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公开(公告)号：US06689193B1
公开(公告)日：2004-02-10
申请号：US10018740
申请日：2002-04-25
IPC分类号： B22F904
CPC分类号： C22C23/00 , B22F9/023 , B22F9/04 , B22F2009/041 , B22F2998/00 , B22F2998/10 , B22F2999/00 , C01B3/0031 , C01B3/0042 , C22C1/0408 , H01M4/02 , H01M4/383 , H01M4/46 , Y02E60/327 , Y10S420/90 , B22F1/0044
摘要： To produce a hydrogen absorbing alloy powder, a starting powder and a plurality of balls are thrown into a container of a ball mill, and then, the inside of the container is maintained in a hydrogen atmosphere to conduct a mechanical alloying.
摘要翻译： 为了制造吸氢合金粉末，将起始粉末和多个球投入球磨机的容器中，然后将容器内保持在氢气氛中进行机械合金化。
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公开(公告)号：US20120040825A9
公开(公告)日：2012-02-16
申请号：US12974264
申请日：2010-12-21
申请人： Mitsuya Hosoe , Izuru Kanoya , Terumi Furuta , Hiroshi Sakai
发明人： Mitsuya Hosoe , Izuru Kanoya , Terumi Furuta , Hiroshi Sakai
IPC分类号： B01J20/02
CPC分类号： C01B3/0031 , F17C11/005 , Y02E60/321 , Y02E60/327 , Y02E60/362
摘要： A mixed powder of AlH3 and MgH2 is ball-milled in a hydrogen atmosphere while applying force of 5 G through 30 G (in which G is gravitational acceleration), and the thus-obtained milled product is dehydrogenated to produce a hydrogen storage material. The hydrogen storage material comprises an amorphous phase containing an Al—Mg alloy as a mother phase, and a crystalline Al phase having a maximum length of 100 nm or less, the crystalline Al phase being distributed as a dispersed phase in the mother phase.
摘要翻译： 将AlH3和MgH2的混合粉末在氢气气氛中球磨，同时施加5G至30G（其中G为重力加速度）的力，并将由此获得的研磨产物脱氢以产生储氢材料。 储氢材料包括含有作为母相的Al-Mg合金的非晶相和最大长度为100nm以下的结晶Al相，所述结晶Al相以分散相分布在母相中。
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公开(公告)号：US20060054022A1
公开(公告)日：2006-03-16
申请号：US11226029
申请日：2005-09-14
申请人： Mitsuya Hosoe , Izuru Kanoya , Ryogo Sakamoto , Terumi Furuta , Hajime Goto
发明人： Mitsuya Hosoe , Izuru Kanoya , Ryogo Sakamoto , Terumi Furuta , Hajime Goto
IPC分类号： B01D53/02
CPC分类号： B82Y30/00 , F17C11/005 , Y02E60/321 , Y02E60/324 , Y10S502/526
摘要： A hydrogen storage tank comprises a hydrogen adsorbent accommodated in a pressure-resistant container. The hydrogen adsorbent is capable of adsorbing and retaining hydrogen gas of a volume exceeding an occupation volume occupied by the hydrogen adsorbent itself. As for the hydrogen adsorbent, the amount of endothermic heat, which is generated when the adsorbed hydrogen gas is released, is not more than 16 kJ per mol of hydrogen molecules. The hydrogen adsorbent is prevented from leaking outside of the pressure-resistant container by a filter.
摘要翻译： 储氢罐包括容纳在耐压容器中的氢吸附剂。 氢吸附剂能够吸附和保留体积超过氢吸附剂本身占据的占有体积的氢气。 对于氢吸附剂，吸附氢气释放时产生的吸热量不大于16kJ / mol氢分子。 通过过滤器防止氢吸附剂泄漏到耐压容器的外部。
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公开(公告)号：US08258077B2
公开(公告)日：2012-09-04
申请号：US13019340
申请日：2011-02-02
申请人： Mitsuya Hosoe , Izuru Kanoya , Hiroshi Sakai , Terumi Furuta
发明人： Mitsuya Hosoe , Izuru Kanoya , Hiroshi Sakai , Terumi Furuta
CPC分类号： B01J20/02 , B01J20/0211 , B01J20/3021 , B82Y30/00 , Y02E60/324 , Y02E60/362
摘要： A crystalline Al phase and a crystalline TiH2 phase each having a maximum length of 200 nm or less are dispersed in an amorphous phase containing an Al—Mg alloy to obtain a hydrogen storage material capable of reversibly storing and releasing hydrogen.
摘要翻译： 将具有最大长度为200nm以下的结晶Al相和结晶性TiH 2相分散在含有Al-Mg合金的非晶相中，得到能够可逆地储存和释放氢的储氢材料。
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公开(公告)号：US20110065921A1
公开(公告)日：2011-03-17
申请号：US12879068
申请日：2010-09-10
申请人： Hiroshi Sakai , Izuru Kanoya , Terumi Furuta , Mitsuya Hosoe
发明人： Hiroshi Sakai , Izuru Kanoya , Terumi Furuta , Mitsuya Hosoe
IPC分类号： C07F1/08
CPC分类号： C07F1/005
摘要： An organometallic complex [Cu2(pyridine-3,5-dicarboxylate)2]n is provided by bonding a plurality of Cu2(pyridine-3,5-dicarboxylate)2 repeating units to each other. The organometallic complex can be obtained by the steps of dissolving copper acetate monohydrate or anhydrate and pyridine-3,5-dicarboxylic acid in a solvent, heating the solution at 50° C. to 140° C. for 24 to 168 hours to generate a reaction product, and then removing a guest molecule from the reaction product.
摘要翻译： 通过将多个Cu 2（吡啶-3,5-二羧酸酯）2重复单元彼此结合而提供有机金属络合物[Cu2（吡啶-3,5-二羧酸酯）2] n。 有机金属络合物可以通过以下步骤获得：将乙酸铜一水合物或无水物和吡啶-3,5-二羧酸溶解在溶剂中，将溶液在50℃加热至140℃24至168小时，以产生 反应产物，然后从反应产物中除去客体分子。
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公开(公告)号：US08394738B2
公开(公告)日：2013-03-12
申请号：US12974264
申请日：2010-12-21
申请人： Mitsuya Hosoe , Izuru Kanoya , Terumi Furuta , Hiroshi Sakai
发明人： Mitsuya Hosoe , Izuru Kanoya , Terumi Furuta , Hiroshi Sakai
CPC分类号： C01B3/0031 , F17C11/005 , Y02E60/321 , Y02E60/327 , Y02E60/362
摘要： A mixed powder of AlH3 and MgH2 is ball-milled in a hydrogen atmosphere while applying force of 5 G through 30 G (in which G is gravitational acceleration), and the thus-obtained milled product is dehydrogenated to produce a hydrogen storage material. The hydrogen storage material comprises an amorphous phase containing an Al—Mg alloy as a mother phase, and a crystalline Al phase having a maximum length of 100 nm or less, the crystalline Al phase being distributed as a dispersed phase in the mother phase.
摘要翻译： 将AlH3和MgH2的混合粉末在氢气气氛中球磨，同时施加5G至30G（其中G为重力加速度）的力，并将由此获得的研磨产物脱氢以产生储氢材料。 储氢材料包括含有作为母相的Al-Mg合金的非晶相和最大长度为100nm以下的结晶Al相，所述结晶Al相以分散相分布在母相中。
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公开(公告)号：US20100035104A1
公开(公告)日：2010-02-11
申请号：US12537648
申请日：2009-08-07
申请人： Mitsuya Hosoe , Terumi Furuta , Hiroshi Sakai , Izuru Kanoya
发明人： Mitsuya Hosoe , Terumi Furuta , Hiroshi Sakai , Izuru Kanoya
CPC分类号： H01M8/04216 , C01B3/0026 , H01M2250/20 , Y02E60/327 , Y02T90/32
摘要： A crystalline AlH3 is ball-milled in a hydrogen atmosphere while applying a force of 10 G to 30 G (in which G is gravitational acceleration). The milling time is more than 10 minutes and less than 60 minutes. The hydrogen storage material thus produced has a structure containing a plurality of matrix phases and a grain boundary phase disposed between the matrix phases. The matrix phases comprise Al and have a side length of 1 to 200 nm, and the grain boundary phase comprises an amorphous phase and contains hydrogen in the state of a solid solution.
摘要翻译： 将结晶AlH3在氢气气氛中球磨，同时施加10G至30G（其中G为重力加速度）的力。 研磨时间超过10分钟，少于60分钟。 这样制造的储氢材料具有包含多个基质相和配置在基体相之间的晶界相的结构。 基体相包含Al，并且具有1至200nm的边长，并且晶界相包含非晶相并且以固溶态的状态含有氢。
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公开(公告)号：US07431151B2
公开(公告)日：2008-10-07
申请号：US11226029
申请日：2005-09-14
申请人： Mitsuya Hosoe , Izuru Kanoya , Ryogo Sakamoto , Terumi Furuta , Hajime Goto
发明人： Mitsuya Hosoe , Izuru Kanoya , Ryogo Sakamoto , Terumi Furuta , Hajime Goto
CPC分类号： B82Y30/00 , F17C11/005 , Y02E60/321 , Y02E60/324 , Y10S502/526
摘要： A hydrogen storage tank comprises a hydrogen adsorbent accommodated in a pressure-resistant container. The hydrogen adsorbent is capable of adsorbing and retaining hydrogen gas of a volume exceeding an occupation volume occupied by the hydrogen adsorbent itself. As for the hydrogen adsorbent, the amount of endothermic heat, which is generated when the adsorbed hydrogen gas is released, is not more than 16 kJ per mol of hydrogen molecules. The hydrogen adsorbent is prevented from leaking outside of the pressure-resistant container by a filter.
摘要翻译： 储氢罐包括容纳在耐压容器中的氢吸附剂。 氢吸附剂能够吸附和保留体积超过氢吸附剂本身占据的占有体积的氢气。 对于氢吸附剂，吸附氢气释放时产生的吸热量不大于16kJ / mol氢分子。 通过过滤器防止氢吸附剂泄漏到耐压容器的外部。
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公开(公告)号：US08845960B2
公开(公告)日：2014-09-30
申请号：US12537648
申请日：2009-08-07
申请人： Mitsuya Hosoe , Terumi Furuta , Hiroshi Sakai , Izuru Kanoya
发明人： Mitsuya Hosoe , Terumi Furuta , Hiroshi Sakai , Izuru Kanoya
IPC分类号： C22C21/00
CPC分类号： H01M8/04216 , C01B3/0026 , H01M2250/20 , Y02E60/327 , Y02T90/32
摘要： A crystalline AlH3 is ball-milled in a hydrogen atmosphere while applying a force of 10 G to 30 G (in which G is gravitational acceleration). The milling time is more than 10 minutes and less than 60 minutes. The hydrogen storage material thus produced has a structure containing a plurality of matrix phases and a grain boundary phase disposed between the matrix phases. The matrix phases comprise Al and have a side length of 1 to 200 nm, and the grain boundary phase comprises an amorphous phase and contains hydrogen in the state of a solid solution.
摘要翻译： 将结晶AlH3在氢气气氛中球磨，同时施加10G至30G（其中G为重力加速度）的力。 研磨时间超过10分钟，少于60分钟。 这样制造的储氢材料具有包含多个基质相和配置在基体相之间的晶界相的结构。 基体相包含Al，并且具有1至200nm的边长，并且晶界相包含非晶相并且以固溶态的状态含有氢。
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公开(公告)号：US08283468B2
公开(公告)日：2012-10-09
申请号：US12879068
申请日：2010-09-10
申请人： Hiroshi Sakai , Izuru Kanoya , Terumi Furuta , Mitsuya Hosoe
发明人： Hiroshi Sakai , Izuru Kanoya , Terumi Furuta , Mitsuya Hosoe
IPC分类号： C07D213/80 , C07F1/08
CPC分类号： C07F1/005
摘要： An organometallic complex [Cu2(pyridine-3,5-dicarboxylate)2]n is provided by bonding a plurality of Cu2(pyridine-3,5-dicarboxylate)2 repeating units to each other. The organometallic complex can be obtained by the steps of dissolving copper acetate monohydrate or anhydrate and pyridine-3,5-dicarboxylic acid in a solvent, heating the solution at 50° C. to 140° C. for 24 to 168 hours to generate a reaction product, and then removing a guest molecule from the reaction product.
摘要翻译： 通过将多个Cu 2（吡啶-3,5-二羧酸酯）2重复单元彼此结合而提供有机金属络合物[Cu2（吡啶-3,5-二羧酸酯）2] n。 有机金属络合物可以通过以下步骤获得：将乙酸铜一水合物或无水物和吡啶-3,5-二羧酸溶解在溶剂中，将溶液在50℃加热至140℃24至168小时，以产生 反应产物，然后从反应产物中除去客体分子。
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