Method for treating residues containing salt, produced during the production of amino-functional organosilanes
    1.
    发明授权
    Method for treating residues containing salt, produced during the production of amino-functional organosilanes 有权
    在制备氨基官能有机硅烷时生产的含有盐的残留物的方法

    公开(公告)号:US09079926B2

    公开(公告)日:2015-07-14

    申请号:US12995871

    申请日:2009-04-20

    IPC分类号: C07F7/10 C07F7/18

    CPC分类号: C07F7/1892

    摘要: The invention relates to a method for treating an ammonium halogenide and/or residue containing organic aminhydrohalogenides, produced during the production of an amino-functional organosilane of general formula (I) R2N[(CH2)2NH]z(Z)Si(R″)n(OR′)3-n (Ia), wherein the production of the amino-functional organosilane according to formula (Ia) is based on the conversion of a halogen-functional organosilane of general formula (II) X—Z—Si(R″)n(OR′)3-n (II), with excess ammonia or an organic amine of general formula (III) RNH[(CH2)2NH]zR (III) and subsequently separating and treating the raw product and the resulting residue containing salt. The treatment consists of adding an essentially non-polar organic solvent and an aqueous lye to the residue. The mixture is reacted, subsequently the aqueous phase is separated from the organic phase, the organic solvent contained in the organic phase is removed from said phase and the residual organic phase is recovered.

    摘要翻译: 本发明涉及在制备通式(I)的氨基官能有机硅烷R2N [(CH2)2NH] z(Z)Si(R“)中产生的含有卤化胺和(或)残余物的有机氨基卤化氢的方法, )n(OR')3-n(Ia),其中根据式(Ia)的氨基官能的有机硅烷的制备基于通式(II)的卤素官能的有机硅烷的转化X-Z-Si (R“)n(OR')3-n(II)与过量氨或通式(III)的有机胺RNH [(CH2)2NH] zR(III)反应,随后分离和处理原料和 产生残留物含盐。 该处理包括向残余物中加入基本上非极性的有机溶剂和水性碱液。 使混合物反应,随后将水相与有机相分离,从所述相中除去有机相中包含的有机溶剂,并回收残留的有机相。

    Aqueous silane systems based on tris(alkoxysilylalkyl)amines and the use thereof

    公开(公告)号:US08772432B2

    公开(公告)日:2014-07-08

    申请号:US13258724

    申请日:2010-03-19

    IPC分类号: C08G77/26

    摘要: The invention relates to an aqueous composition based on tris-silylated amino-functional silicon compounds, which is substantially free of organic solvents and which substantially does not release any alcohol even during the cross-linking process, and to method for the production thereof, and to the use thereof, for example for the hydrophobization of metal, glass or mineral surfaces, such as concrete and bricks, as adhesion promoter or for rock consolidation, among other things.

    PROCESS FOR PREPARING ALKYLAMINOALKYLALKOXYSILANES
    4.
    发明申请
    PROCESS FOR PREPARING ALKYLAMINOALKYLALKOXYSILANES 有权
    制备烷基氨基烷基氧化硅的方法

    公开(公告)号:US20110118496A1

    公开(公告)日:2011-05-19

    申请号:US12995852

    申请日:2009-04-17

    IPC分类号: C07F7/20

    CPC分类号: C07F7/1892 Y02P20/582

    摘要: A process for preparing an alkylaminoalkylalkoxysilane of formula (I) R—(NR′)—Y—Si(R1)n(OR2)3-n (I) in which R is a linear, branched or cyclic alkyl group having 1 to 12 carbon atoms, R′ is a hydrogen (H) or is a linear, branched or cyclic alkyl group having 1 to 12 carbon atoms, Y is a bivalent alkyl group from the group of —CH2—, —(CH2)2—, —(CH2)3—, —(CH2)(CH(CH3))(CH2)— and —(CH2)4—, R1 and R2 groups are the same or different and are each a linear or branched alkyl group having 1 to 4 carbon atoms, and n is 0 or 1 or 2, by reacting an alkylamine, used in excess, with a haloalkylalkoxysilane, distilling off excess free alkylamine, treating the remaining product mixture with the alkylaminoalkylalkoxysilane and working up.

    摘要翻译: 制备式(I)所示的烷基氨基烷基烷氧基烷氧基硅烷的方法R-(NR')-Y-Si(R 1)n(OR 2)3-n(I)其中R是具有1至12个直链,支链或环状的烷基 碳原子,R'是氢(H)或是具有1至12个碳原子的直链,支链或环状烷基,Y是来自-CH 2 - , - (CH 2)2 - , - (CH 2)3 - , - (CH 2)(CH(CH 3))(CH 2) - 和 - (CH 2)4 - ,R 1和R 2相同或不同,各自为具有1-4个 碳原子,n为0或1或2,通过使过量使用的烷基胺与卤代烷基烷氧基硅烷反应,蒸馏掉过量的游离烷基胺,用烷基氨基烷基烷氧基硅烷处理剩余的产物混合物并加工。

    AQUEOUS CORROSION PROTECTION FORMULATION BASED ON SILANES
    6.
    发明申请
    AQUEOUS CORROSION PROTECTION FORMULATION BASED ON SILANES 审中-公开
    基于硅烷的水溶性腐蚀保护配方

    公开(公告)号:US20140106176A1

    公开(公告)日:2014-04-17

    申请号:US14007481

    申请日:2012-02-27

    IPC分类号: C09D5/08

    摘要: The present invention relates to a composition comprising a specific binder containing at least one cocondensate based on at least one ω-glycidyloxyalkylalkoxysilane and a bis(alkoxyalkylsilyl)amine, water, alcohol in an amount of less than 3% by weight, based on the composition, at least one addition selected from the group consisting of particulate metals, metal alloys and metal compounds and optionally at least one additive, where the pH of the composition is from 1 to 14 and the dry residue of the binder is from 1 to 50% by weight, based on the binder used, a process for the production thereof and also the use thereof for coatings, in particular for the protection of metals against corrosion.

    摘要翻译: 本发明涉及包含基于至少一种ω缩水甘油氧烷基烷氧基硅烷和双(烷氧基烷基甲硅烷基)胺的至少一种缩聚物的特定粘合剂,其组合物含量小于3重量% ,选自由颗粒金属,金属合金和金属化合物组成的组中的至少一种添加剂和任选的至少一种添加剂,其中组合物的pH为1至14,粘合剂的干燥残余物为1至50% ,基于所使用的粘合剂,其制备方法以及其用于涂料的用途,特别是用于保护金属免受腐蚀。

    Process for preparing alkylaminoalkylalkoxysilanes
    8.
    发明授权
    Process for preparing alkylaminoalkylalkoxysilanes 有权
    制备烷基氨基烷基烷氧基硅烷的方法

    公开(公告)号:US08426628B2

    公开(公告)日:2013-04-23

    申请号:US12995852

    申请日:2009-04-17

    IPC分类号: C07F7/10

    CPC分类号: C07F7/1892 Y02P20/582

    摘要: A process for preparing an alkylamino-alkylalkoxysilane of formula (I) R—(NR′)—Y—Si(R1)n(OR2)3-n (I) in which R is a linear, branched or cyclic alkyl group having 1 to 12 carbon atoms, R′ is a hydrogen (H) or is a linear, branched or cyclic alkyl group having 1 to 12 carbon atoms, Y is a bivalent alkyl group from the group of —CH2—, —(CH2)2—, —(CH2)3—, —(CH2)(CH(CH3))(CH2)— and —(CH2)4—, R1 and R2 groups are the same or different and are each a linear or branched alkyl group having 1 to 4 carbon atoms, and n is 0 or 1 or 2, by reacting an alkylamine, used in excess, distilling off excess free alkylamine, treating the remaining product mixture with the alkylaminoalkylalkoxysilane and working up.

    摘要翻译: 制备式(I)R(R')-Y-Si(R 1)n(OR 2)3-n(I)的烷基氨基 - 烷基烷氧基硅烷的方法,其中R是具有1 至12个碳原子,R'为氢(H)或为具有1至12个碳原子的直链,支链或环状烷基,Y为-CH 2 - , - (CH 2)2 - , - (CH 2)3 - , - (CH 2)(CH(CH 3))(CH 2) - 和 - (CH 2)4 - ,R 1和R 2相同或不同, 通过使过量使用的烷基胺蒸馏出过量的游离烷基胺,将剩余的产物混合物与烷基氨基烷基烷氧基硅烷一起处理并处理,使n为0或1或2。