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公开(公告)号:US20190259918A1
公开(公告)日:2019-08-22
申请号:US16342390
申请日:2017-10-20
Applicant: NGK SPARK PLUG CO., LTD.
Inventor: Shohei TAKAKU , Yusuke KATSU , Tsuneyuki ITO , Yuki SHIMURA , Takeshi MITSUOKA , Jun MOTEKI
Abstract: An optical wavelength conversion member and a light-emitting device including the optical wavelength conversion member. The optical wavelength conversion member (9) is formed of a ceramic sintered body having a fluorescent phase containing fluorescent crystal grains as a main component and a translucent phase containing translucent crystal grains as a main component. Crystal grains of the fluorescent phase have a composition represented by formula A3B5O12:Ce, where the element A is selected from Sc, Y, and lanthanoids (except for Ce), and the element B is selected from Al and Ga. In the optical wavelength conversion member (9), 0.3
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公开(公告)号:US20190245119A1
公开(公告)日:2019-08-08
申请号:US16343188
申请日:2017-10-24
Applicant: NGK SPARK PLUG CO., LTD.
Inventor: Yusuke KATSU , Shohei TAKAKU , Tsuneyuki ITO , Takeshi MITSUOKA , Jun MOTEKI
IPC: H01L33/50 , H01L33/48 , B32B7/027 , B32B15/04 , C09K11/77 , C09K11/02 , C04B35/117 , C04B35/44 , C04B35/645
CPC classification number: H01L33/502 , B32B7/027 , B32B15/04 , B32B2307/302 , C04B35/117 , C04B35/44 , C04B35/50 , C04B35/645 , C04B2235/3217 , C04B2235/3222 , C04B2235/6585 , C09K11/02 , C09K11/08 , C09K11/7774 , G02B5/20 , H01L33/483 , H01L33/50 , H01L33/505 , H01L2933/0041
Abstract: A method for producing an optical wavelength conversion member (9) composed of a sintered body containing, as main components, Al2O3 and a component represented by formula A3B5O12:Ce; an optical wavelength conversion member; an optical wavelength conversion component including the optical wavelength conversion member; and a light-emitting device including the optical wavelength conversion member or the optical wavelength conversion component. The production method of the sintered body includes firing in a firing atmosphere having a pressure of 104 Pa or more and an oxygen concentration of 0.8 vol. % or more and less than 25 vol. %.
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公开(公告)号:US20190233333A1
公开(公告)日:2019-08-01
申请号:US16312362
申请日:2017-06-19
Applicant: NGK SPARK PLUG CO., LTD.
Inventor: Jun MOTEKI , Yusuke KATSU , Takeshi MITSUOKA
IPC: C04B35/117
Abstract: The durability of a ceramic sintered body is improved, and a reduction in its light emission intensity and the occurrence of a chromaticity variation are suppressed. The ceramic sintered body contains alumina and a compound represented by M13-XM2XM35O12. The volume percent of the compound in the ceramic sintered body is from 3% to 70% inclusive. The ratio of the intensity of XRD from a complex oxide of aluminum and M2 to the intensity of XRD from the compound in the ceramic sintered body is less than 0.05. The average grain diameter of the alumina contained in the ceramic sintered body is from 0.30 (μm) to 3.00 (μm) inclusive. M1 is at least one selected from Sc, Y, and lanthanoid elements, and M2 is at least one selected from lanthanoid elements except any lanthanoid element selected for M1. M3 is at least one of Al and Ga, and X is from 0.003 to 0.500 inclusive.
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公开(公告)号:US20190198726A1
公开(公告)日:2019-06-27
申请号:US16328161
申请日:2017-10-18
Applicant: NGK SPARK PLUG CO., LTD.
Inventor: Jun MOTEKI , Shohei TAKAKU , Yusuke KATSU , Takeshi MITSUOKA , Tsuneyuki ITO
IPC: H01L33/50 , H01L33/16 , C04B35/44 , C04B35/115 , C04B35/117 , C09K11/77
Abstract: An optical wavelength conversion member including a polycrystalline ceramic sintered body containing, as main components, Al2O3 crystal grains and crystal grains of a component represented by formula A3B5O12:Ce, wherein A is at least one element selected from Sc, Y and lanthanoids (except for Ce), and B is at least one element selected from Al and Ga. Further, the following relations are satisfied: 0%≤X≤25%, 9%≤Y≤45%, and 48%≤Z≤90%, wherein X represents a proportion corresponding to the ratio a/N, Y represents a proportion corresponding to the ratio b/N, and Z represents a proportion corresponding to the ratio c/N and a, b, c and N are as defined herein. Also disclosed is a light-emitting device including the optical wavelength conversion member.
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公开(公告)号:US20190245118A1
公开(公告)日:2019-08-08
申请号:US16342621
申请日:2017-10-20
Applicant: NGK SPARK PLUG CO., LTD.
Inventor: Jun MOTEKI , Shohei TAKAKU , Yusuke KATSU , Takeshi MITSUOKA , Tsuneyuki ITO
CPC classification number: H01L33/502 , C04B35/50 , C04B2235/3222 , C09K11/08 , G02B5/20 , H01L33/50
Abstract: An optical wavelength conversion member and a light-emitting device including the optical wavelength conversion member. The light-emitting device (1) includes a container (3), a light-emitting element (5), and an optical wavelength conversion member (9). The optical wavelength conversion member (9) is composed of a polycrystalline ceramic sintered body containing, as main components, Al2O3 crystal grains and crystal grains of a component represented by formula A3B5O12:Ce. Specifically, A and B of the A3B5O12 individually represent at least one element selected from the following element groups: A: Sc, Y, and lanthanoids (except for Ce), and B: Al and Ga; the at least one element selected from the element groups is present in each crystal grain and the crystal grain boundary of the ceramic sintered body; and the element concentration of the crystal grain boundary is higher than the element concentration of the crystal grain.
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公开(公告)号:US20160023952A1
公开(公告)日:2016-01-28
申请号:US14419511
申请日:2013-12-27
Applicant: NGK SPARK PLUG CO., LTD.
Inventor: Jun MOTEKI , Yusuke KATSU , Takeshi MITSUOKA
IPC: C04B35/10
CPC classification number: C04B35/10 , C04B35/117 , C04B35/119 , C04B35/5626 , C04B35/62685 , C04B35/645 , C04B2235/3206 , C04B2235/3208 , C04B2235/3217 , C04B2235/3224 , C04B2235/3225 , C04B2235/3241 , C04B2235/3244 , C04B2235/3251 , C04B2235/3272 , C04B2235/3839 , C04B2235/3843 , C04B2235/3847 , C04B2235/5436 , C04B2235/5445 , C04B2235/80 , C04B2235/85 , C04B2235/96 , C04B2235/9607
Abstract: In a ceramic composition mainly composed of alumina (Al2O3), tungsten carbide (WC) and zirconia (ZrO2), zirconium (Zr) is distributed in a first grain boundary as an interface where an alumina (Al2O3) crystal grain is adjacent to a tungsten carbide (WC) crystal grain and in a second grain boundary as an interface where two alumina (Al2O3) crystal grains are adjacent to each other.
Abstract translation: 在主要由氧化铝(Al 2 O 3),碳化钨(WC)和氧化锆(ZrO 2)组成的陶瓷组合物中,锆(Zr)分布在作为界面的第一晶界中,其中氧化铝(Al 2 O 3)晶粒与钨 碳化物(WC)晶粒和作为其中两个氧化铝(Al 2 O 3)晶粒彼此相邻的界面的第二晶界。
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