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    Process for preparing triallyl isocyanurate (TAIC)
    1.
    发明授权
    Process for preparing triallyl isocyanurate (TAIC) 有权
    三烯丙基异氰脲酸酯（TAIC）的制备方法

    公开(公告)号：US08198431B2

    公开(公告)日：2012-06-12

    申请号：US12307592

    申请日：2007-06-14

    申请人： Peter Werle ,  Hans-Peter Krimmer ,  Manfred Schmidt ,  Klaus Stadtmueller ,  Martin Trageser

    发明人： Peter Werle ,  Hans-Peter Krimmer ,  Manfred Schmidt ,  Klaus Stadtmueller ,  Martin Trageser

    IPC分类号： C07D487/22 ,  C07B47/00

    CPC分类号： C07D251/34

    摘要： The invention is directed to an improved, reliably performable process for preparing triallyl isocyanurate (TAIC) by Cu2+-catalysed rearrangement of triallyl cyanurate (TAC) at at least 90° C. According to the invention, TAC and, if required, also a Cu2+ catalyst and solvent are fed continuously to a start reaction mixture after onset of the initially inhibited isomerization reaction, the isomerization is performed at from 90 to 160° C. and an amount of reaction mixture equivalent to the amount of reactant is drawn off continuously and sent to the workup. Preference is given to effecting the isomerization in TAIC as the reaction medium.

    摘要翻译： 本发明涉及通过三聚氰尿酸三烯丙酯（TAC）在至少90℃下通过Cu 2+催化重排制备三烯丙基异氰脲酸酯（TAIC）的改进的，可靠的可操作的方法。根据本发明，如果需要，TAC和Cu 2+ 催化剂和溶剂在最初抑制的异构化反应开始后连续进料到起始反应混合物中，异构化在90至160℃下进行，反应混合物的量等于反应物的量连续排出并发送 到后台。 优选在TAIC中作为反应介质进行异构化。

    PROCESS FOR PREPARING TRIALLYL ISOCYANURATE (TAIC)
    2.
    发明申请
    PROCESS FOR PREPARING TRIALLYL ISOCYANURATE (TAIC) 有权
    制备三异氰酸酯（TAIC）的方法

    公开(公告)号：US20090312545A1

    公开(公告)日：2009-12-17

    申请号：US12307592

    申请日：2007-06-14

    申请人： Peter Werle ,  Hans-Peter Krimmer ,  Manfred Schmidt ,  Klaus Stadtmueller ,  Martin Trageser

    发明人： Peter Werle ,  Hans-Peter Krimmer ,  Manfred Schmidt ,  Klaus Stadtmueller ,  Martin Trageser

    IPC分类号： C07D251/30

    CPC分类号： C07D251/34

    摘要： The invention is directed to an improved, reliably performable process for preparing triallyl isocyanurate (TAIC) by Cu2+-catalysed rearrangement of triallyl cyanurate (TAC) at least 90° C. According to the invention, TAC and, if required, also a Cu2+ catalyst and solvent are fed continuously to a start reaction mixture after onset of the initially inhibited isomerization reaction, the isomerization is performed at from 90 to 160° C. and an amount of reaction mixture equivalent to the amount of reactant is drawn off continuously and sent to the workup. Preference is given to effecting the isomerization in TAIC as the reaction medium.

    摘要翻译： 本发明涉及一种改进的，可靠的可行的制备三烯丙基异氰脲酸酯（TAIC）的方法，所述三烯丙基异氰脲酸酯是通过三异丙烯酸三烯丙酯（TAC）至少90℃的Cu 2+催化重排来制备的。根据本发明，如果需要，TAC和Cu 2+催化剂 在最初抑制的异构化反应开始后，将溶剂连续加入到起始反应混合物中，异构化在90〜160℃下进行，反应混合物的量等同于反应物的量连续排出并送至 的后卫。 优选在TAIC中作为反应介质进行异构化。

    Hydrolytically stable postcrosslinked superabsorbents
    6.
    发明授权
    Hydrolytically stable postcrosslinked superabsorbents 失效
    水解稳定的后交联超吸收剂

    公开(公告)号：US07728079B2

    公开(公告)日：2010-06-01

    申请号：US11885250

    申请日：2006-02-24

    申请人： Jörg Harren ,  Jörg Issberner ,  Mirko Walden ,  Rainer Teni ,  Franck Furno ,  Peter Werle ,  Hans-Peter Krimmer

    发明人： Jörg Harren ,  Jörg Issberner ,  Mirko Walden ,  Rainer Teni ,  Franck Furno ,  Peter Werle ,  Hans-Peter Krimmer

    IPC分类号： C08F8/30

    CPC分类号： C08J3/24 ,  C08F220/06 ,  C08J2333/02

    摘要： The present invention relates to a process for producing postcrosslinked water-absorbing polymeric formations, comprising the steps of contacting water-absorbing polymeric formations P1 obtained by polymerization of ethylenically unsaturated acid-functional monomers or salts thereof in the presence of a crosslinker with a fluid F1 comprising a postcrosslinker, heating the water-absorbing polymeric formations in contact with the fluid F1 to a temperature in a range from 40 to 300° C. to obtain postcrosslinked water-absorbing polymeric formations P2, the water-absorbing polymeric formations P1 having a thermal stability, as determined in accordance with the test method described herein, of less than 3.0%. The invention also relates to water-absorbing polymeric formations, to the water-absorbing polymeric formations obtainable by this process, to water-absorbing polymeric formations based on crosslinked carboxyl-bearing monomers, to a composite comprising water-absorbing polymeric formations and a substrate, to a process for producing a composite, to a composite obtainable by this process, to chemical products comprising water-absorbing polymeric formations or a composite, to the use of water-absorbing polymeric formations or of a composite in chemical products and also to the use of triallyl isocyanurate as an internal crosslinker in the production of water-absorbing polymeric formations based on crosslinked carboxyl-bearing monomers.

    摘要翻译： 本发明涉及一种生产后交联吸水聚合物地层的方法，包括以下步骤：将交联剂存在下烯属不饱和酸官能单体或其盐聚合得到的吸水聚合物地层P1与流体F1 包括后交联剂，将与流体F1接触的吸水聚合物层加热到40-300℃的温度，以获得后交联的吸水聚合物层P2，吸水聚合物层P1具有热 根据本文所述的测试方法测定的稳定性小于3.0％。 本发明还涉及吸水聚合物地层，可通过该方法获得的吸水聚合物地层，基于交联的含羧基单体的吸水聚合物地层，包括吸水聚合物地层和基底的复合材料， 涉及通过该方法可获得的复合材料的方法，涉及包含吸水聚合物结构或复合材料的化学产品，使用吸水聚合物结构或化学产品中的复合材料，以及使用 的三烯丙基异氰脲酸酯作为内部交联剂在基于交联的含羧基单体的吸水性聚合物地层的生产中。

    Hydrolytically Stable Postcrosslinked Superabsorbents
    7.
    发明申请
    Hydrolytically Stable Postcrosslinked Superabsorbents 失效
    水解稳定的后交联超吸收剂

    公开(公告)号：US20080214740A1

    公开(公告)日：2008-09-04

    申请号：US11885250

    申请日：2006-02-24

    申请人： Jorg Harren ,  Jorg Issberner ,  Mirko Walden ,  Rainer Teni ,  Franck Furno ,  Peter Werle ,  Hans-Peter Krimmer

    发明人： Jorg Harren ,  Jorg Issberner ,  Mirko Walden ,  Rainer Teni ,  Franck Furno ,  Peter Werle ,  Hans-Peter Krimmer

    IPC分类号： C08F8/30

    CPC分类号： C08J3/24 ,  C08F220/06 ,  C08J2333/02

    摘要： The present invention relates to a process for producing postcrosslinked water-absorbing polymeric formations, comprising the steps of contacting water-absorbing polymeric formations P1 obtained by polymerization of ethylenically unsaturated acid-functional monomers or salts thereof in the presence of a crosslinker with a fluid F1 comprising a postcrosslinker, heating the water-absorbing polymeric formations in contact with the fluid F1 to a temperature in a range from 40 to 300° C. to obtain postcrosslinked water-absorbing polymeric formations P2, the water-absorbing polymeric formations P1 having a thermal stability, as determined in accordance with the test method described herein, of less than 3.0%. The invention also relates to water-absorbing polymeric formations, to the water-absorbing polymeric formations obtainable by this process, to water-absorbing polymeric formations based on crosslinked carboxyl-bearing monomers, to a composite comprising water-absorbing polymeric formations and a substrate, to a process for producing a composite, to a composite obtainable by this process, to chemical products comprising water-absorbing polymeric formations or a composite, to the use of water-absorbing polymeric formations or of a composite in chemical products and also to the use of triallyl isocyanurate as an internal crosslinker in the production of water-absorbing polymeric formations based on crosslinked carboxyl-bearing monomers.

    摘要翻译： 本发明涉及一种生产后交联的吸水聚合物地层的方法，包括以下步骤：通过烯键式不饱和酸官能单体或其盐的聚合获得的吸水聚合物地层P 1 存在具有包含后交联剂的流体F 1 N的交联剂，将与流体F 1 1接触的吸水聚合物层加热到40〜 300℃以获得后交联的吸水聚合物组合物P 2，根据测试方法测定的具有热稳定性的吸水性聚合物组合物P 1 <1> 如本文所述，小于3.0％。 本发明还涉及吸水聚合物地层，可通过该方法获得的吸水聚合物地层，基于交联的含羧基单体的吸水聚合物地层，包括吸水聚合物地层和基底的复合材料， 涉及通过该方法可获得的复合材料的方法，涉及包含吸水聚合物结构或复合材料的化学产品，使用吸水聚合物结构或化学产品中的复合材料，以及使用 的三烯丙基异氰脲酸酯作为内部交联剂在基于交联的含羧基单体的吸水性聚合物地层的生产中。