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公开(公告)号：US08268186B2
公开(公告)日：2012-09-18
申请号：US12579496
申请日：2009-10-15
IPC分类号： A62D1/00 , C07C311/03 , C07C311/09 , C07C311/24
CPC分类号： C07C311/24 , A62D1/0071 , A62D1/0085 , C07C311/09
摘要： A compound of Formula (I): wherein Ra is linear or branched F(CF2)n(CH2CF2)m—, or linear or branched F(CF2)o interrupted by 1 to 6 catenary oxygen atoms, each oxygen bonded to two carbon atoms, m is 1 to 4, n is 2 to 6, o is 2 to 7, A is O or (CH2)k—COO, R1 is hydrogen or a methyl, R2 and R3 are each independently alkyl having 1 to 6 carbon atoms, and p, q and k are each independently integers from 1 to 10, which is suitable for use as a surfactant and in fire fighting formulations.
摘要翻译： 式（I）的化合物：其中R a是直链或支链的F（CF 2）n（CH 2 CF 2）m - 或被1至6个链状氧原子间隔的直链或支链的F（CF 2）o，每个氧键合到两个碳原子 ，m为1至4，n为2至6，o为2至7，A为O或（CH 2）k-COO，R 1为氢或甲基，R 2和R 3各自为具有1至6个碳原子的烷基 ，p，q和k各自独立地为1至10的整数，其适合用作表面活性剂和消防制剂。
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公开(公告)号：US20110089362A1
公开(公告)日：2011-04-21
申请号：US12579496
申请日：2009-10-15
IPC分类号： A62D1/00 , C07C229/02 , C07C311/01
CPC分类号： C07C311/24 , A62D1/0071 , A62D1/0085 , C07C311/09
摘要： A compound of Formula (I): wherein Ra is linear or branched F(CF2)n(CH2CF2)m—, or linear or branched F(CF2)o interrupted by 1 to 6 catenary oxygen atoms, each oxygen bonded to two carbon atoms, m is 1 to 4, n is 2 to 6, o is 2 to 7, A is O or (CH2)k—COO, R1 is hydrogen or a methyl, R2 and R3 are each independently alkyl having 1 to 6 carbon atoms, and p, q and k are each independently integers from 1 to 10, which is suitable for use as a surfactant and in fire fighting formulations.
摘要翻译： 式（I）的化合物：其中R a是直链或支链的F（CF 2）n（CH 2 CF 2）m - 或被1至6个链状氧原子间隔的直链或支链的F（CF 2）o，每个氧键合到两个碳原子 ，m为1至4，n为2至6，o为2至7，A为O或（CH 2）k-COO，R 1为氢或甲基，R 2和R 3各自为具有1至6个碳原子的烷基 ，p，q和k各自独立地为1至10的整数，其适合用作表面活性剂和消防制剂。
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公开(公告)号：US08263670B2
公开(公告)日：2012-09-11
申请号：US11890414
申请日：2007-08-06
IPC分类号： B01D12/00 , B01F17/14 , C09D5/00 , C09D7/06 , C09D7/12 , C07F9/09 , C09K3/18 , C11D1/34 , C08L21/02 , C09D201/00
摘要： A compound of Formula 1 Rf-A-OP(O)(O−M+)(O—RH) Formula 1 wherein Rf is a C2 to C6 linear or branched perfluoroalkyl optionally interrupted by one, two or three ether oxygen atoms; A is (CH2CF2)m(CH2)n—, (CH2)oSO2N(CH3)(CH2)p—, O(CF2)q(CH2)r—, or OCHFCF2OE-; m is 1 to 4; n, o, p, and r are each independently 2 to 20; q is 2; E is a C2 to C20 linear or branched alkyl group optionally interrupted by oxygen, sulfur, or nitrogen atoms; a cyclic alkyl group, or a C6 to C10 aryl group; M is a Group I metal or an ammonium cation (NHxR2y)+ wherein R2 is a C1 to C4 alkyl, x is 1 to 4, y is 0 to 3 and x+y is 4; and RH is a C1 to C20 linear, branched, or cyclic alkyl, or a C6 to C10 aryl, and its use as a surfactant is disclosed.
摘要翻译： 式1的化合物Rf-A-OP（O）（O-M +）（O-RH）式1其中Rf是任选被一个，两个或三个醚氧原子间隔的C2至C6直链或支链全氟烷基; A是（CH 2 CF 2）m（CH 2）n - ，（CH 2）o SO 2 N（CH 3）（CH 2）p - ，O（CF 2）q（CH 2）r - 或OCHFCF 2 OE-; m为1〜4; n，o，p和r各自独立地为2〜20; q是2; E是任选被氧，硫或氮原子间隔的C2至C20直链或支链烷基; 环状烷基或C6〜C10芳基; M为I族金属或铵阳离子（NH x R 2y）+，其中R 2为C 1至C 4烷基，x为1至4，y为0至3，x + y为4; 并且RH是C1至C20直链，支链或环状烷基或C6至C10芳基，并且其用作表面活性剂。
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公开(公告)号：US20090042996A1
公开(公告)日：2009-02-12
申请号：US11890395
申请日：2007-08-06
IPC分类号： A61K31/045 , A61K31/66 , C07C309/63 , C07C31/125 , C07C311/01 , C07C69/00 , C07F7/02 , C07F9/02 , C09G1/06 , C09K13/00 , C09K3/00 , C11D1/00 , C11D1/04 , C11D1/34 , C11D3/20
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)x—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]s—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)xCH2CH(OH)—(CH2CH2O)x—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)zC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHxR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z—, then at least one of s or e is a positive integer.
摘要翻译： （Rf-A）aQ - （[B] kR）b式1 <？在线公式“=”在线公式“end =”lead“ description =“In-line Formulas”end =“tail”？>其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHR 1 O）x - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] s - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH）（V）CH 2 C（O） - （CH2CH2O）xCH2CH（OH） - （CH2CH2O）x-（CH2）m-Si [OSi（R2）3] 2-，-SO2NR2-， - （CH2CH2O）zC（O）CH（SO3-M +）CH2C O）（OCH 2 CH 2）z - ，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1价金属或铵（NHxR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O） M +）（O） - 或Q为 - （CH 2 CH 2 O）z C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）z - 时，则s或e中的至少一个为正整数。
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公开(公告)号：US20110183268A1
公开(公告)日：2011-07-28
申请号：US13080361
申请日：2011-04-05
申请人： Charles D. Lang , Stephen Sorich , Charles Kenneth Taylor , Douglas Robert Anton , Alberto Goenaga , Paul Anthony Sant
发明人： Charles D. Lang , Stephen Sorich , Charles Kenneth Taylor , Douglas Robert Anton , Alberto Goenaga , Paul Anthony Sant
IPC分类号： G03F7/20
CPC分类号： H01L51/0004 , H01L51/0003 , H01L51/0005 , H01L51/0011 , H01L51/0018 , H01L51/5012 , H01L51/56
摘要： There is provided a process for forming a contained second layer over a first layer, including the steps: forming the first layer having a first surface energy; treating the first layer with a reactive surface-active composition to form a treated first layer having a second surface energy which is lower than the first surface energy; exposing the treated first layer with radiation; and forming the second layer. There is also provided an organic electronic device made by the process.
摘要翻译： 提供了一种用于在第一层上形成包含的第二层的方法，包括以下步骤：形成具有第一表面能的第一层; 用反应性表面活性组合物处理第一层以形成具有低于第一表面能的第二表面能的经处理的第一层; 用辐射暴露经处理的第一层; 并形成第二层。 还提供了通过该方法制造的有机电子装置。
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公开(公告)号：US20100267843A1
公开(公告)日：2010-10-21
申请号：US12758280
申请日：2010-04-12
IPC分类号： A61K47/08 , C09G1/02 , C08K5/52 , C11D3/36 , C09D11/02 , C09G1/00 , B01F17/14 , C25D3/02 , C09K13/00 , C12N1/00 , D21H23/76 , C09K3/00
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)x—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]s—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)xCH2CH(OH)—(CH2CH2O)x—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)zC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHxR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z—, then at least one of s or e is a positive integer.
摘要翻译： 式1的表面活性剂（Rf-A）a-Q - （[B] k-R）b式1其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHR 1 O）x - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] s - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m -C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH） - ; - （CH2CH2O）xCH2CH（OH） - （CH2CH2O）x-（CH2）m-Si [OSi（R2）3] 2-，-SO2NR2-， - （CH2CH2O）zC（O）CH（SO3-M +）CH2C O）（OCH 2 CH 2）z - ，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1价金属或铵（NHxR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O） M +）（O） - 或Q为 - （CH 2 CH 2 O）z -C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）z - 时，则s或e中的至少一个为正整数。
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公开(公告)号：US07728163B2
公开(公告)日：2010-06-01
申请号：US11890395
申请日：2007-08-06
IPC分类号： C07F9/02
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)x—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]s—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)xCH2CH(OH)—(CH2CH2O)x—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)zC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHxR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)z—, then at least one of s or e is a positive integer.
摘要翻译： 式1的表面活性剂（Rf-A）a-Q - （[B] k-R）b式1其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHR 1 O）x - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] s - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m -C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH） - ; - （CH2CH2O）xCH2CH（OH） - （CH2CH2O）x-（CH2）m-Si [OSi（R2）3] 2-，-SO2NR2-， - （CH2CH2O）zC（O）CH（SO3-M +）CH2C O）（OCH 2 CH 2）z - ，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1价金属或铵（NHxR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O） M +）（O） - 或Q为 - （CH 2 CH 2 O）z -C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）z - 时，则s或e中的至少一个为正整数。
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公开(公告)号：US08242301B2
公开(公告)日：2012-08-14
申请号：US12758280
申请日：2010-04-12
IPC分类号： C07F9/02
CPC分类号： C07C69/675 , C07C43/137 , C07C309/65 , C07F7/0838 , C07F7/1804 , C07F9/091 , C11D1/004
摘要： A surfactant of formula 1 (Rf-A)a-Q-([B]k—R)b Formula 1 wherein a and b are each independently 1 or 2; Rf is a linear or branched perfluoroalkyl radical having from 2 to about 20 carbon atoms, optionally interrupted with at least one oxygen; R is a C1 to C20 linear, branched or cyclic alkyl, or a C6 to C10 aryl; B is —(CH2CHR1O)X—, k is 0 or 1, x is 1 to about 20, A is —(CH2)m[(CHR1CH2O)]S—[(CH2)m(CH)tCHOH(CH2)m]e—, wherein each m is independently 0 to 3, s is 0 to about 30, t is 0 or 1, and e is 0 or 1, R1 is H or CH3, Q is: —OP(O)(O−M+)(O)—, —O—, —S—(CH2)m—C(O)—O—, —SO2—O— —CH2CH2O—C(O)CH2C(OH)(V)CH2C(O)O—; —(CH2CH2O)XCH2CH(OH)—(CH2CH2O)X—(CH2)m—Si[OSi(R2)3]2—, —SO2NR2—, —(CH2CH2O)ZC(O)CH(SO3−M+)CH2C(O)(OCH2CH2)Z— wherein z is 1 to about 15, or a bond when s is a positive integer, V is —C(O)OR3 and R3 is H, CH3 or Rf; R2 is C1 to C4 alkyl, and M+ is a Group 1 metal or an ammonium (NHXR2y)+ cation wherein x+y=4, and R2 is C1 to C4 alkyl, provided that when Q is —OP(O)(O−M+)(O)— or when Q is —(CH2CH2O)Z—C(O)CH(SO3−M+)CH2C(O)(OCH2CH2)Z—, then at least one of s or e is a positive integer.
摘要翻译： 式1的表面活性剂（Rf-A）a-Q - （[B] k-R）b式1其中a和b各自独立地为1或2; Rf是具有2至约20个碳原子的直链或支链全氟烷基，任选被至少一个氧中断; R为C1至C20直链，支链或环状烷基或C6至C10芳基; B是 - （CH 2 CHRO）X - ，k是0或1，x是1至约20，A是 - （CH 2）m [（CHR 1 CH 2 O）] S - [（CH 2）m（CH）t CHOH（CH 2）m] e-，其中每个m独立地为0至3，s为0至约30，t为0或1，e为0或1，R 1为H或CH 3，Q为：-OP（O）（O-M + ）（O） - ， - O - ， - S-（CH 2）m -C（O）-O-，-SO 2 -O-CH 2 CH 2 O-C（O）CH 2 C（OH） - ; - （CH 2 CH 2 O）XCH 2 CH（OH） - （CH 2 CH 2 O）X（CH 2）m -Si [OSi（R 2）3] 2-，-SO 2 NR 2 - ， - （CH 2 CH 2 O） O）（OCH 2 CH 2）Z-，其中z为1至约15，或当s为正整数时为键，V为-C（O）OR 3且R 3为H，CH 3或R f; R2是C1-C4烷基，M +是1族金属或铵（NHXR2y）+阳离子，其中x + y = 4，R2是C1-C4烷基，条件是当Q是-OP（O）（O- M +）（O） - 或Q为 - （CH 2 CH 2 O）Z-C（O）CH（SO 3 -M +）CH 2 C（O）（OCH 2 CH 2）Z - 时，则s或e中的至少一个为正整数。
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公开(公告)号：US07553985B2
公开(公告)日：2009-06-30
申请号：US11265037
申请日：2005-11-02
IPC分类号： C07F9/02
CPC分类号： C07C309/10 , C07C67/287 , C07C309/17 , C07F9/091 , Y10T428/31855
摘要： A composition of formula I [Rf(CH2)m(O)n]x-A wherein Rf is a straight or branched perfluoroalkyl group having from about 2 to about 20 carbon atoms, or a mixture thereof, m is a positive integer equal to or greater than 3, n is 0 or 1, x is 1 to about 3, A is —P(O)(OR1)y(OM+)3−y−x, —C(O)CH(SO3−M+)CH2C(O)—, —(CH2CH2O)d(CH2CHR2O)eR3, or —SO2B, M+ is an alkali metal ion, NH4+, or NH2+(CH2CH2OH)2, B is N(R2)2 or N(CH2CH3)(CH2CH2OH), R1 is C1 to C3 alkyl, R2 is C1 to C4 alkyl, R3 is H or CH3, y is 0 to about 1, d is 0 to about 16, e is 0 to about 16, provided that (d+e) is from about 3 to about 16 is disclosed.
摘要翻译： 式I的组合<？in-line-formula description =“In-line Formulas”end =“lead”？> [Rf（CH2）m（O）n] xA <？in-line-formula description =“In 其中R f为具有约2-约20个碳原子的直链或支链全氟烷基，或其混合物，m为等于或大于3的正整数，n为0 或1，x为1至约3，A为-P（O）（OR1）y（OM +）3-yx，-C（O）CH（SO3-M +）CH2C（O） - ， - （CH2CH2O） （CH2CHR2O）eR3或-SO2B，M +是碱金属离子，NH4 +或NH2 +（CH2CH2OH）2，B是N（R2）2或N（CH2CH3）（CH2CH2OH），R1是C1至C3烷基，R2是 C1至C4烷基，R3为H或CH3，y为0至约1，d为0至约16，e为0至约16，条件是（d + e）为约3至约16。
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公开(公告)号：US20070218582A1
公开(公告)日：2007-09-20
申请号：US11401151
申请日：2006-04-10
申请人： Charles D. Lang , Stephen Sorich , Charles Kenneth Taylor , Douglas Robert Anton , Alberto Goenaga , Paul Anthony Sant
发明人： Charles D. Lang , Stephen Sorich , Charles Kenneth Taylor , Douglas Robert Anton , Alberto Goenaga , Paul Anthony Sant
CPC分类号： H01L51/0004 , H01L51/0003 , H01L51/0005 , H01L51/0011 , H01L51/0018 , H01L51/5012 , H01L51/56
摘要： There is provided a process for forming a contained second layer over a first layer, including the steps: forming the first layer having a first surface energy; treating the first layer with a reactive surface-active composition to form a treated first layer having a second surface energy which is lower than the first surface energy; exposing the treated first layer with radiation; and forming the second layer. There is also provided an organic electronic device made by the process.
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