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公开(公告)号：US20140171665A1
公开(公告)日：2014-06-19
申请号：US14136272
申请日：2013-12-20
Applicant: Shell Oil Company
Inventor： Jeroen VAN WESTRENEN
IPC: C07C7/10 , C07D301/03
CPC classification number: C07C7/10 , C07C1/20 , C07C7/08 , C07C11/04 , C07C11/06 , C07D301/03 , Y02P30/42 , C07C11/02
Abstract: The present invention provides a process for removing oxygenate from an olefin stream comprising oxygenate, comprising providing to an oxygenate recovery zone the olefin stream comprising oxygenate and a solvent comprising ethanol, treating the olefin stream comprising oxygenate with the solvent, and retrieving from the oxygenate recovery zone at least one oxygenate-depleted olefinic product stream comprising olefin and a spent solvent comprising at least part of the oxygenate.
Abstract translation: 本发明提供从包含含氧化合物的烯烃流中除去含氧化合物的方法，包括向含氧物回收区提供包含含氧化合物和包含乙醇的溶剂的烯烃流，用溶剂处理包含含氧化合物的烯烃流，并从含氧化合物回收 区域包含烯烃和包含至少部分含氧化合物的废溶剂的至少一种含氧化合物贫化烯烃产物流。
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公开(公告)号：US20130096328A1
公开(公告)日：2013-04-18
申请号：US13653116
申请日：2012-10-16
Applicant: SHELL OIL COMPANY
Inventor： Leslie Andrew CHEWTER , Hervé HENRY , Pieter OLDENHOVE , Rajaram RAMESH , Jeroen VAN WESTRENEN
IPC: C07D301/19
CPC classification number: C07D301/19 , Y02P20/125
Abstract: The invention relates to an integrated process for preparing an epoxide from an oxygenate, wherein the production of a lower olefin from the oxygenate and the subsequent epoxidation of the lower olefin is combined and wherein isobutene, a by-product of the lower olefin production, is converted into a hydroperoxide that is used for the conversion of the lower olefin into the corresponding epoxide.
Abstract translation: 本发明涉及从含氧化合物制备环氧化物的综合方法，其中从含氧化合物制备低级烯烃和随后的低级烯烃环氧化合并，其中异丁烯是较低烯烃生产的副产物是 转化为用于将低级烯烃转化成相应的环氧化物的氢过氧化物。
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公开(公告)号：US20150353441A1
公开(公告)日：2015-12-10
申请号：US14655348
申请日：2013-12-24
Applicant: SHELL OIL COMPANY
Inventor： Sivakumar SADASIVAN VIJAYAKUMARI , Jeroen VAN WESTRENEN
IPC: C07C1/20
Abstract: The invention relates to a process for the preparation of an olefinic product comprising ethylene and/or propylene from an oxygenate comprising: a) an oxygenate conversion step wherein a gaseous effluent comprising olefins is obtained; b) separation of water from the effluent; c) compression of the effluent; d) acid gas removal from the effluent wherein the water-depleted compressed gaseous effluent is treated with a caustic solution in a caustic tower and a non-aqueous liquid stream comprising one or more aromatic C7+ hydrocarbons is added to the caustic solution to control the formation of red oil; and e) separating the olefinic product from the gaseous effluent treated in step d).
Abstract translation: 本发明涉及一种从含氧化合物制备包含乙烯和/或丙烯的烯烃产物的方法，包括：a）含氧化合物转化步骤，其中获得包含烯烃的气态流出物; b）将水从流出物中分离出来; c）流出物的压缩; d）从流出物中除去酸性气体，其中将贫水的压缩气体流出物用苛性塔中的苛性碱溶液和包含一种或多种芳族C 7 +烃的非水液体流加入到苛性碱溶液中以控制形成 的红油; 和e）从在步骤d）中处理的气态流出物中分离烯烃产物。
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公开(公告)号：US20150251979A1
公开(公告)日：2015-09-10
申请号：US14717189
申请日：2015-05-20
Applicant: SHELL OIL COMPANY
IPC: C07C29/10 , C07D301/03 , C07C1/20
CPC classification number: C07C29/106 , C07C1/20 , C07C29/132 , C07D301/03 , C07D301/10
Abstract: The invention relates to a process for the production of ethylene oxide, comprising the steps of: producing ethylene by converting a stream comprising an oxygenate into a stream comprising ethylene and ethane; producing ethylene oxide by subjecting ethylene and ethane from the stream comprising ethylene and ethane to oxidation conditions resulting in a stream comprising ethylene oxide, unconverted ethylene and ethane; and recovering ethylene oxide from the stream comprising ethylene oxide, unconverted ethylene and ethane.
Abstract translation: 本发明涉及生产环氧乙烷的方法，包括以下步骤：通过将包含含氧化合物的料流转化成包含乙烯和乙烷的料流来生产乙烯; 通过使来自包含乙烯和乙烷的物流的乙烯和乙烷经历氧化条件产生包含环氧乙烷，未转化的乙烯和乙烷的物流来生产环氧乙烷; 并从包含环氧乙烷，未转化的乙烯和乙烷的物流中回收环氧乙烷。
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5.发明申请公开(公告)号：US20140343336A1
公开(公告)日：2014-11-20
申请号：US14360947
申请日：2012-11-28
Inventor： Sivakumar SADASIVAN VIJAYAKUMARI , Jeroen VAN WESTRENEN
CPC classification number: B01J29/90 , B01J20/18 , B01J20/3408 , B01J20/3458 , B01J29/40 , B01J29/85 , B01J38/12 , C07C1/20 , C07C4/06 , C07C2529/00 , Y02P20/584 , Y02P30/42 , C07C11/02
Abstract: The present invention relates to a process for the oxidative regeneration of a deactivated catalyst comprising providing a catalyst comprising molecular sieve in hydrogen form to a guard zone; passing a regeneration gas stream comprising oxidant through the guard zone to remove part of one or both of any alkali metal ion and alkaline earth metal ion from the regeneration gas stream, to provide a treated regeneration gas stream; providing deactivated catalyst comprising molecular sieve in a regeneration zone, said deactivated catalyst from one or both of an oxygenate to olefin process and an olefin cracking process; regenerating the deactivated catalyst in the regeneration zone with the treated regeneration gas stream to provide regenerated molecular sieve catalyst; wherein said catalyst in said guard zone is one or both of deactivated catalyst comprising molecular sieve in hydrogen form and regenerated catalyst comprising regenerated molecular sieve in hydrogen form.
Abstract translation: 本发明涉及一种失活催化剂的氧化再生方法，包括提供包含氢形式的分子筛的催化剂至保护区; 使包含氧化剂的再生气流通过保护区，从再生气流中除去部分碱金属离子和碱土金属离子中的一种或两种，以提供经处理的再生气流; 在再生区域中提供包含分子筛的失活催化剂，所述失活催化剂由含氧化合物与烯烃方法中的一种或两种以及烯烃裂解方法组成; 用经处理的再生气流再生再生区中的失活催化剂以提供再生分子筛催化剂; 其中所述保护区中的所述催化剂是包含氢形式的分子筛的失活催化剂中的一种或两种，以及包含氢形式的再生分子筛的再生催化剂。
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Patent Agency Ranking
公开(公告)号：US20140187836A1
公开(公告)日：2014-07-03
申请号：US14136123
申请日：2013-12-20
Applicant: Shell Oil Company
Inventor： Sivakumar SADASIVAN VIJAYAKUMARI , Jeroen VAN WESTRENEN
Abstract: The present invention relates to a process for removing oxygenate from an olefin stream comprising oxygenate, comprising providing to an oxygenate recovery zone the olefin stream comprising oxygenate and a liquid solvent comprising: (a) butanol; (b)alkyl tert-alkyl ether; or (c) alkyl tert-alkyl ether and butanol, treating the olefin stream comprising oxygenate with the liquid solvent, and retrieving from the oxygenate recovery zone at least one oxygenate-depleted olefinic product stream comprising olefin and a spent liquid solvent comprising at least part of the oxygenate.
Abstract translation: 本发明涉及从包含含氧化合物的烯烃流中除去含氧化合物的方法，包括向含氧物回收区提供包含含氧化合物和液体溶剂的烯烃流，其包含：（a）丁醇; （b）烷基叔烷基醚; 或（c）烷基叔烷基醚和丁醇，用液体溶剂处理包含含氧化合物的烯烃物流，并从含氧物回收区回收至少一种含有烯烃的含氧化合物的烯烃产物流和废液体溶剂，该废液包含至少部分 的含氧化合物。
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公开(公告)号：US20140187835A1
公开(公告)日：2014-07-03
申请号：US14136079
申请日：2013-12-20
Applicant: Shell Oil Company
Inventor： Jeroen VAN WESTRENEN , Sivakumar SADASIVAN VIJAYAKUMARI
IPC: C07C1/22
Abstract: The invention relates to a process for the preparation of ethylene and/or propylene comprising: (a) an oxygenate conversion step wherein a gaseous effluent comprising olefins is obtained; (b) subjecting the effluent to water removal and compression steps; (c) acid gas removal from the effluent obtained in step (b), wherein the gaseous effluent is treated with a caustic solution and a non-aqueous liquid stream comprising aromatic C7+ hydrocarbons is added to the caustic solution to control the formation of red oil, to obtain a treated gaseous effluent and a spent liquid phase comprising spent caustic solution, aromatic C7+ hydrocarbons and high molecular weight contaminants; and (d) separating an aqueous phase and a non-aqueous phase from the spent liquid phase; (e) purifying the non-aqueous phase by membrane separation using a hydrophobic non-porous or nano-porous membrane; and (f) separating the olefinic product from the treated gaseous effluent.
Abstract translation: 本发明涉及一种制备乙烯和/或丙烯的方法，包括：（a）含氧化合物转化步骤，其中获得包含烯烃的气态流出物; （b）使废水进行除水和压缩步骤; （c）从步骤（b）中获得的流出物中除去酸性气体，其中用苛性碱溶液处理气体流出物，并将包含芳族C 7 +烃的非水液体流加入苛性碱溶液中以控制形成红色油 ，以获得经处理的气态流出物和包含废碱溶液，芳族C 7+烃和高分子量污染物的废液相; 和（d）从废液相中分离出水相和非水相; （e）使用疏水性无孔或纳米多孔膜通过膜分离纯化非水相; 和（f）从经处理的气态流出物中分离出烯属产物。
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公开(公告)号：US20140148631A1
公开(公告)日：2014-05-29
申请号：US13932296
申请日：2013-07-01
Applicant: SHELL OIL COMPANY
Inventor： Leslie Andrew CHEWTER , Ye-Mon CHEN , Timothy NISBET , Sivakumar SADASIVAN VIJAYAKUMARI , Jeroen VAN WESTRENEN
IPC: C07C1/22
CPC classification number: C07C1/22 , B01J8/0055 , B01J8/008 , B01J8/1827 , B01J8/1863 , B01J2208/0084 , B01J2208/00911 , B01J2219/0004 , C07C1/20 , C07C4/06 , Y02P30/42 , C07C11/04 , C07C11/06
Abstract: The present invention provides a process for preparing ethylene and/or propylene, wherein an oxygenate feedstock is contacted with a zeolite-comprising catalyst at a temperature in the range of from 500 to 700° C. to obtain a reactor effluent comprising ethylene and/or propylene and the oxygenate feedstock is contacted with the catalyst in a riser reactor having a reactor wall defining a flow trajectory towards a downstream outlet for reactor effluent, wherein at least oxygenate feedstock and catalyst are provided at one or more upstream inlets of the riser reactor and wherein C5 olefins are admitted to the riser reactor at one or more of locations along the length of the flow trajectory. The invention further provides a reaction system suitable for preparing ethylene and propylene.
Abstract translation: 本发明提供一种制备乙烯和/或丙烯的方法，其中在500-700℃的温度下，含氧化合物原料与含沸石的催化剂接触，以获得包含乙烯和/或 丙烯和含氧化合物原料在具有反应器壁的提升管反应器中与催化剂接触，反应器壁限定朝向下游出口进行反应器流出物的流动轨迹，其中在提升管反应器的一个或多个上游入口处提供至少含氧化合物原料和催化剂， 其中C5烯烃在沿着流动轨迹的长度的一个或多个位置处进入提升管反应器。 本发明还提供了适用于制备乙烯和丙烯的反应体系。
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公开(公告)号：US20160257625A1
公开(公告)日：2016-09-08
申请号：US15032800
申请日：2014-10-30
Applicant: SHELL OIL COMPANY
Inventor： Jeroen Gerard MARSMAN , Leslie Andrew CHEWTER , Sivakumar SADASIVAN VIJAYAKUMARI , Jeroen VAN WESTRENEN
CPC classification number: C07C1/20 , C07C7/04 , C07C2529/00 , C07C2529/40 , Y02P30/42 , C07C11/04 , C07C11/06
Abstract: A process for converting oxygenates to olefms comprising: a) contacting an oxygenate containing stream with a molecular sieve catalyst under oxygenate to olefms conversion conditions in a reactor to form an effluent comprising olefms; b) separating C3-hydrocarbons from C4+ hydrocarbons in the effluent; c) separating C1 hydrocarbons and other light gases from C2+ hydrocarbons; d) separating C2 hydrocarbons from the C3 hydrocarbons; e) sending the C3 hydrocarbons to a C3 splitter to separate pro pylene from propane; f) removing propylene from the C3 splitter; and g) removing propane from the C3 splitter.
Abstract translation: 一种将含氧化合物转化为烯烃的方法，包括：a）在含氧化合物下使含氧化合物的物流与分子筛催化剂接触，以在烯烃转化条件下在反应器中形成含烯烃的流出物; b）将C3-烃与流出物中的C4 +烃分离; c）从C2 +烃分离C1烃和其他轻质气体; d）从C3烃中分离C2烃; e）将C3碳氢化合物送入C3分离器以将丙烯与丙烷分离; f）从C3分离器中除去丙烯; 和g）从C3分离器中除去丙烷。
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公开(公告)号：US20150353440A1
公开(公告)日：2015-12-10
申请号：US14655345
申请日：2013-12-24
Applicant: SHELL OIL COMPANY
Inventor： Antonius Gijsbertus Johannes KLOTH , Sivakumar SADASIVAN VIJAYAKUMARI , Jeroen VAN WESTRENEN
IPC: C07C1/20
CPC classification number: C07C1/20 , C07C7/005 , C07C2529/00 , Y02P30/42 , Y02P30/48 , C07C11/04 , C07C11/06
Abstract: The invention relates to process for the preparation of an olefinic product comprising ethylene and/or propylene from an oxygenate, the process comprising the following steps: a) an oxygenate conversion step wherein a gaseous effluent comprising olefins and a water-soluble oxygenate is obtained; b) separation of water from the effluent; c) compression of the effluent; d) acid gas removal from the compressed gaseous effluent obtained in step c), wherein the compressed gaseous effluent is treated with a caustic solution in a caustic tower; and e) separating the olefinic product from the gaseous effluent treated in step d), wherein, in a final stage in the caustic tower, water-depleted compressed gaseous effluent is treated with a water stream that is essentially free of water-soluble oxygenate and a spent water stream comprising caustic and water-soluble oxygenate is obtained, which spent water stream is withdrawn from the process.
Abstract translation: 本发明涉及从含氧化合物制备包含乙烯和/或丙烯的烯烃产物的方法，该方法包括以下步骤：a）含氧化合物转化步骤，其中获得包含烯烃和水溶性含氧化合物的气态流出物; b）将水从流出物中分离出来; c）流出物的压缩; d）从步骤c）中获得的压缩气态流出物中除去酸性气体，其中将压缩的气态流出物用苛性塔中的苛性碱溶液处理; 和e）从在步骤d）中处理的气态流出物中分离烯烃产物，其中在苛性塔中的最后阶段，用基本上不含水溶性含氧化合物的水流处理含水贫化的压缩气体流出物， 得到包含苛性和水溶性含氧化合物的废水流，从该方法中取出废水流。
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