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公开(公告)号：US07692007B2
公开(公告)日：2010-04-06
申请号：US11632313
申请日：2005-06-17
IPC分类号： C07D239/00 , C07D233/00 , C07D211/92 , C07F5/02
CPC分类号： C07D233/54 , C07D213/06
摘要： The invention relates to a process for the preparation of onium salts having a low chloride content by reaction of an onium chloride with an acid, where the hydrochloric acid forming is removed by azeotropic distillation by coordination to an organic solvent which forms an azeotropic mixture with water.
摘要翻译： 本发明涉及通过氯化铟与酸的反应制备氯化物含量低的鎓盐的方法，其中通过与与水形成共沸混合物的有机溶剂的共沸蒸馏除去形成的盐酸， 。
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公开(公告)号：US20080027230A1
公开(公告)日：2008-01-31
申请号：US11632313
申请日：2005-06-17
IPC分类号： C07D211/04 , C07C211/03 , C07D233/54 , C07F9/28
CPC分类号： C07D233/54 , C07D213/06
摘要： The invention relates to a process for the preparation of onium salts having a low chloride content by reaction of an onium chloride with an acid, where the hydrochloric acid forming is removed by azeotropic distillation by coordination to an organic solvent which forms an azeotropic mixture with water.
摘要翻译： 本发明涉及通过氯化铟与酸的反应制备氯化物含量低的鎓盐的方法，其中通过与与水形成共沸混合物的有机溶剂的共沸蒸馏除去形成的盐酸， 。
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3.发明授权Process for the preparation of organic salts containing bis(perfluoroalkyl) phosphinate anions 失效制备含有双（全氟烷基）次膦酸根阴离子的有机盐的方法公开(公告)号：US07576242B2
公开(公告)日：2009-08-18
申请号：US10579555
申请日：2004-10-26
IPC分类号： C07F9/02
摘要： The invention relates to a method for the production of organic salts containing bis(perfluoroalkyl)phosphinate anions. According to said method, a tris(perfluoroalkyl)phosphine oxide is reacted with an alcohol and an organic base, which is stronger than the alcohol. The invention also relates to the salts which are produced according to said method and to the use thereof as ionic liquids.
摘要翻译： 本发明涉及一种生产含有双（全氟烷基）次膦酸根阴离子的有机盐的方法。 根据所述方法，三（全氟烷基）氧化膦与醇和有机碱反应，其比醇强。 本发明还涉及根据所述方法制备的盐及其作为离子液体的用途。
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公开(公告)号：US08436199B2
公开(公告)日：2013-05-07
申请号：US12625648
申请日：2009-11-25
IPC分类号： C07F5/02
CPC分类号： C07F15/008 , C07F5/027 , C07F17/00
摘要： The invention relates to boron-containing acids of the general formula (I) [B(RF)4-x-y(CN)xFy]−H+ (I), where x=0, 1, 2, 3 or 4, y=0, 1, 2 or 3 x+y≦4, and in which the ligands RF may be identical or different and RF stands for a perfluorinated or partially fluorinated C1-12-alkyl group and where the CN group is bonded to the B atom via the C atom, and complexes thereof with a solvent, to salts comprising a cation and the anion of a selection of the acids according to the invention, and to processes for the preparation of the salts.
摘要翻译： 本发明涉及通式（I）[B（RF）4-xy（CN）x F y] -H +（I）的含硼酸，其中x = 0,1,2,3或4，y = 0 ，1,2或3个x + y @ 4，并且其中配体RF可以相同或不同，RF代表全氟化或部分氟化的C1-12烷基，其中CN基团通过 C原子及其与溶剂的络合物，以及包含阳离子和根据本发明的酸选择阴离子的盐，以及盐的制备方法。
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5.发明授权公开(公告)号：US07939644B2
公开(公告)日：2011-05-10
申请号：US10568526
申请日：2004-07-22
申请人： Nikolai (Mykola) Ignatyev , Urs Welz-Biermann , Helge Willner , Maik Finze , Eduard Bernhardt , Andriy Kucheryna
发明人： Nikolai (Mykola) Ignatyev , Urs Welz-Biermann , Helge Willner , Maik Finze , Eduard Bernhardt , Andriy Kucheryna
IPC分类号： C09B23/00 , C09B23/04 , C09B23/06 , C09B23/08 , C09B23/16 , C09B44/10 , C09B44/14 , C09B44/16 , C09B44/18 , C09B44/20
CPC分类号： C07D241/46 , C07D263/54 , C07D277/62 , C09B23/06 , C09B67/0083 , C09B69/06
摘要： The present invention relates to dyes of the general formula CAT+ Y− (I), where Y− is an anion selected from the group of the cyanoborates, fluoroalkylphosphates, fluoroalkylborates or imidates and CAT+ is a cation selected from the group of the azine, xanthene, polymethine, styryl, azo, tetrazolium, pyrylium, benzopyrylium, thiopyrylium, benzothiopyrylium, thiazine, oxazine, triarylmethane, diarylmethane, methine, acridine, quinoline, isoquinoline or quaternary azafluorenone dyes, for colouring plastics and plastic fibres, for the preparation of flexographic printing inks, as ball-point pen pastes, as stamp ink, for colouring leather and paper, for use in data acquisition systems, reprography, in ink microfilters, in photogalvanics, laser technology and the photo industry.
摘要翻译： 本发明涉及通式CAT + Y-（I）的染料，其中Y-是选自氰基硼酸盐，氟烷基磷酸盐，氟烷基硼酸盐或亚胺酸盐的阴离子，CAT +是选自吖嗪，呫吨 ，聚甲炔，苯乙烯基，偶氮，四唑鎓，吡喃鎓，苯并吡喃鎓，硫代吡喃鎓，苯并硫代吡喃鎓，噻嗪，恶嗪，三芳基甲烷，二芳基甲烷，次甲基，吖啶，喹啉，异喹啉或季氮芴酮染料，用于着色塑料和塑料纤维，用于制备柔性版印刷 油墨，作为圆珠笔，作为印花油墨，用于着色皮革和纸张，用于数据采集系统，复印，墨水微滤器，光电镀，激光技术和照相行业。
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6.发明申请PROCESS FOR THE PREPARATION OF ONIUM SALTS WITH DIALKYLPHOSPHATE, DIALKYLPHOSPHINATE OR (O-ALKYL)ALKYL- OR ALKYLPHOSPHONATE ANIONS HAVING A LOW HALIDE CONTENT 审中-公开用二烷基磷酸盐，二烷基磷酸盐或（O-烷基）烷基 - 或烷基膦酸盐阴离子制备低盐含量的方法公开(公告)号：US20090253914A1
公开(公告)日：2009-10-08
申请号：US11721615
申请日：2005-11-18
IPC分类号： C07D213/20 , C07D233/58 , C07F9/09 , C07C211/13
CPC分类号： C07D213/20 , C07D233/54 , C07F9/11 , C07F9/301 , C07F9/409
摘要： The invention relates to a process for the preparation of onium salts with dialkylphosphate, dialkylphosphinate or (O-alkyl)alkyl- or alkylphosphonate anions by reaction of an onium halide with a triallyl phosphate, alkyl dialkylphosphinate, dialkyl alkylphosphonate or trialkylsilyl ester or mixed alkyl trialkylsilyl ester of phosphoric, dialkylphosphinic or alkylphosphonic acid.
摘要翻译： 本发明涉及通过卤化鎓与磷酸三烯丙酯，烷基二烷基次膦酸盐，烷基膦酸二烷基酯或三烷基甲硅烷基酯或混合的烷基三烷基甲硅烷基酯的混合物制备与磷酸二烷基酯，二烷基次膦酸盐或（O-烷基）烷基 - 或烷基膦酸盐阴离子的鎓盐的方法 磷酸，二烷基次膦酸或烷基膦酸的酯。
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7.发明授权Process for the preparation of mono- and bis(fluoroalkyl)phosphoranes and the corresponding acids and phosphates 失效单和双（氟烷基）磷烷及相应的酸和磷酸盐的制备方法公开(公告)号：US07541488B2
公开(公告)日：2009-06-02
申请号：US10579556
申请日：2004-10-22
申请人： Nikolai (Mykola) Ignatyev , Urs Welz-Biermann , Michael Schmidt , Andriy Kucheryna , Helge Willner
发明人： Nikolai (Mykola) Ignatyev , Urs Welz-Biermann , Michael Schmidt , Andriy Kucheryna , Helge Willner
IPC分类号： C07F9/22
CPC分类号： C07F9/535
摘要： The invention relates to a method for producing mono(fluoroalkyl)phosphoric acids or bis(fluoroalkyl)phosphoric acids, mono(fluoroalkyl)phosphates or bis(fluoroalkyl)phosphates, and the corresponding phosphoranes thereof. The inventive method comprises at least the step of reacting a bis(fluoroalkyl)phosphonic acid, a (fluoroalkyl)phosphonic acid, or a corresponding derivative of said acids with anhydrous hydrogen fluoride.
摘要翻译： 本发明涉及一种（氟代烷基）磷酸或双（氟代烷基）磷酸，单（氟烷基）磷酸酯或双（氟烷基）磷酸酯及其相应的磷烷的制备方法。 本发明的方法至少包括使双（氟烷基）膦酸，（氟代烷基）膦酸或所述酸的相应衍生物与无水氟化氢反应的步骤。
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公开(公告)号：US07439395B2
公开(公告)日：2008-10-21
申请号：US10588190
申请日：2005-01-17
IPC分类号： C07C277/00 , C07C279/00
CPC分类号： C07D233/28 , C07C211/15 , C07C277/08 , C07D233/48 , C07F9/28 , C07C279/04
摘要： The present invention relates to a two-step process for the preparation of guanidinium salts of the formula (1), where the substituents R have a meaning indicated in Claim, and A− is a sulfonate, alkyl- or arylsulfate, hydrogensulfate, imide, methanide, carboxylate, phosphate, phosphinate, phosphonate, borate, thiocyanate, perchlorate, fluorosilicate or nitrate, and to intermediate compounds from this process.
摘要翻译： 本发明涉及用于制备式（1）的胍盐的两步方法，其中取代基R具有权利要求中所述的含义，并且A是磺酸盐，烷基 - 或芳基硫酸盐，硫酸氢盐，酰亚胺，甲烷化物，羧酸盐，磷酸盐，次膦酸盐，膦酸盐，硼酸盐，硫氰酸盐，高氯酸盐，氟硅酸盐或硝酸盐，以及来自该方法的中间体化合物。
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公开(公告)号：US07999111B2
公开(公告)日：2011-08-16
申请号：US11995460
申请日：2006-06-14
IPC分类号： C07D211/10 , C07D233/58 , C07D207/06 , C07C211/63 , C07C321/14 , C07F9/54
CPC分类号： C07C381/00 , C07B45/02 , C07C209/68 , C07C303/32 , C07D213/06 , C07D233/54 , C07D295/037 , C07F9/5407 , C07F9/5435 , C07C309/04 , C07C211/63
摘要： The invention relates to a process for the preparation of onium alkylsulfonates by reaction of an onium halide or carboxylate with a symmetrically substituted dialkyl sulfite or with an asymmetrically substituted dialkyl sulfite at temperatures of 50 to 170° C.
摘要翻译： 本发明涉及通过卤化鎓或羧酸盐与对称取代的二烷基亚硫酸盐或与不对称取代的二烷基亚硫酸盐在50至170℃的温度下反应来制备烷基磺酸鎓的方法。
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10.发明申请公开(公告)号：US20110190480A1
公开(公告)日：2011-08-04
申请号：US13084109
申请日：2011-04-11
申请人： Nikolai (Mykola) IGNATYEV , Urs Welz-Biermann , Helge Willner , Maik Finze , Eduard Bernhardt , Andriy Kucheryna
发明人： Nikolai (Mykola) IGNATYEV , Urs Welz-Biermann , Helge Willner , Maik Finze , Eduard Bernhardt , Andriy Kucheryna
IPC分类号： C09B29/52 , C07F5/02 , C07F9/6509 , C07F9/655 , C09B19/00 , C09B11/12 , C09B15/00 , C09B21/00 , C07F9/653 , C07F9/572 , C07F9/6541 , C07F9/6553
CPC分类号： C07D241/46 , C07D263/54 , C07D277/62 , C09B23/06 , C09B67/0083 , C09B69/06
摘要： The present invention relates to dyes of the general formula CAT+ Y− (I), where Y− is an anion selected from the group of the cyanoborates, fluoroalkylphosphates, fluoroalkylborates or imidates and CAT+ is a cation selected from the group of the azine, xanthene, polymethine, styryl, azo, tetrazolium, pyrylium, benzopyrylium, thiopyrylium, benzothiopyrylium, thiazine, oxazine, triarylmethane, diarylmethane, methine, acridine, quinoline, isoquinoline or quaternary azafluorenone dyes, for colouring plastics and plastic fibres, for the preparation of flexographic printing inks, as ball-point pen pastes, as stamp ink, for colouring leather and paper, for use in data acquisition systems, reprography, in ink microfilters, in photogalvanics, laser technology and the photo industry.
摘要翻译： 本发明涉及通式CAT + Y-（I）的染料，其中Y-是选自氰基硼酸盐，氟烷基磷酸盐，氟烷基硼酸盐或亚胺酸盐的阴离子，CAT +是选自吖嗪，呫吨 ，聚甲炔，苯乙烯基，偶氮，四唑鎓，吡喃鎓，苯并吡喃鎓，硫代吡喃鎓，苯并硫代吡喃鎓，噻嗪，恶嗪，三芳基甲烷，二芳基甲烷，次甲基，吖啶，喹啉，异喹啉或季氮芴酮染料，用于着色塑料和塑料纤维，用于制备柔性版印刷 油墨，作为圆珠笔，作为印花油墨，用于着色皮革和纸张，用于数据采集系统，复印，墨水微滤器，光电镀，激光技术和照相行业。
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