：US11699532
申请日：2007-01-29
申请人： Michael E. Broadus , Richard M. Dayrit , Bryan E. Freeman , Frank M. Hofmeister , Brian P. Rivers , Roger D. Vrooman , Christopher K. Robinson , George D. Bolden , Robert W. Campbell , Nathanael R. Miranda
发明人： Michael E. Broadus , Richard M. Dayrit , Bryan E. Freeman , Frank M. Hofmeister , Brian P. Rivers , Roger D. Vrooman , Christopher K. Robinson , George D. Bolden , Robert W. Campbell , Nathanael R. Miranda
CPC分类号： B29C55/28 , B29C47/0021 , B29C47/0026 , B29C47/003 , B29C47/0057 , B29C47/0059 , B29C47/065 , B29C47/8805 , B29C47/883 , B29C47/8835 , B29C47/8845 , B29C47/8895 , B29C61/003 , B29K2077/00
摘要： As a first aspect, the present invention is directed to a process for making a heat-shrinkable annular film, comprising: (A) extruding an annular extrudate downward from an annular die; (B) quenching the annular extrudate by applying a quenching liquid to the annular extrudate; (C) reheating the extrudate to an orientation temperature of from 130° F. to 210° F., resulting in a reheated annular extrudate; and (D) orienting the reheated annular extrudate while the reheated annular extrudate is in the solid state, the orientation being carried out with a total orientation factor of at least 2, so that the resulting oriented, heat-shrinkable film has a total free shrink at 185° F. of at least 10 percent. The extrudate comprises at least one semi-crystalline polyamide selected from the group consisting of: (i) polyamide 6, (ii) polyamide 66, (iii) polyamide 6/66, and (iv) polyamide 6/12. The semi-crystalline polyamide makes up at least 5 volume percent of the annular extrudate. At least 50% of the quenching liquid cascades down the annular extrudate for a distance of at least 2 inches. The quenching liquid makes initial contact with the annular extrudate within 0.1 to 8 inches of the annular die.
摘要翻译： 作为第一方面，本发明涉及一种制造热收缩性环状膜的方法，包括：（A）从环形模具向下挤出环形挤出物; （B）通过向环形挤出物施加淬火液淬火环形挤出物; （C）将挤出物再加热到取向温度为130°F至210°F，得到再加热的环状挤出物; 和（D）在重新加热的环状挤出物处于固态的同时使再加热的环状挤出物定向，所述取向以总取向因子至少为2进行，使得得到的取向的热收缩膜具有总自由收缩 在185°F下至少10％。 挤出物包含至少一种选自以下的半结晶聚酰胺：（i）聚酰胺6，（ii）聚酰胺66，（iii）聚酰胺6/66和（iv）聚酰胺6/12。 半结晶聚酰胺占环形挤出物的至少5体积％。 至少50％的淬火液体将环形挤出物向下延伸至少2英寸的距离。 淬火液体与环形挤出物初始接触在环形模具的0.1至8英寸内。
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公开(公告)号：US6042913A
公开(公告)日：2000-03-28
申请号：US28564
申请日：1998-02-24
IPC分类号： B65B11/52 , B32B7/02 , B32B7/06 , B32B27/08 , B32B27/28 , B32B27/32 , B65D75/26 , B65D75/30 , B65D75/58 , C08L23/08 , C08L23/16 , B65D81/20
CPC分类号： B32B7/06 , B32B27/08 , B65D75/26 , B65D75/305 , B65D75/5855 , Y10T428/14 , Y10T428/1419 , Y10T428/1452 , Y10T428/1462 , Y10T428/1471 , Y10T428/1476 , Y10T428/24331 , Y10T428/2495
摘要： A composite film and vacuum skin package for packaging a product such as a fresh red meat is disclosed. The composite film is thermoformed and sealed under vacuum to a support member to completely enclose a product which is positioned on the support member. The composite film is a permeable film weakly bonded to an impermeable film, permitting the impermeable film to be peeled from the package while leaving the permeable film intact so that the fresh red meat product can bloom from a purplish color to a desirable red color upon exposure to oxygen. The permeable and impermeable films are fully peelable without the need for a migratable wax to enhance peelability.
摘要翻译： 公开了一种用于包装诸如新鲜红肉的产品的复合膜和真空皮肤包装。 将复合膜热成型并在真空下密封到支撑构件以完全包围位于支撑构件上的产品。 复合膜是一种弱粘结到不渗透膜的渗透膜，允许不透水膜从包装上剥离，同时使可渗透膜完好无损，使得新鲜的红肉产品在暴露时可以从紫色绽放成期望的红色 到氧气。 可渗透和不渗透的膜是完全可剥离的，而不需要可迁移的蜡来增强剥离性。
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公开(公告)号：US5834079A
公开(公告)日：1998-11-10
申请号：US812637
申请日：1997-03-07
CPC分类号： C08K3/36 , B32B27/18 , C08K5/0008 , Y10T428/1352 , Y10T428/1359 , Y10T428/2826 , Y10T428/31913
摘要： An article of manufacture includes an oxygen scavenger and a zeolite. The article can be in the form of e.g. a film or sealing compound. A package can be made from the article for containing an oxygen-sensitive article such as food. The zeolite reduces migration of odor causing by-products of the oxygen scavenging process. A method of making an article of manufacture having reduced migration of byproducts of an oxygen scavenging reaction includes providing an article including an oxygen scavenger and a zeolite; and exposing the article to actinic radiation.
摘要翻译： 制品包括除氧剂和沸石。 该物品可以是例如， 胶片或密封胶。 可以从用于含有氧敏感性物品（例如食物）的物品制成包装。 沸石减少了引起氧气清除过程的副产物的气味迁移。 制造具有减少氧清除反应副产物迁移的制品的方法包括提供包含除氧剂和沸石的制品; 并将物品暴露于光化辐射。
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公开(公告)号：US06686006B1
公开(公告)日：2004-02-03
申请号：US08857276
申请日：1997-05-16
IPC分类号： B32B2704
CPC分类号： B32B27/08 , B32B7/12 , B32B2307/7244 , B32B2307/74 , B32B2439/00 , B32B2439/70 , B65D81/267 , C08K3/36 , C08K5/0008 , Y10T428/1352 , Y10T428/1359 , Y10T428/259
摘要： An article of manufacture includes an oxygen scavenger and an amorphous silica. The article can be in the form of e.g. a film or sealing compound. A package can be made from the article for containing an oxygen-sensitive article such as food. The amorphous silica reduces migration of odor causing by-products of the oxygen scavenging process. A method of making an article of manufacture having reduced migration of by-products of an oxygen scavenging reaction includes providing an article including an oxygen scavenger and an amorphous silica; and exposing the article to actinic radiation.
摘要翻译： 制品包括除氧剂和无定形二氧化硅。 该物品可以是例如， 胶片或密封胶。 可以从用于含有氧敏感性物品（例如食物）的物品制成包装。 无定形二氧化硅减少气味导致氧气清除过程的副产物的迁移。 制造具有减少氧清除反应副产物迁移的制品的方法包括提供包含除氧剂和无定形二氧化硅的制品; 并将物品暴露于光化辐射。
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公开(公告)号：US06391403B1
公开(公告)日：2002-05-21
申请号：US09691570
申请日：2000-10-18
IPC分类号： B32B2704
CPC分类号： B32B27/18 , A61L33/068 , B32B27/08 , B32B2439/00 , B32B2581/00 , C08G83/007 , C08K3/36 , C08K5/0008 , C08L71/02 , Y10T428/131 , Y10T428/1334 , Y10T428/1341 , Y10T428/1352 , Y10T428/1355 , Y10T428/1359 , Y10T428/1379 , Y10T428/1397 , Y10T428/249956 , Y10T428/2813 , Y10T428/2826 , Y10T428/31855 , Y10T428/31909 , Y10T428/31913 , C08L23/04 , C08L2666/26
摘要： An article of manufacture includes an oxygen scavenger and a zeolite. The article can be in the form of e.g. a film or sealing compound. A package can be made from the article for containing an oxygen-sensitive article such as food. The zeolite reduces migration of odor causing by-products of the oxygen scavenging process. A method of making an article of manufacture having reduced migration of by-products of an oxygen scavenging reaction includes providing an article including an oxygen scavenger and a zeolite; and exposing the article to actinic radiation.
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10.发明授权Method and apparatus for triggering oxygen scavenging material as a wall component in a container 失效用于将氧气清除材料作为容器中的壁组分触发的方法和装置公开(公告)号：US06233907B1
公开(公告)日：2001-05-22
申请号：US09230595
申请日：1999-06-24
IPC分类号： B65D8124
CPC分类号： B65D81/267
摘要： A method for triggering an oxygen scavenging component of a container for packaging an oxygen sensitive material includes the steps of providing a container defining an internal space and having an internal oxygen scavenging component including an oxidizable organic compound, exposing the oxygen scavenging component to a source of actinic radiation, positioned within said internal space, at a wavelength, intensity, and residence time so as to provide a dose of actinic radiation sufficient to activate the oxygen scavenging component, and packaging an oxygen sensitive material in the internal space of the container whereby the oxygen scavenging component scavenges the oxygen from the internal space of the container. An apparatus and packaging system are also disclosed.
摘要翻译： 触发用于包装氧敏感材料的容器的除氧组分的方法包括以下步骤：提供限定内部空间并具有包含可氧化有机化合物的内部氧清除组分的容器，将氧清除组分暴露于 光化辐射，位于所述内部空间内，以波长，强度和停留时间，以提供足以激活除氧组分的光化辐射剂量，以及将氧敏感材料包装在容器的内部空间中，由此， 除氧组分清除容器内部空间的氧气。 还公开了一种装置和包装系统。
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