Process for dehydrating hydrous sodium beta-naphtholate
    1.
    发明申请
    Process for dehydrating hydrous sodium beta-naphtholate 审中-公开
    脱水含水β-萘酚钠的方法

    公开(公告)号:US20050043564A1

    公开(公告)日:2005-02-24

    申请号:US10915354

    申请日:2004-08-11

    CPC分类号: C07C51/15 C07C65/11

    摘要: The present invention provides a process for dehydrating hydrous sodium β-naphtholate comprising: the step of heating the hydrous sodium β-naphtholate or a mixture of the hydrous sodium β-naphtholate and β-naphthol which comprises no more than 0.2 mole of β-naphthol per one mole of sodium β-naphtholate in a solvent at a temperature of 260-300° C. under an inert gas. The process makes it possible to dehydrate hydrous sodium β-naphtholate thoroughly in a short time with less production of tarry components.

    摘要翻译: 本发明提供了一种脱水含水β-萘酚钠的方法,包括:加氢含水β-萘酚钠或β-萘酚钠水合β-萘酚的混合物的步骤,其包含不超过0.2摩尔β-萘酚 每摩尔β-萘酚钠在溶剂中,在惰性气体下,温度为260-300℃。 该方法使得可以在短时间内彻底地脱水β-萘酚钠水合物,同时产生较少的焦油组分。

    Crystal of 2-hydroxynaphthalene-3-carboxylic acid and process for the preparation thereof
    2.
    发明授权
    Crystal of 2-hydroxynaphthalene-3-carboxylic acid and process for the preparation thereof 有权
    2-羟基萘-3-羧酸的晶体及其制备方法

    公开(公告)号:US06403827B1

    公开(公告)日:2002-06-11

    申请号:US09720994

    申请日:2001-01-03

    IPC分类号: C07C6334

    摘要: The present invention provides crystalline 2-hydroxynaphthalene-3-carboxylic acid (BON) characterized in that the average particle size is equal to or more than 157 &mgr;m and the proportion of the particles of which particle size is less than 74 &mgr;m is equal to or less than 14%. The crystalline composition of the present invention can be prepared by a process comprising the step of recrystallizing BON, especially at a high temperature, or by carrying out the acid precipitation step in the method for preparing BON at a high temperature.

    摘要翻译: 本发明提供结晶的2-羟基萘-3-羧酸(BON),其特征在于平均粒径等于或大于157μm,粒径小于74μm的颗粒的比例等于或等于 小于14%。 本发明的结晶组合物可以通过包括重结晶BON的步骤,特别是在高温下或通过在高温下进行BON制备方法进行酸沉淀步骤的方法来制备。

    Granule of parahydroxybenzoic acid or parahydroxybenzoic ester and process for producing the same
    5.
    发明授权
    Granule of parahydroxybenzoic acid or parahydroxybenzoic ester and process for producing the same 有权
    对羟基苯甲酸或对羟基苯甲酸酯的颗粒及其制备方法

    公开(公告)号:US06673962B2

    公开(公告)日:2004-01-06

    申请号:US10311633

    申请日:2002-12-18

    IPC分类号: C07C6501

    CPC分类号: C07C65/03 C07C69/88

    摘要: Granular product of parahydroxybenzoic acid or its ester which exhibits well suppressed dusting and caking tendency and a process for preparing the product are provided. The granular product of parahydroxybenzoic acid or its ester according to the instant invention has an average particle size of equal to or more than 150 &mgr;m and a hardness of 10-3000 g. The granular product of the invention can be prepared by dry compressing powdery parahydroxybenzoic acid or its ester to give compressed material, pulverizing and classifying the material.

    摘要翻译: 提供了显示良好抑制粉尘和结块倾向的对羟基苯甲酸或其酯的颗粒产物和制备该产品的方法。 本发明的对羟基苯甲酸或其酯的粒状产物的平均粒径为150μm以上,硬度为10〜3000g。 本发明的颗粒状产品可以通过干燥压制粉末状的对羟基苯甲酸或其酯来制备,得到压缩材料,粉碎和分级材料。

    Granules of 2-hydroxynaphthalene-3-carboxylic acid and method for preparing the same
    6.
    发明授权
    Granules of 2-hydroxynaphthalene-3-carboxylic acid and method for preparing the same 有权
    2-羟基萘-3-羧酸颗粒及其制备方法

    公开(公告)号:US06562998B1

    公开(公告)日:2003-05-13

    申请号:US09869143

    申请日:2001-06-26

    IPC分类号: C07C6334

    CPC分类号: C07C65/11

    摘要: Granular product of 2-hydroxynaphthalene-3-carboxylic acid with well-suppressed dusting tendency, and process for preparing the same is provided. Granular product of 2-hydroxynaphthalene-3-carboxylic acid having an average particle size of 150 &mgr;m or more and a hardness of 70-3000 g, and a process for preparing the same comprising the steps of dry compressing powdery 2-hydroxynaphthalene-3-carboxylic acid to give compressed material and pulverizing and classifying the same.

    摘要翻译: 提供具有良好抑制粉尘倾向的2-羟基萘-3-羧酸的颗粒产物及其制备方法。平均粒度为150μm以上的2-羟基萘-3-羧酸的粒状产物和 硬度为70-3000g,其制备方法包括以下步骤:将粉末状2-羟基萘-3-羧酸干燥,得到压缩材料并粉碎和分级。

    Liquid-crystal polyester resin
    7.
    发明授权
    Liquid-crystal polyester resin 有权
    液晶聚酯树脂

    公开(公告)号:US06984712B2

    公开(公告)日:2006-01-10

    申请号:US10496490

    申请日:2002-11-25

    IPC分类号: C08G63/06 C08F20/00 C09K19/32

    摘要: The present invention provides a liquid-crystalline polyester resin which comprises monomer units derived from 2-hydroxy-3-naphthoic acid and/or 2-hydroxynaphthalene-3,6-dicarboxylic acid in an amount of 1-5000 mmol % based on the total monomer components of the resin and an alkaline metal compound in an amount of 10-3000 ppm as alkaline metal based on the total monomer components of the resin. The liquid-crystalline polyester resin of the present invention has good colorability, improved heat resistance and good mechanical properties.

    摘要翻译: 本发明提供一种液晶聚酯树脂,其包含基于总量为1-5000mmol%的来源于2-羟基-3-萘甲酸和/或2-羟基萘-3,6-二羧酸的单体单元 树脂的单体组分和碱金属化合物,其量为基于树脂总单体成分的碱金属为10-3000ppm。 本发明的液晶聚酯树脂具有良好的着色性,耐热性和良好的机械性能。