Method for extracting impurities using ionic liquids
    2.
    发明授权
    Method for extracting impurities using ionic liquids 失效
    使用离子液体提取杂质的方法

    公开(公告)号:US07605297B2

    公开(公告)日:2009-10-20

    申请号:US10565187

    申请日:2004-07-03

    IPC分类号: A62D3/36

    CPC分类号: C07B63/00 Y02P20/542

    摘要: The invention relates to a process for the extractive removal of phenols, alcohols, amines, phoshines, hydroxylamines, hydrazines, oximes, imines, water, carboxylic acids, amino acids, hydroxamic acids, sulfinic acids, sulfonic acids, peroxycarboxylic acids, phosphonous acids, phosphinous acids, phosphonic acids, phosphinic acids or phosphoric acids from aprotic solvents by means of ionic liquids of the formula [K]n+[A]n−, where n, [K]+ and An− are defined as in the description.

    摘要翻译: 本发明涉及一种用于萃取去除酚,醇,胺,磷,羟胺,肼,肟,亚胺,水,羧酸,氨基酸,异羟肟酸,亚磺酸,磺酸,过氧羧酸,膦酸, 通过式[K] n + [A] n-,其中n,[K] +和An-的离子液体由非质子传递溶剂中的膦酸,次膦酸或次膦酸或磷酸定义如说明书中所定义。

    Method of preparing ionic liquids
    4.
    发明申请
    Method of preparing ionic liquids 失效
    离子液体的制备方法

    公开(公告)号:US20070142646A1

    公开(公告)日:2007-06-21

    申请号:US10587248

    申请日:2005-01-26

    IPC分类号: C07D233/02 C07D213/06

    CPC分类号: C07D233/56

    摘要: In the process for preparing ionic liquids, an ionic liquid is firstly reacted with an alkoxide or with barium hydroxide and is subsequently neutralized with an acid. The ionic liquid contains a phosphonium and/or ammonium cation and an anion selected from the group consisting of halides, arylsulfonates, alkylsulfonates, sulfate, hydroxysulfate, alkylsulfates, hydrogencarbonate, carbonate. triflate and carboxylates. In this process, virtually any anions can be introduced into the ionic liquids.

    摘要翻译: 在制备离子液体的过程中,首先使离子液体与醇盐或氢氧化钡反应,随后用酸中和。 离子液体含有鏻和/或铵阳离子和选自卤化物,芳基磺酸盐,烷基磺酸盐,硫酸盐,羟基硫酸盐,烷基硫酸盐,碳酸氢盐,碳酸盐的阴离子。 三氟甲磺酸酯和羧酸盐。 在这个过程中,几乎可以将任何阴离子引入到离子液体中。

    Method for producing n-phosphonomethyl iminodiacetic acid
    5.
    发明授权
    Method for producing n-phosphonomethyl iminodiacetic acid 失效
    n-膦酰基甲基亚氨基二乙酸的制备方法

    公开(公告)号:US07084298B2

    公开(公告)日:2006-08-01

    申请号:US10451740

    申请日:2002-01-11

    IPC分类号: C07F9/22 C07F9/28

    CPC分类号: C07F9/3808

    摘要: The present invention relates to a process for the preparation of N-phosphonomethyliminodiacetic acid by reacting an alkali metal salt of iminodiacetic acid with phosphorus trichloride in aqueous solution with formation of the hydrochloride of iminodiacetic acid, phosphorous acid and of the corresponding alkali metal chloride, followed by reaction with a formaldehyde source and, if desired, recovery of the N-phosphonomethyliminodiacetic acid from the reaction mixture, in which water, which may comprise HCl, is removed from the reaction mixture during and/or after reacting the alkali metal salt of iminodiacetic acid with phosphorus trichloride until the concentration of iminodiacetic acid hydrochloride is at least 40% by weight, based on the weight of the reaction mixture minus the weight of alkali metal chloride.The process makes possible the preparation of N-phosphonomethyliminodiacetic acid in a simple fashion and in high yield.

    摘要翻译: 本发明涉及一种通过将亚氨基二乙酸的碱金属盐与三氯化磷在水溶液中反应制备N-膦酰甲基亚氨基二乙酸的方法,形成亚氨基二乙酸,亚磷酸和相应的碱金属氯化物的盐酸盐,随后 通过与甲醛源反应,并且如果需要,从反应混合物中回收N-膦酰甲基亚氨基二乙酸,其中可以包含HCl的水在反应混合物中和/或之后反应亚氨基二乙酸的碱金属盐 酸与三氯化磷直到亚氨基二乙酸盐酸盐的浓度为至少40重量%,基于反应混合物的重量减去碱金属氯化物的重量。 该方法可以以简单的方式以高产率制备N-膦酰基甲基亚氨基二乙酸。

    CATALYST FOR CURING EPOXIDES
    9.
    发明申请
    CATALYST FOR CURING EPOXIDES 有权
    用于固化环氧化物的催化剂

    公开(公告)号:US20100179299A1

    公开(公告)日:2010-07-15

    申请号:US12602724

    申请日:2008-06-06

    IPC分类号: C08G59/68

    CPC分类号: C08G59/686

    摘要: The use of 1,3-substituted imidazolium salts of the formula I in which R1 and R3 independently of one another are an organic radical having 1 to 20 C atoms, R2, R4, and R5 independently of one another are an H atom or an organic radical having 1 to 20 C atoms, it also being possible for R4 and R5 together to form an aliphatic or aromatic ring, and X is a thiocyanate anion as latent catalysts for curing compositions comprising epoxy compounds.

    摘要翻译: 其中R 1和R 3彼此独立地是具有1至20个C原子的有机基团,R 2,R 4和R 5彼此独立的式I的1,3-取代咪唑盐是H原子或 具有1至20个C原子的有机基团,R4和R5一起形成脂族或芳族环,X是硫氰酸根阴离子作为用于固化包含环氧化合物的组合物的潜在催化剂。