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    Overbased calcium salicylate greases
    4.
    发明授权
    Overbased calcium salicylate greases 有权
    高碱性水杨酸钙油脂

    公开(公告)号：US07407920B2

    公开(公告)日：2008-08-05

    申请号：US10911132

    申请日：2004-07-29

    Applicant: William D. Olson ,  Ronald J. Muir ,  Wayne MacKwood

    Inventor： William D. Olson ,  Ronald J. Muir ,  Wayne MacKwood

    IPC: C10M159/20 ,  C10M169/06

    CPC classification number: C10M163/00 ,  C10M117/04 ,  C10M159/22 ,  C10M169/06 ,  C10M2201/062 ,  C10M2207/126 ,  C10M2207/128 ,  C10M2207/26 ,  C10N2210/02 ,  C10N2250/10 ,  C10N2260/14

    Abstract: A process and composition for forming a non-Newtonian oil composition in the form of a grease comprising an overbased calcium salicylate and solid particles of colloidally dispersed calcium carbonate in the form of calcite is disclosed wherein the process comprises the steps of heating overbased calcium salicylate, amorphous calcium carbonate, and a converting agent comprising a fatty acid of twelve to twenty-four carbon atoms in an oleaginous medium, and then adding sufficient water, alcohol, and carbon dioxide to the mixture to complete the conversion of the amorphous calcium carbonate to calcite.

    Abstract translation: 公开了一种用于形成脂肪形式的非牛顿油组合物的方法和组合物，其包含高碱性水杨酸钙和以方解石形式的胶体分散的碳酸钙的固体颗粒，其中所述方法包括以下步骤：加热高碱性水杨酸钙， 无定形碳酸钙和含油介质中含有12至24个碳原子的脂肪酸的转化剂，然后向混合物中加入足够的水，醇和二氧化碳，以完成无定形碳酸钙转化为方解石 。

    Overbased magnesium deposit control additive for residual fuel oils
    5.
    发明授权
    Overbased magnesium deposit control additive for residual fuel oils 失效
    用于残余燃料油的高碱性镁沉积物控制添加剂

    公开(公告)号：US06197075B1

    公开(公告)日：2001-03-06

    申请号：US09054005

    申请日：1998-04-02

    Applicant: Ronald J. Muir ,  Theo I. Eliades

    Inventor： Ronald J. Muir ,  Theo I. Eliades

    IPC: C10L118

    CPC classification number: C10L1/1828 ,  C07C51/414 ,  C07F3/003 ,  C07G17/00 ,  C10L1/10 ,  C10L1/1233 ,  C10L1/125 ,  C10L1/1616 ,  C10L1/1824 ,  C10L1/1855 ,  C10L1/1881 ,  C10L1/1883 ,  C10L1/189 ,  C10L1/19 ,  C10L1/198 ,  C10L1/202 ,  C10L1/205 ,  C10L1/2225 ,  C10L1/2437 ,  C10L10/04

    Abstract: An overbased magnesium composition deposit control additive for residual fuel oils and turbine fuels is an overbased magnesium sulfonate, carboxylate or phenate or mixtures thereof containing at least 14% and upwards to about 18% by weight of magnesium and containing a succinic anhydride and lower carboxylic acid co-promoter reaction product. The additive when added to fuel oils, such as residual fuel oils containing high asphaltenes, reduces, if not eliminates, magnesium/asphaltene deposits or sediment and the consequential plugging of filters. The additive also reduces, if not eliminates, vanadium caused corrosion in the turbine. The invention is also the process for preparing the overbased composition or deposit control additive, wherein the overbasing reaction incorporates the combination of a lower carboxylic acid, preferably acetic acid and a succinic anhydride, preferably dodecenyl succinic anhydride (DDSA), as the co-promoter.

    Abstract translation: 用于残余燃料油和涡轮机燃料的高碱性镁组合物沉积物控制添加剂是高碱性磺酸镁，羧酸盐或酚盐或其混合物，其含有至少14重量％至约18重量％的镁并含有琥珀酸酐和低级羧酸 共促进剂反应产物。 当添加到燃料油中的添加剂，例如含有高沥青质的残余燃料油，减少（如果不消除）镁/沥青质沉积物或沉淀物以及由此导致的过滤器堵塞。 该添加剂还减少了如果不消除，钒在涡轮机中引起腐蚀。 本发明也是制备高碱性组合物或沉积物控制添加剂的方法，其中高碱性反应包含低级羧酸，优选乙酸和琥珀酸酐，优选十二碳烯基琥珀酸酐（DDSA）的组合，作为助催化剂 。

    Method for producing lubricant detergents
    9.
    发明授权
    Method for producing lubricant detergents 有权
    生产润滑剂的方法

    公开(公告)号：US07009072B2

    公开(公告)日：2006-03-07

    申请号：US10674896

    申请日：2003-09-29

    Applicant: Ronald J. Muir

    Inventor： Ronald J. Muir

    IPC: C07C65/10 ,  C07C65/05 ,  C07C65/03 ,  C07C65/01

    CPC classification number: C10M159/20 ,  C07C51/353 ,  C07C51/412 ,  C07C51/414 ,  C10M2207/028 ,  C07C65/05

    Abstract: The invention is a process for producing alkaline earth metal salicylates for use as lubricant detergents and to compositions prepared by the process. The process comprises two steps. Step 1 is the alkylation of salicylic acid is conducted using C14 or greater linear α-olefins to produce alkyl salicylic acids in commercially acceptable yields. The alkylation conditions produce predominately mono-substituted para alkyl salicylic acids that are oil soluble. Step 2 is the oil soluble acid is subsequently neutralized and overbased by carbonation of lime using CO2 in the presence of a promoter and a surfactant. The reaction mixture after overbasing is filtered and solvents are removed by distillation. Alternatively, alkyl salicylic acid can be reacted with a previously overbased alkaline earth sulfonate, e.g., calcium sulfonate, to produce alkaline earth salicylate salts comprising varying percentages of dispersed alkaline earth carbonate salts. In this method, no filtration of the end product is required, and, thus, it is commercially preferred.

    Abstract translation: 本发明是用于制备用作润滑剂洗涤剂的碱土金属水杨酸盐和通过该方法制备的组合物的方法。 该过程包括两个步骤。 步骤1是使用C 14或更多直链α-烯烃进行水杨酸的烷基化，以商业上可接受的产率制备烷基水杨酸。 烷基化条件主要是油溶性的单取代对位烷基水杨酸。 步骤2是在助催化剂和表面活性剂的存在下，随后通过使用CO 2 CO 2碳酸化中和并高碱性的油溶性酸。 过碱后的反应混合物过滤，通过蒸馏除去溶剂。 或者，烷基水杨酸可以与先前高碱性的碱土磺酸盐例如磺酸钙反应，以产生包含不同百分比的分散的碱土金属碳酸盐的碱土水杨酸盐。 在该方法中，不需要最终产物的过滤，因此是商业上优选的。

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