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    Cross-coupling reaction catalyst
    2.
    发明授权
    Cross-coupling reaction catalyst 有权

    公开(公告)号：US12017208B2

    公开(公告)日：2024-06-25

    申请号：US17269093

    申请日：2019-08-28

    Applicant: N.E. CHEMCAT CORPORATION ,  NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY

    Inventor： Tomoteru Mizusaki ,  Yukio Takagi ,  Junchul Choi ,  Norihisa Fukaya ,  Kazuhiro Matsumoto

    IPC: B01J31/22 ,  C07C209/10

    CPC classification number: B01J31/22 ,  C07C209/10 ,  B01J2531/824

    Abstract: It is an object of the present invention to provide a catalyst for a cross-coupling reaction in which an organometallic complex is sufficiently immobilized on a carrier and an object product can be easily obtained in a high yield and in a relatively short reaction time with a relatively small amount of use. The catalyst for a cross-coupling reaction of the present invention has a carrier part composed of a synthetic resin and an organometallic complex part immobilized on the carrier part by chemical bonding, and has a structure represented by formula (P1), wherein in (P1) R1, R2 may be the same or different, and is a substituent such as a hydrogen atom. R3, R4, R5, R6, R8, R9 may be the same or different and are substituents, such as a hydrogen. X represents a halogen atom, and R7 represents a substituent having 3 to 20 carbon atoms with a π bond. RS1 represents the main chain of the synthetic resin precursors having —CH2OH group at their end.

    ORGANOMETALLIC COMPLEX CATALYST
    3.
    发明申请
    ORGANOMETALLIC COMPLEX CATALYST 审中-公开

    公开(公告)号：US20190308182A1

    公开(公告)日：2019-10-10

    申请号：US16466436

    申请日：2017-12-06

    Applicant: NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY ,  N.E. CHEMCAT CORPORATION

    Inventor： Junchul Choi ,  Norihisa Fukaya ,  Shunya Onozawa ,  Kazuhiko Sato ,  Hiroyuki Yasuda ,  Tomoteru Mizusaki ,  Yukio Takagi

    IPC: B01J31/22

    Abstract: An organometallic complex catalyst is disclosed for use in a cross-coupling reaction. In formula (1), M is the coordination center and represents a metal atom such as Pd or an ion thereof. R1, R2, and R3 may be the same or different and are a substituent such as a hydrogen atom. R4, R5, R6, and R7 may be the same or different and are a substituent such as a hydrogen atom. X represents a halogen atom. R8 represents a substituent that has a π bond and 3-20 carbon atoms. With regard to the electron-donating properties of R1-R7 with respect to the coordination center M of the ligand containing R1-R7 that is indicated in formula (2), R1-R7 are arranged in combination such that the TEP value obtained from infrared spectroscopy shifts toward the high frequency side compared to the TEP value of the ligand of formula (2-1).

    ORGANOMETALLIC COMPLEX CATALYST
    5.
    发明申请
    ORGANOMETALLIC COMPLEX CATALYST 有权

    公开(公告)号：US20220032278A1

    公开(公告)日：2022-02-03

    申请号：US17490143

    申请日：2021-09-30

    Applicant: NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY ,  N.E. CHEMCAT CORPORATION

    Inventor： Junchul Choi ,  Norihisa Fukaya ,  Shunya Onozawa ,  Kazuhiko Sato ,  Hiroyuki Yasuda ,  Tomoteru Mizusaki ,  Yukio Takagi

    IPC: B01J31/22

    Abstract: An organometallic complex catalyst that makes it possible to obtain a higher yield of a desired product than conventional catalysts in a cross-coupling reaction. The organometallic complex catalyst has a structure represented by formula (1) and is for use in a cross-coupling reaction. In formula (1), M is the coordination center and represents a metal atom such as Pd or an ion thereof. R1, R2, and R3 may be the same or different and are a substituent such as a hydrogen atom. R4, R5, R6, and R7 may be the same or different and are a substituent such as a hydrogen atom. X represents a halogen atom. R8 represents a substituent that has a π bond and 3-20 carbon atoms. With regard to the electron-donating properties of R1-R7 with respect to the coordination center M of the ligand containing R1-R7 that is indicated in formula (2), R1-R7 are arranged in combination such that the TEP value obtained from infrared spectroscopy shifts toward the low frequency side compared to the TEP value of the ligand of formula (2-1).

    Organometallic complex catalyst
    6.
    发明授权
    Organometallic complex catalyst 有权

    公开(公告)号：US11167278B2

    公开(公告)日：2021-11-09

    申请号：US16466413

    申请日：2017-12-06

    Applicant: NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY ,  N.E. CHEMCAT CORPORATION

    Inventor： Junchul Choi ,  Norihisa Fukaya ,  Shunya Onozawa ,  Kazuhiko Sato ,  Hiroyuki Yasuda ,  Tomoteru Mizusaki ,  Yukio Takagi

    IPC: B01J31/22

    Abstract: An organometallic complex catalyst that makes it possible to obtain a higher yield of a desired product than conventional catalysts in a cross-coupling reaction. The organometallic complex catalyst has a structure represented by formula (1) and is for use in a cross-coupling reaction. In formula (1), M is the coordination center and represents a metal atom such as Pd or an ion thereof. R1, R2, and R3 may be the same or different and are a substituent such as a hydrogen atom. R4, R5, R6, and R7 may be the same or different and are a substituent such as a hydrogen atom. X represents a halogen atom. R8 represents a substituent that has a π bond and 3-20 carbon atoms. With regard to the electron-donating properties of R1-R7 with respect to the coordination center M of the ligand containing R1-R7 that is indicated in formula (2), R1-R7 are arranged in combination such that the TEP value obtained from infrared spectroscopy shifts toward the low frequency side compared to the TEP value of the ligand of formula (2-1).

    CROSS-COUPLING REACTION CATALYST
    7.
    发明申请
    CROSS-COUPLING REACTION CATALYST 有权

    公开(公告)号：US20210308660A1

    公开(公告)日：2021-10-07

    申请号：US17269093

    申请日：2019-08-28

    Applicant: N.E. CHEMCAT CORPORATION ,  NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY

    Inventor： Tomoteru Mizusaki ,  Yukio Takagi ,  Junchul Choi ,  Norihisa Fukaya ,  Kazuhiro Matsumoto

    IPC: B01J31/22 ,  C07C209/10

    Abstract: It is an object of the present invention to provide a catalyst for a cross-coupling reaction in which an organometallic complex is sufficiently immobilized on a carrier and an object product can be easily obtained. The catalyst for a cross-coupling reaction of the present invention has a carrier part composed of a synthetic resin and an organometallic complex part immobilized on the carrier part by chemical bonding, and has a structure represented by formula (P1), wherein in (P1) R1, R2 may be the same or different, and is a substituent such as a hydrogen atom. R3, R4, R5, R6, R8, R9 may be the same or different and are substituents, such as a hydrogen. X represents a halogen atom, and R7 represents a substituent having 3 to 20 carbon atoms with a π bond. RS1 represents the main chain of the synthetic resin precursors having —CH2OH group at their end.

    Organometallic complex catalyst
    9.
    发明授权
    Organometallic complex catalyst 有权

    公开(公告)号：US11161103B2

    公开(公告)日：2021-11-02

    申请号：US16466436

    申请日：2017-12-06

    Applicant: NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY ,  N.E. CHEMCAT CORPORATION

    Inventor： Junchul Choi ,  Norihisa Fukaya ,  Shunya Onozawa ,  Kazuhiko Sato ,  Hiroyuki Yasuda ,  Tomoteru Mizusaki ,  Yukio Takagi

    IPC: B01J31/22

    Abstract: An organometallic complex catalyst is disclosed for use in a cross-coupling reaction. In formula (1), M is the coordination center and represents a metal atom such as Pd or an ion thereof. R1, R2, and R3 may be the same or different and are a substituent such as a hydrogen atom. R4, R5, R6, and R7 may be the same or different and are a substituent such as a hydrogen atom. X represents a halogen atom. R8 represents a substituent that has a π bond and 3-20 carbon atoms. With regard to the electron-donating properties of R1-R7 with respect to the coordination center M of the ligand containing R1-R7 that is indicated in formula (2), R1-R7 are arranged in combination such that the TEP value obtained from infrared spectroscopy shifts toward the high frequency side compared to the TEP value of the ligand of formula (2-1).

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