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    Thermosetting resin and its production
    2.
    发明授权
    Thermosetting resin and its production 失效
    热固性树脂及其生产

    公开(公告)号：US4205152A

    公开(公告)日：1980-05-27

    申请号：US859102

    申请日：1977-12-09

    申请人： Ryuzo Mizuguchi ,  Atsushi Takahashi ,  Shin-ichi Ishikura ,  Akimitsu Uenaka

    发明人： Ryuzo Mizuguchi ,  Atsushi Takahashi ,  Shin-ichi Ishikura ,  Akimitsu Uenaka

    IPC分类号： C08F220/58 ,  C08F246/00 ,  C09D133/24 ,  C08F20/06 ,  C08F220/06 ,  C08F28/00

    CPC分类号： C08F220/58 ,  C08F246/00 ,  C09D133/24 ,  Y10S526/923

    摘要： A thermosetting resin which is a linear copolymer having a molecular weight of 10,000 to 1,000,000 and a glass transition point of -30.degree. to +80.degree. C., obtained by polymerizing in an aqueous medium a monomer mixture comprising (1) 0.1 to 50% by weight of at least one polymerizable monomer having an ampho-ionic structure, selected from the group consisting of (i) compounds representable by the formula: ##STR1## wherein R.sub.1 is a hydrogen atom or a methyl group, R.sub.2 and R.sub.3 are each, the same or different, a C.sub.1 -C.sub.6 alkyl group, A is O or NH, m.sub.1 and n.sub.1 are each, the same or different, an integer of 1 to 12 and X.sup..crclbar. is SO.sub.3.sup..crclbar., SO.sub.4.sup..crclbar. or CO.sub.2.sup..crclbar. and (ii) compounds representable by either one of the formulae: ##STR2## wherein R.sub.4 is a hydrogen atom or a methyl group, R.sub.5 is a hydrogen atom or a C.sub.1 -C.sub.3 alkyl group, m.sub.2 is an integer of 0 to 6 and n.sub.2 is an integer of 1 to 6, and A and X.sup.- are as defined above, (2) 0.5 to 70% by weight of at least one polymerizable monomer containing a reactive amide group, representable by the formula: ##STR3## wherein R.sub.6 is a hydrogen atom or a methyl group and R.sub.7 is a hydrogen atom or a C.sub.1 -C.sub.4 alkyl group and (3) 1 to 99.4% by weight of at least one of other polymerizable monomers.

    摘要翻译： 一种热固性树脂，它是一种线性共聚物，其分子量为10,000至1,000,000，玻璃化转变温度为-30℃至+ 80℃。通过在水性介质中聚合单体混合物获得，该单体混合物包含（1）0.1至50％ 的至少一种具有两性离子结构的可聚合单体，其选自（i）由下式表示的化合物：其中R 1是氢原子或甲基，R 2和R 3 各自相同或不同，C1-C6烷基，A为O或NH，m1和n1各自相同或不同，为1〜12的整数，X（ - ）为SO 3（ - ），SO 4 （ - ）或CO 2（ - ）和（ii）可以由下式之一表示的化合物：其中R 4是氢原子或甲基，R 5是氢原子 或C1-C3烷基，m2为0〜6的整数，n2为1〜6的整数，A和X定义如上，（2）0.5〜70重量％的至少一种可聚合 单体含量 其中R6是氢原子或甲基，R7是氢原子或C1-C4烷基，和（3）1到99.4重量％的下式表示的反应性酰胺基团： 的至少一种其它可聚合单体。

    Ampho-ionic group-containing alkyd resins
    4.
    发明授权
    Ampho-ionic group-containing alkyd resins 失效
    含两性离子基团的醇酸树脂

    公开(公告)号：US4322324A

    公开(公告)日：1982-03-30

    申请号：US208641

    申请日：1980-11-20

    申请人： Ryuzo Mizuguchi ,  Shin-ichi Ishikura ,  Keizo Ishii

    发明人： Ryuzo Mizuguchi ,  Shin-ichi Ishikura ,  Keizo Ishii

    IPC分类号： C08G63/00 ,  B01F17/52 ,  C08G63/49 ,  C08G63/68 ,  C08G63/685 ,  C08G63/688 ,  C09D167/00

    CPC分类号： C08G63/6884

    摘要： An alkyd resin containing ampho-ionic groups of the formula: ##STR1## wherein A is a C.sub.1 -C.sub.6 alkylene or a phenylene group, is disclosed. Said resin is prepared by reacting a polyol, a polybasic acid and an ampho-ionic compound of the formula: ##STR2## wherein A is as defined above, R.sub.1 is a hydroxyalkyl, R.sub.2 and R.sub.3 are H or alkyl optionally containing sulfo and/or hydroxyl group.

    摘要翻译： 公开了含有下式的两性离子基团的醇酸树脂：其中A是C1-C6亚烷基或亚苯基。 所述树脂通过使多元醇，多元酸和下式的两性离子化合物反应制备：其中A如上所定义，R 1是羟烷基，R 2和R 3是H或任选地含有磺基和/或 羟基。

    Amphoteric amino sulfonate derivatives of epoxy resins
    5.
    发明授权
    Amphoteric amino sulfonate derivatives of epoxy resins 失效
    环氧树脂的两性氨基磺酸酯衍生物

    公开(公告)号：US4379872A

    公开(公告)日：1983-04-12

    申请号：US293077

    申请日：1981-08-17

    申请人： Shin-Ichi Ishikura ,  Kazunori Kanda ,  Ryuzo Mizuguchi

    发明人： Shin-Ichi Ishikura ,  Kazunori Kanda ,  Ryuzo Mizuguchi

    IPC分类号： C08G59/14 ,  C08G59/40 ,  C09D151/08 ,  C08L63/00

    CPC分类号： C09D151/08 ,  C08G59/1483 ,  C08G59/4064

    摘要： Amphoteric amino sulfonate derivatives of epoxy resins having at least one terminal group of the formula: ##STR1## wherein R.sub.1 and R.sub.2 are hydrogen or methyl, R.sub.3 is hydrogen or C.sub.1 -C.sub.20 alkyl or substituted alkyl, and R.sub.4 is C.sub.1 -C.sub.6 alkylene or substituted alkylene, which are reaction products of an epoxy resin having a plurality of terminal groups of the formula: ##STR2## wherein R.sub.1 and R.sub.2 are as defined, with an amino sulfonate of the formula:R.sub.3 --NH--R.sub.4 --SO.sub.3 Mwherein R.sub.3 and R.sub.4 are as defined, and M is a cation.

    摘要翻译： 具有至少一个下式的末端基团的环氧树脂的两性氨基磺酸酯衍生物：其中R 1和R 2是氢或甲基，R 3是氢或C 1 -C 20烷基或取代的烷基，R 4是C 1 -C 6亚烷基或取代的 亚烷基，其是具有下列式的多个端基的环氧树脂的反应产物：其中R 1和R 2如上所定义，与下式的氨基磺酸盐：R3-NH-R4-SO3M，其中R3和R4 如上所定义，M为阳离子。

    Process for preparing hydroxyalkylaminosulfonic acids
    7.
    发明授权
    Process for preparing hydroxyalkylaminosulfonic acids 失效
    制备羟烷基氨基磺酸的方法

    公开(公告)号：US4481150A

    公开(公告)日：1984-11-06

    申请号：US412977

    申请日：1982-08-27

    申请人： Keizou Ishii ,  Ryuzo Mizuguchi ,  Shinichi Ishikura ,  Tamotsu Yoshioka

    发明人： Keizou Ishii ,  Ryuzo Mizuguchi ,  Shinichi Ishikura ,  Tamotsu Yoshioka

    IPC分类号： C07C309/14 ,  C07C143/02

    CPC分类号： C07C309/14

    摘要： A process for preparing hydroxyalkylaminosulfonic acids which comprises reacting a hydroxyalkylamine of the formula: ##STR1## wherein R.sub.1 is a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, and R.sub.2 is a hydrogen atom, a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, or a lower alkyl group, with an alkali metal salt of an .alpha.,.beta.-unsaturated sulfonic acid of the formula: ##STR2## wherein R.sub.3 is a hydrogen atom or a methyl group and M is an alkali metal, followed by elimination of the alkali metal to give a hydroxyalkylaminosulfonic acid of the formula: ##STR3## wherein R.sub.1 and R.sub.3 are each as defined above and R.sub.2 ' is a hydrogen atom, a C.sub.1 -C.sub.20 hydroxyalkyl group optionally containing --O-- or --COO-- in the alkyl chain, a lower alkyl group or a group of the formula: ##STR4## wherein R.sub.3 is as defined above.

    摘要翻译： 一种制备羟烷基氨基磺酸的方法，其包括使下式的羟烷基胺反应：其中R1是在烷基链中任选含有-O-或-COO-的C1-C20羟基烷基，R2是氢原子 ，在烷基链或低级烷基中任选含有-O-或-COO-的C1-C20羟烷基，与下式的α，β-不饱和磺酸的碱金属盐反应：（III） ）其中R3是氢原子或甲基，M是碱金属，然后除去碱金属，得到下式的羟烷基氨基磺酸：其中R 1和R 3各自如上所定义，和 R2'是氢原子，在烷基链中任选地含有-O-或-COO-的C 1 -C 20羟基烷基，低级烷基或下式的基团：其中R 3如上所定义。

    High solid coating composition containing novel microparticles of crosslinked copolymer including amphoionic groups
    8.
    发明授权
    High solid coating composition containing novel microparticles of crosslinked copolymer including amphoionic groups 失效
    含有包含两性基团的交联共聚物的新颖微粒的高固体涂料组合物

    公开(公告)号：US4461870A

    公开(公告)日：1984-07-24

    申请号：US460878

    申请日：1983-01-25

    申请人： Kazunori Kanda ,  Keizou Ishii ,  Katsuaki Kida ,  Shinichi Ishikura ,  Ryuzo Mizuguchi

    发明人： Kazunori Kanda ,  Keizou Ishii ,  Katsuaki Kida ,  Shinichi Ishikura ,  Ryuzo Mizuguchi

    IPC分类号： C08G12/34 ,  C08G59/14 ,  C08G59/40 ,  C09D167/00 ,  C09D201/00 ,  C08L75/00 ,  C08L67/08

    CPC分类号： C09D167/00 ,  C08G12/34 ,  C08G59/14 ,  C08G59/4064 ,  C09D201/00

    摘要： A high solid coating composition comprising(A) a film-forming polymer having functional group(s) capable of reacting with the crosslinking agent (D) hereinafter referred to,(B) a volatile organic liquid diluent in which the polymer (A) is carried,(C) polymer microparticles having an average diameter of from 0.02 to 40 microns, which are insoluble in the combination of the film-forming polymer (A) and the diluent (B) and are maintained in a stabilized state of dispersion therein, and(D) a crosslinking agent dissolved in the diluent (B),which is characterized in that the microparticles (C) are composed of crosslinked copolymer of .alpha.,.beta.-ethylenically unsaturated monomers carrying thereon a resinous portion having an amphoionic group of the formula: ##STR1## wherein R is a member selected from optionally substituted alkylene having 1 to 6 carbon atoms and phenylene group and Y is --COOH or --SO.sub.3 H.

    摘要翻译： 一种高固体涂料组合物，其包含（A）具有能够与交联剂（D）反应的官能团的成膜聚合物，以下称为（B）其中聚合物（A）为其中的挥发性有机液体稀释剂 携带（C）平均直径为0.02〜40微米的聚合物微粒，其不溶于成膜聚合物（A）和稀释剂（B）的组合，并保持在其中的稳定的分散状态， 和（D）溶解在稀释剂（B）中的交联剂，其特征在于，微粒（C）由α，β-烯键式不饱和单体的交联共聚物组成，所述α，β-烯属不饱和单体带有具有下式的两性基团的树脂部分 ：其中R是选自具有1-6个碳原子的任意取代的亚烷基和亚苯基，Y是-COOH或-SO 3 H的成员。

    Novel peroxide monomer and a polymer therefrom
    10.
    发明授权
    Novel peroxide monomer and a polymer therefrom 失效
    新型过氧化单体和聚合物

    公开(公告)号：US5070167A

    公开(公告)日：1991-12-03

    申请号：US661622

    申请日：1991-02-28

    申请人： Noriyuki Tsuboniwa ,  Satoshi Urano ,  Ryuzo Mizuguchi

    发明人： Noriyuki Tsuboniwa ,  Satoshi Urano ,  Ryuzo Mizuguchi

    IPC分类号： C07C409/40 ,  C08F20/36 ,  C08F20/58 ,  C08G18/72

    CPC分类号： C08G18/728 ,  C07C409/40 ,  C08F20/36 ,  C08F20/58

    摘要： Disclosed is a peroxide monomer having the formula:CH.sub.2 =CR--A--OO--B (I)wherein R represents a hydrogen atom or an alkyl having 1 to 5 carbon atoms, A represents --NH--CO--, --CO--NH--CO--, or --CO--O--CH.sub.2 CH.sub.2 --NH--CO--, and B represents a moiety which has excluded the group (--OOH) from a hydroperoxide and a preparation thereof. The present invention also provides a polymer whose a main chain composed of carbon-carbon bonds is bonded with a pendant peroxide group represented by the formula:--A--OO--B (II)wherein A and B is the same as mentioned above, the content of the pendant peroxide group being 0.1 to 99.9% by weight and a molecular weight of said polymer being 1,000 to 100,000; and a preparation thereof.