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    Optochemical sensor and method of making the same
    1.
    发明授权
    Optochemical sensor and method of making the same 有权
    光化学传感器及其制作方法

    公开(公告)号：US07556774B2

    公开(公告)日：2009-07-07

    申请号：US11275268

    申请日：2005-12-21

    申请人： Neal A. Rakow ,  Michael S. Wendland ,  Michael C. Palazzotto ,  Dora M. Paolucci ,  Richard J. Poirier ,  Stefan H. Gryska ,  John E. Trend ,  Moses M. David

    发明人： Neal A. Rakow ,  Michael S. Wendland ,  Michael C. Palazzotto ,  Dora M. Paolucci ,  Richard J. Poirier ,  Stefan H. Gryska ,  John E. Trend ,  Moses M. David

    IPC分类号： G01N21/00

    CPC分类号： G01N21/783 ,  G01N2021/7779

    摘要： A method of making an optochemical sensor, the method comprising: providing a reflective substrate having a major surface; affixing a detection layer comprising at least one intrinsically microporous polymer to at least a portion of the major surface; depositing a substantially continuous semi-reflective metallic layer on at least a portion of the detection layer, the semi-reflective metallic layer comprising palladium and having a network of fine irregular cracks therein; and heating the detection layer and semi-reflective metallic layer in the presence of molecular oxygen at a temperature sufficient to cause the cracks to widen. Sensors prepared according to method are also disclosed.

    摘要翻译： 一种制造光化学传感器的方法，所述方法包括：提供具有主表面的反射基板; 将包含至少一个本征微孔聚合物的检测层固定在所述主表面的至少一部分上; 在所述检测层的至少一部分上沉积基本上连续的半反射金属层，所述半反射金属层包含钯并且具有细小的不规则裂纹的网络; 并在分子氧存在下，在足以引起裂纹扩大的温度下加热检测层和半反射金属层。 还公开了根据方法制备的传感器。

    Organic vapor sorbent protective device with thin-film indicator
    4.
    发明授权
    Organic vapor sorbent protective device with thin-film indicator 有权
    有机蒸汽吸附剂保护装置，带薄膜指示剂

    公开(公告)号：US08067110B2

    公开(公告)日：2011-11-29

    申请号：US11530614

    申请日：2006-09-11

    申请人： Neal A. Rakow ,  James P. Mathers ,  Jun-Ying Zhang ,  Dora M. Paolucci ,  Richard J. Poirier ,  Moses M. David ,  John E. Trend ,  Michael S. Wendland

    发明人： Neal A. Rakow ,  James P. Mathers ,  Jun-Ying Zhang ,  Dora M. Paolucci ,  Richard J. Poirier ,  Moses M. David ,  John E. Trend ,  Michael S. Wendland

    IPC分类号： A61L2/28 ,  A61M16/00

    CPC分类号： G01N21/783 ,  G01N21/8422

    摘要： A sorbent media protective device includes an enclosure having a gas inlet, gas outlet and a thin-film multilayer indicator. The thin-film multilayer indicator is proximate sorbent media that can sorb a vapor of interest flowing from the gas inlet towards the gas outlet. The indicator includes a porous detection layer whose optical thickness changes in the presence of the vapor, located between a semireflective layer and a reflective layer permeable to the vapor. With equilibration at the applied vapor concentration between at least a portion of the media and the vapor, the vapor can pass through the reflective layer into the detection layer and change the detection layer optical thickness sufficiently to cause a visibly discernible change in the indicator appearance if viewed through the semireflective layer.

    摘要翻译： 吸附剂介质保护装置包括具有气体入口，气体出口和薄膜多层指示器的外壳。 薄膜多层指示器是吸附剂介质，其可吸附从气体入口流向气体出口的感兴趣的蒸气。 指示剂包括多孔检测层，其光学厚度在存在蒸气的情况下变化，位于半反射层和可透过蒸汽的反射层之间。 在介质的至少一部分与蒸气之间的应用蒸汽浓度下平衡，蒸汽可以穿过反射层进入检测层，并且将检测层的光学厚度充分改变以引起指示器外观中明显的可辨别的变化，如果 通过半反射层观察。

    Organic Vapor Sorbent Protective Device With Thin-Film Indicator
    6.
    发明申请
    Organic Vapor Sorbent Protective Device With Thin-Film Indicator 有权
    有机蒸汽吸附剂保护装置，带薄膜指示器

    公开(公告)号：US20080063575A1

    公开(公告)日：2008-03-13

    申请号：US11530614

    申请日：2006-09-11

    申请人： Neal A. Rakow ,  James P. Mathers ,  Jun-Ying Zhang ,  Dora M. Paolucci ,  Richard J. Poirier ,  Moses M. David ,  John E. Trend ,  Michael S. Wendland

    发明人： Neal A. Rakow ,  James P. Mathers ,  Jun-Ying Zhang ,  Dora M. Paolucci ,  Richard J. Poirier ,  Moses M. David ,  John E. Trend ,  Michael S. Wendland

    IPC分类号： G01N31/22

    CPC分类号： G01N21/783 ,  G01N21/8422

    摘要： A sorbent media protective device includes an enclosure having a gas inlet, gas outlet and a thin-film multilayer indicator. The thin-film multilayer indicator is proximate sorbent media that can sorb a vapor of interest flowing from the gas inlet towards the gas outlet. The indicator includes a porous detection layer whose optical thickness changes in the presence of the vapor, located between a semireflective layer and a reflective layer permeable to the vapor. With equilibration at the applied vapor concentration between at least a portion of the media and the vapor, the vapor can pass through the reflective layer into the detection layer and change the detection layer optical thickness sufficiently to cause a visibly discernible change in the indicator appearance if viewed through the semireflective layer.

    摘要翻译： 吸附剂介质保护装置包括具有气体入口，气体出口和薄膜多层指示器的外壳。 薄膜多层指示器是吸附剂介质，其可吸附从气体入口流向气体出口的感兴趣的蒸气。 指示剂包括多孔检测层，其光学厚度在存在蒸气的情况下变化，位于半反射层和可透过蒸汽的反射层之间。 在介质的至少一部分与蒸气之间的应用蒸汽浓度下平衡，蒸汽可以穿过反射层进入检测层，并且将检测层的光学厚度充分改变以引起指示器外观中明显的可辨别的变化，如果 通过半反射层观察。

    Plasma deposited microporous analyte detection layer
    8.
    发明授权
    Plasma deposited microporous analyte detection layer 有权
    等离子体沉积微孔分析物检测层

    公开(公告)号：US08293340B2

    公开(公告)日：2012-10-23

    申请号：US11275277

    申请日：2005-12-21

    申请人： Moses M. David ,  Neal A. Rakow ,  Dora M. Paolucci ,  John E. Trend

    发明人： Moses M. David ,  Neal A. Rakow ,  Dora M. Paolucci ,  John E. Trend

    IPC分类号： H05H1/24 ,  G01N21/00

    CPC分类号： G01N21/78 ,  G01N21/783 ,  G01N2021/7723 ,  G01N2021/7726 ,  G01N2021/7793

    摘要： Plasma deposited microporous analyte detection layers, method of forming analyte detection layers, and analyte sensors including the same are disclosed. An analyte sensor includes a substrate and a microporous amorphous random covalent network layer. The microporous amorphous random covalent network layer includes silicon, carbon, hydrogen and oxygen with a mean pore size in a range from 0.5 to 10 nanometers and an optical thickness in a range from 0.2 to 2 micrometers.

    摘要翻译： 公开了等离子体沉积的微孔分析物检测层，形成分析物检测层的方法和包括其的分析物传感器。 分析物传感器包括基底和微孔非晶态随机共价网络层。 微孔无定形无规共价网络层包括硅，碳，氢和氧，平均孔径在0.5至10纳米的范围内，光学厚度在0.2至2微米的范围内。

    Organic chemical sensor comprising plasma-deposited microporous layer, and method of making and using
    10.
    发明授权
    Organic chemical sensor comprising plasma-deposited microporous layer, and method of making and using 有权
    含有等离子体沉积微孔层的有机化学传感器及其制造和使用方法

    公开(公告)号：US08378694B2

    公开(公告)日：2013-02-19

    申请号：US12681758

    申请日：2008-09-30

    申请人： Moses M. David ,  Stefan H. Gryska ,  Nelson B. O'Bryan ,  Neal A. Rakow ,  Michael S. Wendland

    发明人： Moses M. David ,  Stefan H. Gryska ,  Nelson B. O'Bryan ,  Neal A. Rakow ,  Michael S. Wendland

    IPC分类号： G01R27/26

    CPC分类号： G01N27/125 ,  Y10T442/624

    摘要： Applicant discloses a sensing element for sensing an organic chemical analyte, comprising a first electrode and a second electrode, and a microporous, hydrophobic, analyte-responsive dielectric material disposed at least in proximity to the first and second electrodes. The analyte-responsive dielectric material may be an amorphous random covalent network comprising a mean pore size of less than about 10 nm and a porosity of at least about 20%. An electrical property of the sensing element, such as capacitance, can be monitored in order to sense an organic chemical analyte.

    摘要翻译： 申请人公开了用于感测有机化学分析物的感测元件，其包括第一电极和第二电极以及至少设置在第一和第二电极附近的微孔，疏水的分析物响应介电材料。 分析物响应介电材料可以是包含小于约10nm的平均孔径和至少约20％的孔隙率的无定形无规共价网络。 可以监测感测元件的电性质，例如电容，以感测有机化学分析物。