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公开(公告)号：US20180044359A1
公开(公告)日：2018-02-15
申请号：US15556808
申请日：2016-03-09
Inventor： Hiroshi Yamashita , Makiko Hatori , Michiyo Yoshinaga , Li-BIAO Han , Shigeru Shimada , Kazuhiko Sato
CPC classification number: C07F7/1896 , C07F7/025 , C07F7/18
Abstract: An object of the invention is to provide a method for efficiently producing an acyloxysilane which is useful as a functional chemical, an acyloxysilane obtained thereby, and the use thereof. The present invention provides: a method for producing an acyloxysilane, including a reaction step of reacting an alkoxysilane with a carboxylic anhydride in the presence of a catalyst, wherein the alkoxysilane is a specified alkoxysilane represented by General Formula (I), the carboxylic anhydride is a specified carboxylic acid represented by General Formula (IIA) or (IIB), the catalyst is an acid catalyst, and an acyloxysilane obtained in the reaction step is a specified acyloxysilane represented by General Formula (IIIA) or (IIIB); and the use of the acyloxysilane as a surface treatment agent or the like.
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2.发明授权公开(公告)号：US10975107B2
公开(公告)日：2021-04-13
申请号：US16490761
申请日：2018-03-01
Inventor： Kazuhiro Matsumoto , Kazuhiko Sato , Shigeru Shimada
Abstract: The purpose of the present invention is to provide a method for producing an oligosiloxane and an oligosiloxane synthesizer, by which an oligosiloxane can be efficiently produced. An oligosiloxane can be efficiently produced by the method for producing an oligosiloxane, which includes a condensation step for generating a hydrosiloxane having a structure represented by the following Formula (d) by reacting an alkoxysilane having a structure represented by the following Formula (b) with a hydrosilane having a structure represented by the following Formula (c) in the presence of a boron compound having Lewis acidity, and a hydrosilylation step for generating an alkoxysiloxane having a structure represented by the following Formula (f) by reacting the hydrosiloxane having the structure represented by Formula (d) generated in the condensation step with a carbonyl compound represented by the following Formula (E) in the presence of a boron compound having Lewis acidity. Moreover, an oligosiloxane having arbitrary substituent sequences can be produced.
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公开(公告)号：US10316046B2
公开(公告)日：2019-06-11
申请号：US15556808
申请日：2016-03-09
Inventor： Hiroshi Yamashita , Makiko Hatori , Michiyo Yoshinaga , Li-Biao Han , Shigeru Shimada , Kazuhiko Sato
Abstract: An object of the invention is to provide a method for efficiently producing an acyloxysilane which is useful as a functional chemical, an acyloxysilane obtained thereby, and the use thereof. The present invention provides: a method for producing an acyloxysilane, including a reaction step of reacting an alkoxysilane with a carboxylic anhydride in the presence of a catalyst, wherein the alkoxysilane is a specified alkoxysilane represented by General Formula (I), the carboxylic anhydride is a specified carboxylic acid represented by General Formula (IIA) or (IIB), the catalyst is an acid catalyst, and an acyloxysilane obtained in the reaction step is a specified acyloxysilane represented by General Formula (IIIA) or (IIIB); and the use of the acyloxysilane as a surface treatment agent or the like.
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公开(公告)号：US10308670B2
公开(公告)日：2019-06-04
申请号：US15116063
申请日：2015-02-03
Inventor： Masayasu Igarashi , Shigeru Shimada , Kazuhiko Sato , Tomohiro Matsumoto
IPC: C07F7/08 , B01J23/44 , B01J23/46 , C01B33/12 , C07F7/18 , B01J37/03 , B01J23/40 , B01J23/52 , B01J37/02
Abstract: The purpose of the present invention is to provide silanol compounds that can be used as raw materials of siloxane compounds and the like, and a composition of the silanol compounds, as well as to provide a production method that makes it possible to produce silanol compounds at excellent yield. A composition comprising 5 mass % to 100 mass % of a silanol compound represented by Formulas (A) to (C) can be prepared by devising to produce silanol compounds under water-free conditions, to produce silanol compounds in a solvent having the effect of suppressing the condensation of silanol compounds, and to perform other such processes, the composition being able to be used as a raw material or the like of siloxane compounds because the silanol compounds can be stably present in the resulting composition.
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公开(公告)号：US20150014669A1
公开(公告)日：2015-01-15
申请号：US14371844
申请日：2013-01-10
Applicant: Sumitomo Chemical Company, Limited , National Institute of Advanced Industrial Science and Technology
Inventor： Nobuhiko Akino , Taichi Abe , Hideo Konno , Shigeru Shimada , Kazuhiko Sato
IPC: H01L51/00
CPC classification number: H01L51/0085 , C07F15/0033 , C08K5/0091 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1059 , C09K2211/185 , H01L51/5012 , H01L51/5016 , H05B33/10
Abstract: A metal complex exhibits blue light emission of high color purity and has a color purity of small temperature dependence, particularly in the blue region. Specifically, the metal complex is represented by Formula (1a): wherein M is a metal atom; R0 is a divalent linking group; each j independently represents 0 or 1; RP1, RP2, RP3, RP4 and RP6 each independently represents a hydrogen atom or the like; RP5 represents a halogen atom or the like; m is an integer of from 1 to 3, n is an integer of from 0 to 2, and m+n is 2 or 3; and the portion represented by Formula (2): represents a bidentate ligand; wherein Rx and Ry are an atom bonding to the metal atom M, and each independently represents a carbon atom, an oxygen atom or a nitrogen atom.
Abstract translation: 金属络合物显示出高色纯度的蓝色发光，具有温度依赖性低的色纯度，特别是在蓝色区域。 具体地，金属络合物由式（1a）表示：其中M是金属原子; R 0是二价连接基团; 每个j独立地表示0或1; RP1，RP2，RP3，RP4和RP6各自独立地表示氢原子等; RP5表示卤素原子等; m为1〜3的整数，n为0〜2的整数，m + n为2或3。 和由式（2）表示的部分：表示二齿配体; 其中Rx和Ry是与金属原子M键合的原子，并且各自独立地表示碳原子，氧原子或氮原子。
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Patent Agency Ranking
公开(公告)号：US20240300984A1
公开(公告)日：2024-09-12
申请号：US18663837
申请日：2024-05-14
Inventor： Masayasu Igarashi , Kazuhiko Sato , Fujio Yagihashi , Tomohiro Matsumoto , Takeshi Nozawa , Shigeru Shimada
CPC classification number: C07F7/0836 , C07F7/21
Abstract: The present invention provides a method for producing a silanol compound capable of efficiently producing a silanol compound. The method for producing a silanol compound includes a proton exchange step of forming a silanol compound having a structure represented by following formula (c) by reacting a silicate having a structure represented by following formula (a) with an acidic compound having an acid dissociation constant pKa of −1 to 20 in dimethyl sulfoxide (DMSO).
(In formula (a), Qi+ represents an i-valent cation and i represents an integer of 1 to 4).-
公开(公告)号：US09735374B2
公开(公告)日：2017-08-15
申请号：US14371844
申请日：2013-01-10
Applicant: Sumitomo Chemical Company, Limited , National Institute of Advanced Industrial Science and Technology
Inventor： Nobuhiko Akino , Taichi Abe , Hideo Konno , Shigeru Shimada , Kazuhiko Sato
CPC classification number: H01L51/0085 , C07F15/0033 , C08K5/0091 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1059 , C09K2211/185 , H01L51/5012 , H01L51/5016 , H05B33/10
Abstract: A metal complex exhibits blue light emission of high color purity and has a color purity of small temperature dependence, particularly in the blue region. Specifically, the metal complex is represented by Formula (1a): wherein M is a metal atom; R0 is a divalent linking group; each j independently represents 0 or 1; RP1, RP2, RP3, RP4 and RP6 each independently represents a hydrogen atom or the like; RP5 represents a halogen atom or the like; m is an integer of from 1 to 3, n is an integer of from 0 to 2, and m+n is 2 or 3; and the portion represented by Formula (2): represents a bidentate ligand; wherein Rx and Ry are an atom bonding to the metal atom M, and each independently represents a carbon atom, an oxygen atom or a nitrogen atom.
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公开(公告)号：US09705097B2
公开(公告)日：2017-07-11
申请号：US14372033
申请日：2013-01-10
Applicant: Sumitomo Chemical Company, Limited , National Institute of Advanced Industrial Science and Technology
Inventor： Nobuhiko Akino , Taichi Abe , Hideo Konno , Shigeru Shimada , Kazuhiko Sato
IPC: H01L51/54 , C09K11/06 , H01L51/00 , C07F15/00 , C07F7/08 , C08K5/00 , H05B33/10 , H01L51/50 , C08K5/56 , H01L51/52
CPC classification number: H01L51/0085 , C07F7/0805 , C07F15/0033 , C08K5/0091 , C08K5/56 , C09K11/06 , C09K2211/1007 , C09K2211/1059 , C09K2211/185 , H01L51/5012 , H01L51/5016 , H01L51/5203 , H05B33/10
Abstract: A highly stable metal complex useful for the manufacture of a light-emitting device has an excellent lifetime property, particularly in a blue region, specifically a metal complex represented by Formula (1): wherein M is a metal atom; each R0 independently represents a divalent linking group; i and j each independently represent 0 or 1; RP1, RP2, RP3, RP4, RP5 and RP6 each independently represent a hydrogen atom and the like, with a proviso that at least one of RP1, RP2, RP3, RP4, RP5 and RP6 is a dendron; m is an integer of from 1 to 3, n is an integer of from 0 to 2, and m+n is 2 or 3; and the portion represented by Formula (2): represents a bidentate ligand; wherein Rx and Ry are an atom bonding to the metal atom M, and each independently represents a carbon atom and the like.
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公开(公告)号：US12024532B2
公开(公告)日：2024-07-02
申请号：US17472421
申请日：2021-09-10
Inventor： Masayasu Igarashi , Kazuhiko Sato , Fujio Yagihashi , Tomohiro Matsumoto , Takeshi Nozawa , Shigeru Shimada
CPC classification number: C07F7/0836 , C07F7/21
Abstract: The present invention provides a method for producing a silanol compound capable of efficiently producing a silanol compound. The method for producing a silanol compound includes a proton exchange step of forming a silanol compound having a structure represented by following formula (c) by reacting a silicate having a structure represented by following formula (a) with an acidic compound having an acid dissociation constant pKa of −1 to 20 in dimethyl sulfoxide (DMSO).
(In formula (a), Qi+ represents an i-valent cation and i represents an integer of 1 to 4).-
公开(公告)号：US20170183363A1
公开(公告)日：2017-06-29
申请号：US15116063
申请日：2015-02-03
Inventor： Masayasu Igarashi , Shigeru Shimada , Kazuhiko Sato , Tomohiro Matsumoto
CPC classification number: C07F7/0836 , B01J23/40 , B01J23/44 , B01J23/462 , B01J23/464 , B01J23/52 , B01J37/0201 , B01J37/03 , C01B33/12 , C07F7/0874 , C07F7/1892
Abstract: The purpose of the present invention is to provide silanol compounds that can be used as raw materials of siloxane compounds and the like, and a composition of the silanol compounds, as well as to provide a production method that makes it possible to produce silanol compounds at excellent yield. A composition comprising 5 mass % to 100 mass % of a silanol compound represented by Formulas (A) to (C) can be prepared by devising to produce silanol compounds under water-free conditions, to produce silanol compounds in a solvent having the effect of suppressing the condensation of silanol compounds, and to perform other such processes, the composition being able to be used as a raw material or the like of siloxane compounds because the silanol compounds can be stably present in the resulting composition.
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