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    Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use
    2.
    发明授权
    Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use 失效
    基于醇的含氟烷基官能的有机硅氧烷的组合物，其制备方法及其用途

    公开(公告)号：US06177582B1

    公开(公告)日：2001-01-23

    申请号：US08984162

    申请日：1997-12-03

    申请人： Peter Jenkner ,  Albert-Johannes Frings ,  Michael Horn ,  Eckhard Just ,  Jaroslaw Monkiewicz ,  Burkhard Standke

    发明人： Peter Jenkner ,  Albert-Johannes Frings ,  Michael Horn ,  Eckhard Just ,  Jaroslaw Monkiewicz ,  Burkhard Standke

    IPC分类号： C07P708

    CPC分类号： C03C25/40 ,  C08G77/24 ,  C09D183/08 ,  C09K3/18 ,  D06M13/513 ,  D06M15/657 ,  D21H19/32 ,  D21H21/16

    摘要： An alcoholic fluoroalkyl-functional group containing organosiloxane based composition is prepared by the controlled hydrolysis of at least one fluoroalkyl-functional group containing organosilane of formula I: R1—Y—(CH2)2SiHx(R2)y(OR)3−x−y  (I), in which R1 is a mono, oligo- or perfluorinated alkyl group having 1-9 C atoms or a mono-, oligo- or perfluorinated aryl group, Y is a CH2, O or S group, R2 and R are each independently a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group and x=0, 1 or 2 and y=0, 1 or 2, where (x+y)≦2, at a temperature in the range of 0-120° C. over a period of 0.5-24 hours and with thorough mixing in an alcoholic medium which contains water and a weak mono- or polybasic acid or a weak base or a weak mono- or polybasic acid and a weak base or an acid or basic salt, the water employed and the alkoxysilane employed being in a molar ratio of 2-500:1.

    摘要翻译： 含有有机硅氧烷的组合物的含氟烷基官能团的组合物是通过控制水解含有式I的有机硅烷的至少一个氟代烷基官能团制备的：其中R 1是具有1-9个C原子的单，低聚或全氟化烷基或 单，低聚或全氟化芳基，Y是CH 2，O或S基团，R 2和R 3各自独立地为具有1-8个碳原子或芳基且x = 0的直链，支链或环状的烷基， 1或2，y = 0,1或2，其中（x + y）<= 2，在0〜120℃的温度范围内，在0.5-24小时内，并在酒精中充分混合 含有水和弱单或多元酸或弱碱或弱单或多元酸和弱碱或酸或碱性盐的介质，所用的水和使用的烷氧基硅烷的摩尔比为2- 500：1。

    Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use
    3.
    发明授权
    Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use 失效
    基于醇的含氟烷基官能的有机硅氧烷的组合物，其制备方法及其用途

    公开(公告)号：US06713186B1

    公开(公告)日：2004-03-30

    申请号：US09685341

    申请日：2000-10-11

    申请人： Peter Jenkner ,  Albert-Johannes Frings ,  Michael Horn ,  Eckhard Just ,  Jaroslaw Monkiewicz ,  Burkhard Standke

    发明人： Peter Jenkner ,  Albert-Johannes Frings ,  Michael Horn ,  Eckhard Just ,  Jaroslaw Monkiewicz ,  Burkhard Standke

    IPC分类号： B32B1500

    CPC分类号： C09K3/18 ,  C03C25/40 ,  C08G77/24 ,  C09D183/08 ,  D06M13/513 ,  D06M15/657 ,  D21H19/32 ,  D21H21/16 ,  Y10T428/31663

    摘要： An alcoholic fluoroalkyl-functional group containing organosiloxane based composition prepared is prepared by the controlled hydrolysis of at least one fluoroalkyl-functional group containing organosilane of formula I: R1—Y—(CH2)2SiHx(R2)y(OR)3−x−y  (I), in which R1 is a mono, oligo- or perfluorinated alkyl group having 1-9 C atoms or a mono-, oligo- or perfluorinated aryl group, Y is a CH2, O or S group, R2 and R are each independently a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group and x=0, 1 or 2 and y=0, 1 or 2, where (x+y)≦2, at a temperature in the range of 0-120° C. over a period of 0.5-24 hours and with thorough mixing in an w alcoholic medium which contains water and a weak mono- or polybasic acid or a weak base or a weak mono- or polybasic acid and a weak base or an acid or basic salt, the water employed and the alkoxysilane employed being in a molar ratio of 2-500:1.

    摘要翻译： 制备的含有机硅氧烷的组合物的含氟烷基官能团的组合物是通过控制水解至少一个含有氟代烷基官能团的式I有机硅烷来制备的：其中R 1是具有1-羟基的单，低聚或全氟化的烷基， 9个C原子或单，低聚或全氟化芳基，Y为CH 2，O或S基团，R 2和R 3各自独立地为具有1-8个C原子的直链，支链或环状烷基或 芳基和x = 0,1或2，y = 0,1或2，其中（x + y）<= 2，在0〜120℃的温度下，在0.5-24小时内 并且在含有水和弱单或多元酸或弱碱或弱单或多元酸和弱碱或酸或碱性盐的w-醇介质中充分混合，使用的水和使用的烷氧基硅烷 摩尔比为2-500:1。

    Block Condensates of Organofunctional Siloxanes, Their Preparation and Use, and Their Properties
    4.
    发明申请
    Block Condensates of Organofunctional Siloxanes, Their Preparation and Use, and Their Properties 审中-公开

    公开(公告)号：US20090005518A1

    公开(公告)日：2009-01-01

    申请号：US11572555

    申请日：2005-06-03

    申请人： Eckhard Just ,  Sabine Giessler-Blank ,  Burkhard Standke

    发明人： Eckhard Just ,  Sabine Giessler-Blank ,  Burkhard Standke

    IPC分类号： C09D183/04 ,  B05D3/10

    CPC分类号： C08G77/24 ,  C08G77/26 ,  C09D183/08

    摘要： The present invention relates to a composition which comprises (i) at least one block condensate of organofunctional siloxanes of the general formula (I) [F]e[QcPb]d (I) and/or (ii) at least one mixture composed of e[F] and d(c[Q]+b[P]) and, where appropriate d[QcPb]. These compositions or block condensates are obtainable via reaction of block units F with block units Q, P, and/or QP, by one of the following methods:—c1) diluting block unit F optionally with an alcohol, adding an organic or inorganic acid and from 0.5 to 150 mol of water per mole of Si of the siloxane used, whereupon at least partial hydrolysis of the block units used takes place, then adding block unit Q and block unit P, and allowing the mixture to react, or—c2) diluting block unit F optionally with an alcohol, mixing with Q, P, and/or block unit QP, then adding an organic or inorganic acid and, using from 0.5 to 150 mol of water per mole of Si of the siloxanes used, carrying out partial hydrolysis and block-condensation, or—c3) diluting block unit F optionally with an alcohol, adding an organic or inorganic acid and from 0.5 to 150 mol of water per mole of Si of the siloxane used, with at least partial hydrolysis, adding block unit QP, and allowing the mixture to react, or—c4) diluting block units Q, P, and/or QP, optionally with an alcohol, adding an organic or inorganic acid and from 0.5 to 1.5 mol of water per mole of Si of the siloxanes used, and at least partially hydrolyzing, then adding block unit F and also from 0 to 148.5 mol of water per mole of Si of the siloxanes used, and allowing the mixture to react, or—c5) diluting block unit F optionally with an alcohol, mixing with from 0.5 to 150 mol of water per mole of Si of the siloxanes used, and with an organic or inorganic acid, and then adding a tetraalkoxysiloxane, and allowing the mixture to react. The present invention further relates to a process for the preparation of these compositions or block condensates, and to their use and to items thus obtainable: abrasion-resistant easy-clean coatings and items equipped with this type of coating.

    PROCESS FOR PREPARING ALKYLAMINOALKYLALKOXYSILANES
    7.
    发明申请
    PROCESS FOR PREPARING ALKYLAMINOALKYLALKOXYSILANES 有权
    制备烷基氨基烷基氧化硅的方法

    公开(公告)号：US20110118496A1

    公开(公告)日：2011-05-19

    申请号：US12995852

    申请日：2009-04-17

    申请人： Eckhard Just ,  Philipp Albert ,  Peter Jenkner

    发明人： Eckhard Just ,  Philipp Albert ,  Peter Jenkner

    IPC分类号： C07F7/20

    CPC分类号： C07F7/1892 ,  Y02P20/582

    摘要： A process for preparing an alkylaminoalkylalkoxysilane of formula (I) R—(NR′)—Y—Si(R1)n(OR2)3-n (I) in which R is a linear, branched or cyclic alkyl group having 1 to 12 carbon atoms, R′ is a hydrogen (H) or is a linear, branched or cyclic alkyl group having 1 to 12 carbon atoms, Y is a bivalent alkyl group from the group of —CH2—, —(CH2)2—, —(CH2)3—, —(CH2)(CH(CH3))(CH2)— and —(CH2)4—, R1 and R2 groups are the same or different and are each a linear or branched alkyl group having 1 to 4 carbon atoms, and n is 0 or 1 or 2, by reacting an alkylamine, used in excess, with a haloalkylalkoxysilane, distilling off excess free alkylamine, treating the remaining product mixture with the alkylaminoalkylalkoxysilane and working up.

    摘要翻译： 制备式（I）所示的烷基氨基烷基烷氧基烷氧基硅烷的方法R-（NR'）-Y-Si（R 1）n（OR 2）3-n（I）其中R是具有1至12个直链，支链或环状的烷基 碳原子，R'是氢（H）或是具有1至12个碳原子的直链，支链或环状烷基，Y是来自-CH 2 - ， - （CH 2）2 - ， - （CH 2）3 - ， - （CH 2）（CH（CH 3））（CH 2） - 和 - （CH 2）4 - ，R 1和R 2相同或不同，各自为具有1-4个 碳原子，n为0或1或2，通过使过量使用的烷基胺与卤代烷基烷氧基硅烷反应，蒸馏掉过量的游离烷基胺，用烷基氨基烷基烷氧基硅烷处理剩余的产物混合物并加工。

    COMPOSITION CONTAINING LOW-VOC, AMINOALKYL-FUNCTIONAL SILICON COMPOUNDS FOR COATING COLORS FOR THE TREATMENT OF PAPER OR FILM
    8.
    发明申请
    COMPOSITION CONTAINING LOW-VOC, AMINOALKYL-FUNCTIONAL SILICON COMPOUNDS FOR COATING COLORS FOR THE TREATMENT OF PAPER OR FILM 审中-公开
    包含用于处理纸张或胶片的涂料的低VOC，氨基官能化硅化合物的组合物

    公开(公告)号：US20110259240A1

    公开(公告)日：2011-10-27

    申请号：US12674601

    申请日：2008-07-04

    申请人： Peter Jenkner ,  Christoph Batz-Sohn ,  Heinz Lach ,  Stefan Scharfe ,  Philipp Albert ,  Eckhard Just

    发明人： Peter Jenkner ,  Christoph Batz-Sohn ,  Heinz Lach ,  Stefan Scharfe ,  Philipp Albert ,  Eckhard Just

    IPC分类号： C09D7/00

    CPC分类号： C08G77/54 ,  B41M5/52 ,  B41M5/5218 ,  B41M5/529 ,  C08L83/14 ,  C09D183/14

    摘要： The present invention relates to the use of a composition in coating agents, which is poor in volatile organic compounds (VOC) or essentially free of VOC, wherein the composition is at least partially based on one or more partially or fully hydrolyzed and optionally condensed or co-condensed aminoalkyl- and oligosilylated-aminoalkyl-, alkoxy- or hydroxy-functional silicon compounds and the alcohol is at least partially removed from the composition. The invention also relates to a composition containing aminoalkyl- or oligosilylated-aminoalkyl-, hydroxy- and optionally alkoxy-functional silicon compounds and to a method for producing such a composition.

    摘要翻译： 本发明涉及组合物在包衣剂中的用途，其在挥发性有机化合物（VOC）中较差或基本上不含VOC，其中该组合物至少部分基于一种或多种部分或全部水解并任选地缩合或 共缩合氨基烷基 - 和寡甲硅烷基化 - 氨基烷基 - ，烷氧基 - 或羟基官能的硅化合物和醇至少部分地从组合物中除去。 本发明还涉及包含氨基烷基 - 或寡甲硅烷基化的 - 氨基烷基 - 羟基 - 和任选的烷氧基官能的硅化合物的组合物以及用于制备这种组合物的方法。

    Specific process for preparing silicon compounds bearing fluoroalkyl groups by hydrosilylation
    9.
    发明授权
    Specific process for preparing silicon compounds bearing fluoroalkyl groups by hydrosilylation 有权
    通过氢化硅烷化制备带有氟烷基的硅化合物的具体方法

    公开(公告)号：US07598409B2

    公开(公告)日：2009-10-06

    申请号：US10583553

    申请日：2004-10-21

    申请人： Eckhard Just ,  Sabine Giessler ,  Peter Jenkner

    发明人： Eckhard Just ,  Sabine Giessler ,  Peter Jenkner

    IPC分类号： C07F7/04

    CPC分类号： C07F7/14

    摘要： The present invention relates to a process for preparing silicon compounds bearing fluoroalkyl groups by hydrosilylation of a fluoroolefin in the presence of a hydrosilylation catalyst, which comprises initially charging and heating a hydrogenchlorosilane, then metering in the fluoroolefin and reacting the reaction mixture and subsequently isolating the hydrosilylation product.

    摘要翻译： 本发明涉及一种在氢化硅烷化催化剂存在下通过氟代烯烃的氢化硅烷化制备含氟烷基的硅化合物的方法，该方法包括首先加入和加热氢氯硅烷，然后计量氟代烯烃并使反应混合物反应， 氢化硅烷化产物。

    Specific process for preparing silicon compounds bearing fluoroalkyl groups by hydrosilylation
    10.
    发明申请
    Specific process for preparing silicon compounds bearing fluoroalkyl groups by hydrosilylation 有权
    通过氢化硅烷化制备带有氟烷基的硅化合物的具体方法

    公开(公告)号：US20070112213A1

    公开(公告)日：2007-05-17

    申请号：US10583553

    申请日：2004-10-21

    申请人： Eckhard Just ,  Sabine Giessler ,  Peter Jenkner

    发明人： Eckhard Just ,  Sabine Giessler ,  Peter Jenkner

    IPC分类号： C07F7/00

    CPC分类号： C07F7/14

    摘要： The present invention relates to a process for preparing silicon compounds bearing fluoroalkyl groups by hydrosilylation of a fluoroolefin in the presence of a hydrosilylation catalyst, which comprises initially charging and heating a hydrogenchlorosilane, then metering in the fluoroolefin and reacting the reaction mixture and subsequently isolating the hydrosilylation product.

    摘要翻译： 本发明涉及一种在氢化硅烷化催化剂存在下通过氟代烯烃的氢化硅烷化制备含氟烷基的硅化合物的方法，该方法包括首先加入和加热氢氯硅烷，然后计量氟代烯烃并使反应混合物反应， 氢化硅烷化产物。