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公开(公告)号：US08598290B2
公开(公告)日：2013-12-03
申请号：US12307022
申请日：2007-06-29
申请人： Mitsuru Kishine , Masanori Kitaichi , Yousuke Nishimura , Manabu Fujisawa , Yoshiki Tanaka , Shintarou Ogata , Yutaka Ueta , Shigeru Morita
发明人： Mitsuru Kishine , Masanori Kitaichi , Yousuke Nishimura , Manabu Fujisawa , Yoshiki Tanaka , Shintarou Ogata , Yutaka Ueta , Shigeru Morita
IPC分类号： C08F14/18
CPC分类号： C08F214/18 , C08F14/18 , C08F2/22
摘要： The present invention provides a method of producing a fluoroelastomer excellent in dispersion stability at low cost, at a high rate of polymerization and in high yields. The present invention is a method of producing a fluoroelastomer comprising an emulsion polymerization of a fluorinated monomer in the presence of a water-soluble radical polymerization initiator, wherein the emulsion polymerization is carried out in the presence of a compound (1) containing a functional group reactive in radical polymerization and a hydrophilic group and a fluorinated compound (2) containing a fluorocarbon group comprising 1 to 6 continuously united carbon atom with fluorine atom directly bound to each of them as well as a hydrophilic group.
摘要翻译： 本发明提供以低成本，高聚合速率和高产率制备分散稳定性优异的含氟弹性体的方法。 本发明是一种在水溶性自由基聚合引发剂的存在下包含含氟单体的乳液聚合的含氟弹性体的方法，其中乳液聚合在含有官能团的化合物（1）的存在下进行， 自由基聚合反应性和亲水性基团以及含有含有1〜6个连续碳原子的碳氟化合物的含氟化合物（2）和与其各自直接键合的氟原子以及亲水基团。
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公开(公告)号：US20090234086A1
公开(公告)日：2009-09-17
申请号：US12307022
申请日：2007-06-29
申请人： Mitsuru Kishine , Masanori Kitaichi , Yousuke Nishimura , Manabu Fujisawa , Yoshiki Tanaka , Shintarou Ogata , Yutaka Ueta , Shigeru Morita
发明人： Mitsuru Kishine , Masanori Kitaichi , Yousuke Nishimura , Manabu Fujisawa , Yoshiki Tanaka , Shintarou Ogata , Yutaka Ueta , Shigeru Morita
CPC分类号： C08F214/18 , C08F14/18 , C08F2/22
摘要： The present invention provides a method of producing a fluoroelastomer excellent in dispersion stability at low cost, at a high rate of polymerization and in high yields.The present invention is a method of producing a fluoroelastomer comprising an emulsion polymerization of a fluorinated monomer in the presence of a water-soluble radical polymerization initiator, wherein the emulsion polymerization is carried out in the presence of a compound (1) containing a functional group reactive in radical polymerization and a hydrophilic group and a fluorinated compound (2) containing a fluorocarbon group comprising 1 to 6 continuously united carbon atom with fluorine atom directly bound to each of them as well as a hydrophilic group.
摘要翻译： 本发明提供以低成本，高聚合速率和高产率制备分散稳定性优异的含氟弹性体的方法。 本发明是一种在水溶性自由基聚合引发剂的存在下包含含氟单体的乳液聚合的含氟弹性体的方法，其中乳液聚合在含有官能团的化合物（1）的存在下进行， 自由基聚合反应性和亲水性基团以及含有含有1〜6个连续碳原子的碳氟化合物的含氟化合物（2）和与其各自直接键合的氟原子以及亲水基团。
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公开(公告)号：US09273172B2
公开(公告)日：2016-03-01
申请号：US12168454
申请日：2008-07-07
IPC分类号： C08F214/22 , C08F2/26 , C08F2/44
CPC分类号： C08F214/22 , C08F2/26
摘要： The present invention provides a method for producing a fluoroelastomer using an emulsifier which is inexpensive and hardly remains in product polymers. The present invention is related to a method for producing a fluoroelastomer, wherein vinylidene fluoride and at least one fluoroolefin monomer other than vinylidene fluoride are copolymerized in the manner of an emulsion polymerization in the presence of an emulsifier represented by C5F11COOM, wherein M represents H, NH4 or an alkali metal.
摘要翻译： 本发明提供使用廉价且几乎不残留在产品聚合物中的乳化剂制备含氟弹性体的方法。 本发明涉及一种含氟弹性体的制造方法，其中在由C5F11COOM表示的乳化剂的存在下，以偏二氟乙烯为单位，将聚偏二氟乙烯和至少一种氟烯烃单体以乳液聚合的方式共聚，其中M表示H， NH4或碱金属。
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4.发明申请公开(公告)号：US20060281946A1
公开(公告)日：2006-12-14
申请号：US10562730
申请日：2004-07-02
IPC分类号： C07C59/135
摘要： This invention provides a novel compound which can be properly used as a surfactant, a method of producing a fluoropolymer, surfactant and a fluoropolymer aqueous dispersions using the novel compound. This invention is a fluoroalkylcarboxylic acid derivative which is represented by the general formula (i): Rf1(OCH2CF2CF2)n1OCX1X2CF2(Rf2)n2COOM (i) wherein Rf1 represents a straight or branched fluoroalkyl group containing 1 to 20 carbon atoms, which fluoroalkyl group may optionally contain 1 to 5 oxygen atoms in the principal chain thereof, Rf2 represents a straight or branched fluoroalkylene group containing 1 to 25 carbon atoms, said fluoroalkylene group may optionally contain 1 to 5 oxygen atoms in the principal chain thereof, n1 represents an integer of 0 to 3, n2 represents an integer of 0 or 1, X1 and X2 are the same or different and each represents hydrogen atom or fluorine atom, and M represents NH4 or a monovalent metal element.
摘要翻译： 本发明提供了可以适当地用作表面活性剂的新型化合物，使用该新化合物的含氟聚合物，表面活性剂和含氟聚合物水分散体的制造方法。 本发明是由通式（i）表示的氟代烷基羧酸衍生物：<？in-line-formula description =“In-line formula”end =“lead”？> Rf < OCH 2 2 CF 2 2 CF 2）n 1 OCX 1 X 2 CF 2（Rf 2）N 2 COOM（i）<？in-line-formula description =“In-Line Formulas “end =”tail“？>其中Rf 1表示含有1至20个碳原子的直链或支链氟烷基，该氟烷基可以任选地在其主链中含有1至5个氧原子，Rf 代表含有1至25个碳原子的直链或支链氟代亚烷基，所述氟亚烷基可以任选地在其主链中含有1至5个氧原子，n1表示0-3的整数，n2表示 0或1的整数，X 1和X 2相同或不同，各自表示氢原子或氟原子，M表示NH 4 或一价金属元素。
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5.发明授权公开(公告)号：US07589234B2
公开(公告)日：2009-09-15
申请号：US10562730
申请日：2004-07-02
IPC分类号： C07C59/135
摘要： This invention provides a novel compound which can be properly used as a surfactant, a method of producing a fluoropolymer, surfactant and a fluoropolymer aqueous dispersions using the novel compound.This invention is a fluoroalkylcarboxylic acid derivative which is represented by the general formula (i): Rf1(OCH2CF2CF2)n1OCX1X2CF2(Rf2)n2COOM (i) wherein Rf1 represents a straight or branched fluoroalkyl group containing 1 to 20 carbon atoms, which fluoroalkyl group may optionally contain 1 to 5 oxygen atoms in the principal chain thereof, Rf2 represents a straight or branched fluoroalkylene group containing 1 to 25 carbon atoms, said fluoroalkylene group may optionally contain 1 to 5 oxygen atoms in the principal chain thereof, n1 represents an integer of 0 to 3, n2 represents an integer of 0 or 1, X1 and X2 are the same or different and each represents hydrogen atom or fluorine atom, and M represents NH4 or a monovalent metal element.
摘要翻译： 本发明提供了可以适当地用作表面活性剂的新型化合物，使用该新化合物的含氟聚合物，表面活性剂和含氟聚合物水分散体的制造方法。 本发明是由通式（i）表示的氟代烷基羧酸衍生物：<？in-line-formula description =“In-line formula”end =“lead”→Rf1（OCH2CF2CF2）n1OCX1X2CF2（Rf2）n2COOM i）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中Rf1表示含有1至20个碳原子的直链或支链氟代烷基，该氟代烷基可任选地含有1至5个氧 其中，R 2表示碳原子数1〜25的直链或支链的氟代亚烷基，所述氟代亚烷基可以在其主链中含有1〜5个氧原子，n1表示0〜3的整数，n2表示 0或1的整数，X 1和X 2相同或不同，各自表示氢原子或氟原子，M表示NH 4或一价金属元素。
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6.发明授权公开(公告)号：US08198480B2
公开(公告)日：2012-06-12
申请号：US12537220
申请日：2009-08-06
IPC分类号： C07C59/135
摘要： This invention provides a novel compound which can be properly used as a surfactant, a method of producing a fluoropolymer, surfactant and a fluoropolymer aqueous dispersions using the novel compound. This invention is a fluoroalkylcarboxylic acid derivative which is represented by the general formula (i): Rf1(OCH2CF2CF2)n1OCX1X2CF2(Rf2)n2COOM (i) wherein Rf1 represents a straight or branched fluoroalkyl group containing 1 to 20 carbon atoms, which fluoroalkyl group may optionally contain 1 to 5 oxygen atoms in the principal chain thereof, Rf2 represents a straight or branched fluoroalkylene group containing 1 to 25 carbon atoms, said fluoroalkylene group may optionally contain 1 to 5 oxygen atoms in the principal chain thereof, n1 represents an integer of 0 to 3, n2 represents an integer of 0 or 1, X1 and X2 are the same or different and each represents hydrogen atom or fluorine atom, and M represents NH4 or a monovalent metal element.
摘要翻译： 本发明提供了可以适当地用作表面活性剂的新型化合物，使用该新化合物的含氟聚合物，表面活性剂和含氟聚合物水分散体的制造方法。 本发明是由通式（i）表示的氟代烷基羧酸衍生物：Rf1（OCH2CF2CF2）n1OCX1X2CF2（Rf2）n2COOM（i）其中Rf1表示含有1至20个碳原子的直链或支链氟代烷基，该氟代烷基可以 在其主链中任选含有1至5个氧原子，Rf2表示含有1至25个碳原子的直链或支链氟代亚烷基，所述氟代亚烷基可以任选地在其主链中含有1至5个氧原子，n1表示整数 0〜3，n2表示0或1的整数，X1和X2相同或不同，表示氢原子或氟原子，M表示NH4或一价金属元素。
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公开(公告)号：US20080227948A1
公开(公告)日：2008-09-18
申请号：US11547662
申请日：2005-04-05
IPC分类号： C08G63/78 , C08G73/00 , C08G63/83 , C08G63/682 , C08G63/685 , C08G63/688
摘要： The present invention provides an elastomeric fluoropolymer excellent in productivity and crosslinkability and a method of producing the same. The present invention is an elastomeric fluoropolymer having a vinyl group-containing fluorinated emulsifier-derived unit (A) and a unit (B) derived from a cure site monomer (b1) and/or bromine atom- and/or iodine atom-containing saturated aliphatic compound (b2), wherein the vinyl group-containing fluorinated emulsifier is a compound having a radical polymerizable unsaturated bond and a hydrophilic group within the molecule.
摘要翻译： 本发明提供了生产率和交联性优异的弹性体含氟聚合物及其制造方法。 本发明是具有含乙烯基的含氟乳化剂衍生单元（A）和由固化部位单体（b1）衍生的单元（B）和/或含有溴原子和/或含碘原子的饱和的单体（B）的弹性体含氟聚合物 脂肪族化合物（b2），其中含乙烯基的含氟乳化剂是分子内具有自由基聚合性不饱和键和亲水基团的化合物。
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公开(公告)号：US20080114118A1
公开(公告)日：2008-05-15
申请号：US11547637
申请日：2005-04-05
摘要： Disclosed is a method for producing a fluorine-containing elastomer polymer which is excellent in productivity and crosslinkability. Specifically disclosed is a method for producing a fluorine-containing elastomer polymer wherein a fluorine-containing monomer is polymerized in an aqueous solvent in the presence of an emulsifying agent containing a fluorine-containing vinyl group and a chain transfer agent. This method for producing a fluorine-containing elastomer polymer is characterized in that the emulsifying agent containing a fluorine-containing vinyl group is composed of a compound having a radically polymerizable unsaturated bond and a hydrophilic group in a molecule.
摘要翻译： 公开了一种生产性和交联性优异的含氟弹性体聚合物的制造方法。 具体公开了一种含氟弹性体聚合物的制造方法，其中含氟单体在含有含氟乙烯基和链转移剂的乳化剂存在下，在含水溶剂中聚合。 该含氟弹性体聚合物的制造方法的特征在于，含有含氟乙烯基的乳化剂由分子内具有自由基聚合性不饱和键和亲水性基团的化合物构成。
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公开(公告)号：US20120306911A1
公开(公告)日：2012-12-06
申请号：US13467386
申请日：2012-05-09
申请人： Tomohiko Okazaki , Michinari Kohno , Yoichi Kobori , Yoshiki Tanaka , Fujio Nobori , Mitsuhiro Hosoki
发明人： Tomohiko Okazaki , Michinari Kohno , Yoichi Kobori , Yoshiki Tanaka , Fujio Nobori , Mitsuhiro Hosoki
IPC分类号： G09G5/00
CPC分类号： G06Q30/0251 , G09F27/00
摘要： According to an illustrative embodiment, a display control method is provided. The method includes defining at least one clipping region, within an image to be displayed, according to detected object information, and defining clipping region content for displaying in the clipping region.
摘要翻译： 根据说明性实施例，提供了显示控制方法。 该方法包括根据检测到的对象信息定义要显示的图像内的至少一个剪切区域，并且定义用于在裁剪区域中显示的剪切区域内容。
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公开(公告)号：US08124173B2
公开(公告)日：2012-02-28
申请号：US12329960
申请日：2008-12-08
CPC分类号： H05K3/285 , H01L23/296 , H01L2224/16225 , H01L2924/00014 , H01L2924/3011 , H05K3/3452 , H05K2201/0162 , Y10T29/49171 , Y10T29/49224 , H01L2224/0401
摘要： A process for packaging an electronic device employs an insulating protective resin layer produced from one or more of the resin compositions: (1) 100 parts of an organic solvent-soluble resin having a polysiloxane skeleton and a polar group, 0.5 to 30 parts of an epoxy compound having an epoxy equivalent of more than 800, and an organic solvent, (2) 100 parts of an organic solvent-soluble resin having a polysiloxane skeleton and a polar group, 0.1 to 10 parts of an epoxy compound having an epoxy equivalent of 100 to 800, 2 to 30 weight parts of a polyvalent isocyanate compound, and an organic solvent; and (3) 100 parts of an organic solvent-soluble resin having a polysiloxane skeleton and a polar group, 0.1 to 20 parts of an epoxy compound having an epoxy equivalent of more than 800, 2 to 30 parts of a polyvalent isocyanate compound, and an organic solvent.
摘要翻译： 包装电子装置的方法采用由一种或多种树脂组合物制成的绝缘保护树脂层：（1）100份具有聚硅氧烷骨架和极性基团的有机溶剂可溶性树脂，0.5〜30份 环氧当量大于800的环氧化合物和有机溶剂，（2）100份具有聚硅氧烷骨架和极性基团的有机溶剂可溶性树脂，0.1至10份具有环氧当量的环氧当量的环氧化合物 100〜800,2重量份至30重量份的多价异氰酸酯化合物和有机溶剂; 和（3）100份具有聚硅氧烷骨架和极性基团的有机溶剂可溶性树脂，0.1〜20份环氧当量大于800的环氧化合物，2〜30份多价异氰酸酯化合物，以及 有机溶剂。
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