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公开(公告)号：US20050181223A1
公开(公告)日：2005-08-18
申请号：US11046751
申请日：2005-02-01
IPC分类号： B32B15/088 , B32B15/08 , C08G69/26 , C09J179/08 , H05K1/03 , H05K3/38
CPC分类号： B32B7/12 , B32B15/08 , B32B15/20 , B32B27/06 , B32B27/281 , B32B27/34 , B32B2307/306 , B32B2307/74 , H05K1/0346 , H05K3/386 , H05K2201/0145 , H05K2201/0154 , H05K2201/0355 , Y10T428/31681
摘要： A flexible metal foil-polyimide laminate is prepared by joining a polyimide film to a metal foil via an intervening adhesive layer. The adhesive is a mixture of polyamic acids: (A) the reaction product of 3,4,3′,4′-biphenyltetracarboxylic anhydride with p-phenylenediamine, (B) the reaction product of 3,4,3′,4′-biphenyltetracarboxylic anhydride with 4,4′-diaminodiphenyl ether, and (C) the reaction product of pyromellitic dianhydride with 4,4′-diaminodiphenyl ether, in a weight ratio (A+B)/C between 75/25 and 25/75. The method is simple and inexpensive, and yields a flexible metal foil-polyimide laminate that is improved in peel strength and curling resistance while maintaining the heat resistance of polyimide.
摘要翻译： 通过中间粘合剂层将聚酰亚胺膜与金属箔接合来制备柔性金属箔 - 聚酰亚胺层压体。 粘合剂是聚酰胺酸的混合物：（A）3,4,3'，4'-联苯四羧酸酐与对苯二胺的反应产物，（B）3,4,3'，4'- 联苯四羧酸酐与4,4'-二氨基二苯醚，（C）均苯四酸二酐与4,4'-二氨基二苯醚的反应产物，重量比（A + B）/ C在75/25和25/75之间。 该方法简单且便宜，并且产生柔软的金属箔 - 聚酰亚胺层压板，其在保持聚酰亚胺的耐热性的同时提高了剥离强度和抗卷曲性。
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2.发明申请公开(公告)号：US20060257660A1
公开(公告)日：2006-11-16
申请号：US11430622
申请日：2006-05-09
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： B32B5/16
CPC分类号： C08F6/008 , C08K3/36 , Y10T428/2982 , C08L27/06
摘要： The present invention provides an antistatic agent for vinyl chloride-based resins which can impart superior antistatic properties to the vinyl chloride-based resin, and which can thereby solve various problems arising from charging of the vinyl chloride-based resin with static electricity, a vinyl chloride-based resin composition containing this antistatic agent, and a method for manufacturing this composition. The present invention provides an antistatic agent for vinyl chloride-based resins which consists of silica particles containing at least 99.0% by mass of SiO2 and 0.00005% 80.5 ppm by mass or less of sodium, and which has such a particle size distribution that at least 98% by mass of the silica particles is occupied by the particles having a particle diameter in the range from 30 to 1,000 nm.
摘要翻译： 本发明提供了一种氯乙烯类树脂的抗静电剂，其可以赋予氯乙烯类树脂优异的抗静电性能，从而可以解决由静电装入氯乙烯类树脂引起的各种问题，乙烯基 含有该抗静电剂的氯化物系树脂组合物及其制造方法。 本发明提供了一种氯乙烯类树脂的抗静电剂，其由含有至少99.0质量％SiO 2和0.00005％80.5质量ppm以下的二氧化硅粒子构成，其具有 这样的粒度分布，使得至少98质量％的二氧化硅粒子被粒径在30〜1000nm的粒子占据。
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公开(公告)号：US07847012B2
公开(公告)日：2010-12-07
申请号：US11758418
申请日：2007-06-05
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： C08L27/06
CPC分类号： C08J9/0038 , C04B26/08 , C04B2111/00129 , C08J9/0066 , C08J2327/06 , C08K3/013 , C08K3/04 , C08K5/49 , C08L27/06 , C08L27/18 , C08L2205/02 , C04B14/024 , C04B14/042 , C04B14/06 , C04B14/10 , C04B14/28 , C04B14/303 , C04B14/304 , C04B14/305 , C04B24/003 , C04B24/2682 , C04B38/02 , C08L2666/04
摘要： A thermally expandable vinyl chloride resin composition is provided. It includes (A) 100 parts by mass of a vinyl chloride resin, (B) 5 to 200 parts by mass of an inorganic filler, (C) 10 to 300 parts by mass of a thermally expandable graphite, (D) 0.1 to 10 parts by mass of a fluororesin, and (E) 10 to 300 parts by mass of a phosphorus compound. The composition exhibits favorable thermal expansion properties and favorable shape retention following thermal expansion upon exposure to high temperatures.
摘要翻译： 提供了一种热膨胀性氯乙烯树脂组合物。 它包括（A）100质量份氯乙烯树脂，（B）5至200质量份无机填料，（C）10至300质量份可热膨胀石墨，（D）0.1至10 质量份的氟树脂，（E）10〜300质量份的磷化合物。 该组合物在暴露于高温下时显示出良好的热膨胀性能和良好的热膨胀后的形状保持性。
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4.发明授权公开(公告)号：US07514495B2
公开(公告)日：2009-04-07
申请号：US11430622
申请日：2006-05-09
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： C08K3/36
CPC分类号： C08F6/008 , C08K3/36 , Y10T428/2982 , C08L27/06
摘要： The present invention provides an antistatic agent for vinyl chloride-based resins which can impart superior antistatic properties to the vinyl chloride-based resin, and which can thereby solve various problems arising from charging of the vinyl chloride-based resin with static electricity, a vinyl chloride-based resin composition containing this antistatic agent, and a method for manufacturing this composition. The present invention provides an antistatic agent for vinyl chloride-based resins which consists of silica particles containing at least 99.0% by mass of SiO2 and 0.00005% 80.5 ppm by mass or less of sodium, and which has such a particle size distribution that at least 98% by mass of the silica particles is occupied by the particles having a particle diameter in the range from 30 to 1,000 nm.
摘要翻译： 本发明提供了一种氯乙烯类树脂的抗静电剂，其可以赋予氯乙烯类树脂优异的抗静电性能，从而可以解决由静电装入氯乙烯类树脂引起的各种问题，乙烯基 含有该抗静电剂的氯化物系树脂组合物及其制造方法。 本发明提供了一种氯乙烯类树脂的抗静电剂，其由含有至少99.0质量％的SiO 2和0.00005％的80.5质量ppm以下的二氧化硅粒子组成，并且其粒径分布至少为 二氧化硅粒子的98质量％被粒径在30〜1000nm的粒子所占据。
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公开(公告)号：US20070282027A1
公开(公告)日：2007-12-06
申请号：US11758418
申请日：2007-06-05
申请人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
发明人： Tatsuya Fujimoto , Ken Yahata , Tadashi Amano
IPC分类号： C08L75/00
CPC分类号： C08J9/0038 , C04B26/08 , C04B2111/00129 , C08J9/0066 , C08J2327/06 , C08K3/013 , C08K3/04 , C08K5/49 , C08L27/06 , C08L27/18 , C08L2205/02 , C04B14/024 , C04B14/042 , C04B14/06 , C04B14/10 , C04B14/28 , C04B14/303 , C04B14/304 , C04B14/305 , C04B24/003 , C04B24/2682 , C04B38/02 , C08L2666/04
摘要： A thermally expandable vinyl chloride resin composition is provided. It includes (A) 100 parts by mass of a vinyl chloride resin, (B) 5 to 200 parts by mass of an inorganic filler, (C) 10 to 300 parts by mass of a thermally expandable graphite, (D) 0.1 to 10 parts by mass of a fluororesin, and (E) 10 to 300 parts by mass of a phosphorus compound. The composition exhibits favorable thermal expansion properties and favorable shape retention following thermal expansion upon exposure to high temperatures.
摘要翻译： 提供了一种热膨胀性氯乙烯树脂组合物。 它包括（A）100质量份氯乙烯树脂，（B）5至200质量份无机填料，（C）10至300质量份可热膨胀石墨，（D）0.1至10 质量份的氟树脂，（E）10〜300质量份的磷化合物。 该组合物在暴露于高温下时显示出良好的热膨胀性能和良好的热膨胀后的形状保持性。
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6.发明授权Process of producing vinyl chloride polymer by using condensation product of dimer of 2,3-dihydroxynaphthalene and formaldehyde 失效通过使用2,3-二羟基萘和甲醛的二聚体的缩合产物生产氯乙烯聚合物的方法
公开(公告)号：US06121390A
公开(公告)日：2000-09-19
申请号：US019803
申请日：1998-02-06
CPC分类号： C08F2/004
摘要： There is provided a polymer scale deposition preventive agent, comprising an alkaline solution of a condensation product having a molecular weight of 500 to 1,000,000 obtained by condensing a dimer compound of 2,3-dihydroxynaphthalene with formaldehyde. By polymerizing vinyl chloride or a monomer mixture containing vinyl chloride in a polymerization vessel wherein a coating film made of said polymer scale deposition preventive agent has been formed on the inner wall surface and the like, polymer scale is effectively prevented from depositing not only on an agitation apparatus but also on areas near the interface between a gas phase and a liquid phase, which prevention of the polymer scale deposition is conventionally difficult. Thus, a vinyl chloride polymer can be obtained which contains colored foreign matters, fish eyes, etc. in small amounts and is small in initial discoloration and is good in quality.
摘要翻译： 提供了一种聚合物垢沉积防止剂，其包含通过将2,3-二羟基萘的二聚体与甲醛缩合得到的分子量为500至1,000,000的缩合产物的碱性溶液。 通过在聚合容器中聚合氯乙烯或含有氯乙烯的单体混合物，其中在内壁表面等上形成由所述聚合物垢沉积防止剂制成的涂膜，有效地防止了聚合物垢不仅沉积在 搅拌装置，而且在气相和液相之间的界面附近的区域，传统上难以防止聚合物垢沉积。 因此，可以获得少量含有有色异物，鱼眼等的氯乙烯聚合物，并且初始变色小，质量好。
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公开(公告)号：US5294684A
公开(公告)日：1994-03-15
申请号：US973570
申请日：1992-11-09
申请人： Ichiro Kaneko , Makoto Fujiwara , Tatsuya Fujimoto
发明人： Ichiro Kaneko , Makoto Fujiwara , Tatsuya Fujimoto
CPC分类号： C08F14/06
摘要： A process for producing a vinyl chloride polymer by polymerizing a monomer comprising vinyl chloride by suspension polymerization in a polymerization vessel on the inner wall surface of which a coating of a polymer scale preventive agent is formed, comprising the steps of applying a high-speed shearing force to a mixture comprising water, the monomer, a polymerization initiator, and (A) a dispersant comprising a partially saponified polyvinyl alcohol having a specified average degree of polymerization and a specified degree of saponification plus (B) a dispersant comprising a hydroxypropylmethylcellulose which has a specified methoxyl substitution degree, a specified hydroxypropoxyl substitution degree, and a specified viscosity and subjecting the mixture to said suspension polymerization. A vinyl chloride polymer having an average particle diameter of 200 to 600 .mu.m and a narrow particle size distribution and excellent in plasticizer take-up, etc. is provided.
摘要翻译： 一种通过在其内壁表面上形成聚合物防垢剂的涂层的聚合容器中通过悬浮聚合使包含氯乙烯的单体聚合来制备氯乙烯聚合物的方法，包括以下步骤：施加高速剪切 对包含水，单体，聚合引发剂的混合物和（A）包含具有指定的平均聚合度和指定皂化度的部分皂化的聚乙烯醇的分散剂加上（B）包含羟丙基甲基纤维素的分散剂，所述分散剂具有 指定的甲氧基取代度，特定的羟丙氧基取代度和指定的粘度，并使混合物进行所述悬浮聚合。 提供平均粒径为200〜600（my）m且窄的粒度分布，增塑剂吸收性优异的氯乙烯系聚合物。
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8.发明授权Composition comprising condensation product of dimer of 2,3-dihydroxynaphthalene and formaldehyde for polymerization 失效组合物，其包含2,3-二羟基萘的二聚体与甲醛的缩合产物，用于聚合公开(公告)号：US06326454B1
公开(公告)日：2001-12-04
申请号：US09595894
申请日：2000-06-20
IPC分类号： C08G820
CPC分类号： C08F2/004
摘要： There is provided a polymer scale deposition preventive agent, comprising an alkaline solution of a condensation product having a molecular weight of 500 to 1,000,000 obtained by condensing a dimer compound of 2,3-dihydroxynaphthalene with formaldehyde. By polymerizing vinyl chloride or a monomer mixture containing vinyl chloride in a polymerization vessel wherein a coating film made of said polymer scale deposition preventive agent has been formed on the inner wall surface and the like, polymer scale is effectively prevented from depositing not only on an agitation apparatus but also on areas near the interface between a gas phase and a liquid phase, which prevention of the polymer scale deposition is conventionally difficult. Thus, a vinyl chloride polymer can be obtained which contains colored foreign matters, fish eyes, etc. in small amounts and is small in initial discoloration and is good in quality.
摘要翻译： 提供了一种聚合物垢沉积防止剂，其包含通过将2,3-二羟基萘的二聚体与甲醛缩合得到的分子量为500至1,000,000的缩合产物的碱性溶液。 通过在聚合容器中聚合氯乙烯或含有氯乙烯的单体混合物，其中在内壁表面等上形成由所述聚合物垢沉积防止剂制成的涂膜，有效地防止了聚合物垢不仅沉积在 搅拌装置，而且在气相和液相之间的界面附近的区域，传统上难以防止聚合物垢沉积。 因此，可以获得少量含有有色异物，鱼眼等的氯乙烯聚合物，并且初始变色小，质量好。
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公开(公告)号：US06288258B1
公开(公告)日：2001-09-11
申请号：US09694370
申请日：2000-10-24
申请人： Mikio Aramata , Tatsuya Fujimoto , Ryuichi Saito , Masahiro Yuyama , Tetsuya Inukai , Hajime Ishizaka
发明人： Mikio Aramata , Tatsuya Fujimoto , Ryuichi Saito , Masahiro Yuyama , Tetsuya Inukai , Hajime Ishizaka
IPC分类号： C07F216
CPC分类号： C07F7/16
摘要： When oganohalosilanes are prepared by charging a reactor with a contact mass containing metallic silicon and a copper catalyst and introducing an organohalide-containing gas into the reactor to effect the direct reaction, 50-10,000 ppm of bronze phosphide is added to the contact mass. The invention is successful in efficiently producing organohalosilanes in a high STY and low T/D.
摘要翻译： 当通过向包含金属硅和铜催化剂的接触物质装入反应器并将含有机卤化物的气体引入反应器以进行直接反应来制备原料卤代硅烷时，将50-10,000ppm的青铜磷化物加入到接触物质中。 本发明成功地在高STY和低T / D下高效地生产有机卤代硅烷。
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