Production of 1-bromopropane
    3.
    发明授权
    Production of 1-bromopropane 失效
    生产1-溴丙烷

    公开(公告)号:US5773672A

    公开(公告)日:1998-06-30

    申请号:US867144

    申请日:1997-06-20

    IPC分类号: C07C17/08 C07C17/00

    CPC分类号: C07C17/08

    摘要: 1-Bromopropane is produced from hydrogen bromide, propene and a catalytically effective amount of an ozonide catalyst and/or one or more active catalytic species formed in situ therefrom. In addition to being highly efficient and highly suitable for use on an industrial scale, the process has the additional advantages of being environmentally friendly, operationally safe, and conservationally beneficial.

    摘要翻译: 1-溴丙烷由溴化氢,丙烯和催化有效量的臭氧化物催化剂和/或由其原位形成的一种或多种活性催化物质制备。 除了高效率,高度适用于工业规模以外,该工艺还具有环保,操作安全,保护性好等优点。

    Reduction of metal halates and recovery of metal halides
    4.
    发明授权
    Reduction of metal halates and recovery of metal halides 失效
    金属卤化物的还原和金属卤化物的回收

    公开(公告)号:US5230879A

    公开(公告)日:1993-07-27

    申请号:US827334

    申请日:1992-01-29

    IPC分类号: C01B9/04 C01D3/10 C01F5/26

    CPC分类号: C01D3/10 C01B9/04 C01F5/26

    摘要: This invention relates to a process for reducing metal halates to metal halides, the process comprising reacting a metal halate with a reducing agent in an aqueous alkaline reaction medium having a pH above about 7, wherein the amount of reducing agent is sufficient to reduce substantially all of the metal halate to metal halide.

    摘要翻译: 本发明涉及将金属卤化物还原成金属卤化物的方法,该方法包括使金属卤化物与还原剂在pH高于约7的碱性水溶液中反应,其中还原剂的量足以基本上减少 的金属卤化物与金属卤化物反应。

    Production of tris(2,4,6-tribromophenoxy)-s-1,3,5-triazine
    6.
    发明授权
    Production of tris(2,4,6-tribromophenoxy)-s-1,3,5-triazine 失效
    三(2,4,6-三溴苯氧基)-s-1,3,5-三嗪的制备

    公开(公告)号:US5965731A

    公开(公告)日:1999-10-12

    申请号:US146155

    申请日:1998-09-03

    IPC分类号: C07D251/34 C07D251/30

    CPC分类号: C07D251/34

    摘要: In an aqueous reaction medium, phenol is brominated with bromine under conditions forming an aqueous hydrobromic acid phase and an organic phase consisting essentially of molten 2,4,6-tribromophenol. The aqueous hydrobromic acid phase and the molten 2,4,6-tribromophenol are separated from each other, and optionally the molten 2,4,6-tribromophenol is washed with an aqueous decolorizing solution. An alkali metal base and water are mixed with the 2,4,6-tribromophenol to form an alkali metal salt of tribromophenol. Then, in a mixture consisting essentially of water and at least one liquid ketone, cyanuric chloride is reacted with at least a portion of the alkali metal 2,4,6-tribromophenolate of such that tris(2,4,6-tribromophenoxy)-s-1,3,5-triazine is produced.

    摘要翻译: 在水性反应介质中,苯酚在形成氢溴酸水相的条件下由溴溴化,基本上由熔融的2,4,6-三溴苯酚组成的有机相进行溴化。 将氢溴酸水溶液相和熔融的2,4,6-三溴苯酚相互分离,任选地,用水性脱色溶液洗涤熔融的2,4,6-三溴苯酚。 将碱金属碱和水与2,4,6-三溴苯酚混合以形成三溴苯酚的碱金属盐。 然后,在基本上由水和至少一种液体酮组成的混合物中,使氰尿酰氯与至少一部分2,4,6-三溴苯酚酸碱金属反应,使得三(2,4,6-三溴苯氧基) - 制备s-1,3,5-三嗪。

    Groundwater treatment process
    7.
    发明授权
    Groundwater treatment process 失效
    地下水处理工艺

    公开(公告)号:US5352335A

    公开(公告)日:1994-10-04

    申请号:US973972

    申请日:1992-11-09

    申请人: Phillip R. Beaver

    发明人: Phillip R. Beaver

    摘要: A continuous process for the extraction of halogenated hydrocarbons from a dilute, halogenated hydrocarbon-containing aqueous fluid, in high efficiency, while dramatically reducing the stripping medium requirement for the extraction and without substantially increasing the amount of halogenated hydrocarbons discharged to the atmosphere.

    摘要翻译: 一种连续的方法,从高稀释的含卤代烃的含水流体中高效地提取卤代烃,同时显着地减少了汽提介质的萃取需求,而且基本不增加排放到大气中的卤代烃的量。

    Rupture disc monitor
    9.
    发明授权
    Rupture disc monitor 失效
    破裂光盘监视器

    公开(公告)号:US4912965A

    公开(公告)日:1990-04-03

    申请号:US331182

    申请日:1989-03-31

    IPC分类号: F16K17/16 F16K37/00 G01M3/26

    CPC分类号: F16K17/16 F16K37/00 G01M3/26

    摘要: This invention relates to an apparatus and process for detecting gas permeability in a main rupture disc which is in gaseous communication with a vessel. The process comprises: fitting a chamber over and in gas-tight association with the outside surface of the main rupture disc; selecting a burst presure for the main rupture disc and a set pressure; obtaining a gaseous pressure within the chamber which is greater than the normal operating pressure within the vessel, and equal to the difference between the set pressure and the burst pressure of the main rupture disc; and monitoring the chamber pressure for a decrease thereof. The apparatus comprises, generally, a chamber, a means for obtaining a gaseous pressure within the chamber, and a means for monitoring a change in pressure in the chamber.

    摘要翻译: 本发明涉及一种用于检测与容器气体连通的主破裂盘中的气体渗透性的装置和方法。 该方法包括:将腔室与主破裂盘的外表面相配合,并与气密相关联; 为主破裂盘选择爆破压力和设定压力; 在腔室内获得大于容器内的正常工作压力的气体压力,并且等于设定压力与主破裂盘的爆破压力之间的差值; 并监测腔室压力以减小腔室压力。 该装置通常包括室,用于获得室内的气体压力的装置以及用于监测室中的压力变化的装置。

    Process for recovering NTA
    10.
    发明授权
    Process for recovering NTA 失效
    恢复NTA的过程

    公开(公告)号:US3956379A

    公开(公告)日:1976-05-11

    申请号:US83664

    申请日:1970-10-23

    申请人: Phillip R. Beaver

    发明人: Phillip R. Beaver

    CPC分类号: C07C227/40

    摘要: It is disclosed that aqueous systems containing the sodium salt of nitrilotriacetate monohydrate (NTA) can be converted into a dry particulate form of NTA of comparatively high bulk density and suitable hygroscopic properties when using a spray drying technique by delivering to the spray dryer an NTA-water mixture which contains a greater amount of NTA than that present in a saturated aqueous solution of NTA. Upon spray drying such a particulate mixture with hot gases in a counter-current or co-current flow under proper conditions, water is removed from the particulate mixture producing a particulate solid NTA product.

    摘要翻译: 公开了将含有次氮基三乙酸钠一水合物(NTA)的钠盐的含水体系转化为具有较高堆积密度的NTA的干颗粒形式,并且当使用喷雾干燥技术时,通过将喷雾干燥器递送至NTA- 水混合物含有比在NTA的饱和水溶液中存在的NTA更大量的NTA。 在合适的条件下,用逆流或并流流动的这种具有热气体的微粒混合物喷雾干燥后,从颗粒状混合物中除去水,产生颗粒固体NTA产物。