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    Process for Preparing Nano Size Zeolites
    1.
    发明申请
    Process for Preparing Nano Size Zeolites 审中-公开
    制备纳米尺寸沸石的方法

    公开(公告)号：US20070224113A1

    公开(公告)日：2007-09-27

    申请号：US11688267

    申请日：2007-03-20

    Applicant: Richard R. Willis ,  Dorothy E. Kuechl ,  Annabelle I. Benin

    Inventor： Richard R. Willis ,  Dorothy E. Kuechl ,  Annabelle I. Benin

    IPC: C01B39/00 ,  C01B33/36

    CPC classification number: C01B39/24 ,  C01B39/04

    Abstract: A process has been developed to synthesize various zeolites with nano size crystals. The process involves forming an aluminosilicate initiator which exhibits the Tyndall effect. This initiator is then mixed with a clear solution comprising reactive sources of Al, Si, M and R plus water. M is an alkali or alkaline earth metal while R is an organoammonium compound. The resultant reaction mixture is reacted at a temperature and for a time sufficient to produce a zeolite such as zeolite Y with average crystallite size less than 500 nm.

    Abstract translation: 已经开发了一种合成具有纳米尺寸晶体的各种沸石的方法。 该方法包括形成具有廷德尔效应的硅铝酸盐引发剂。 然后将该引发剂与包含Al，Si，M和R反应水的水的澄清溶液混合。 M是碱金属或碱土金属，而R是有机铵化合物。 所得反应混合物在足以产生平均微晶尺寸小于500nm的沸石如沸石Y的温度和时间下反应。

    Process for Preparing Nano Size Zeolites
    2.
    发明申请
    Process for Preparing Nano Size Zeolites 审中-公开
    制备纳米尺寸沸石的方法

    公开(公告)号：US20100260664A1

    公开(公告)日：2010-10-14

    申请号：US12822353

    申请日：2010-06-24

    Applicant: Richard R. Willis ,  Dorothy E. Kuechl ,  Annabelle I. Benin

    Inventor： Richard R. Willis ,  Dorothy E. Kuechl ,  Annabelle I. Benin

    IPC: C01B39/02

    CPC classification number: C01B39/04 ,  C01B39/24

    Abstract: A process has been developed to synthesize various zeolites with nano size crystals. The process involves forming an aluminosilicate initiator which exhibits the Tyndall effect and contains no appreciable filterable solids. This initiator is then mixed with a clear solution comprising reactive sources of Al, Si, M and R plus water. M is an alkali or alkaline earth metal while R is an organoammonium compound. The resultant reaction mixture is reacted at a temperature and for a time sufficient to produce a zeolite such as zeolite Y with average crystallite size less than 500 nm or preferably less than 300 nm.

    Abstract translation: 已经开发了一种合成具有纳米尺寸晶体的各种沸石的方法。 该方法包括形成具有廷德尔效应的硅铝酸盐引发剂，并且不含有明显的可过滤固体。 然后将该引发剂与包含Al，Si，M和R反应水的水的澄清溶液混合。 M是碱金属或碱土金属，而R是有机铵化合物。 所得反应混合物在足以产生平均微晶尺寸小于500nm或优选小于300nm的沸石Y沸石的温度和时间下反应。

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