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1.发明申请Method for the hyperpolarisation of atomic nuclei and device for carrying out said method 失效用于实现所述方法的原子核的超极化方法和装置公开(公告)号：US20070080684A1
公开(公告)日：2007-04-12
申请号：US10586000
申请日：2005-01-13
CPC分类号： G01R33/282 , A61K49/1815
摘要： The invention relates to a method for the hyperpolarisation of atomic nuclei by means of optical pumps in a sample cell. Polarisation of an electron spin of an optically pumpable species, which is produced by means of laser light, is transferred to the nucleus spin of an atom which is to be hyperpolarisied. According to the invention, components of the mixture and/or other inert compounds for hyperpolarisation are guided in the sample cell such that the mixture does not come into contact with the inner wall of the sample cell, or does to a small degree. A device for carrying out said method comprises at least one means which guides the components of the mixture of non-optical pumpable species and nuclei which are to be hyperpolarisied, and/or other inert compounds for hyperpolarisation, into the sample cell (5) such that the mixture does not come into contact with the inner wall of the sample cell (5), or does to small degree. As a result, the wall can be prevented from sagging.
摘要翻译： 本发明涉及通过样品池中的光泵对原子核进行超极化的方法。 通过激光产生的可光泵浦物质的电子自旋的极化被转移到要超极化的原子的核心旋转。 根据本发明，用于超极化的混合物和/或其它惰性化合物的组分在样品池中引导，使得混合物不与样品池的内壁接触，或者在很小程度上。 用于执行所述方法的装置包括至少一个装置，其将非光可泵送物质的混合物的组分和要超极化的核的组分和/或用于超极化的其它惰性化合物引导到样品池（5）中， 混合物不与样品池（5）的内壁接触，或者具有很小的程度。 结果，可以防止墙下垂。
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2.发明授权公开(公告)号：US07495435B2
公开(公告)日：2009-02-24
申请号：US10586000
申请日：2005-01-13
IPC分类号： G01V3/00
CPC分类号： G01R33/282 , A61K49/1815
摘要： An apparatus for hyperpolarizing atomic nuclei through optical pumping has a cylindrical optical pumping cell having an inlet and an outlet spaced therefrom. A supply of a mixture of optically pumpable species and hyperpolarizable nuclei is connected to the inlet of the cell. A nozzle at an inlet of the optical pumping cell forms and injects a jet flow of the mixture into the optical pumping cell. It is then drawn out through the outlet such that the mixture touches the inner walls of the optical pumping cell only adjacent the outlet.
摘要翻译： 通过光泵浦使原子核超极化的装置具有圆柱形的光泵浦单元，其具有与其间隔开的入口和出口。 供应光泵浦物质和超极化核的混合物连接到电池入口。 在光泵浦单元的入口处的喷嘴形成并将混合物的喷射流注入到光泵浦单元中。 然后通过出口将其抽出，使得混合物仅在出口附近接触光泵浦单元的内壁。
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公开(公告)号：US07221448B1
公开(公告)日：2007-05-22
申请号：US10018765
申请日：2000-06-07
CPC分类号： G01N21/05 , G01R33/282 , Y10T436/116664
摘要： The invention relates to a sample cell with a glass body comprising a gas inlet and a gas outlet and at least one orifice, a plane glass window is fused into the orifice, the shape and size of the window corresponds to the shape and size of the orifice, the orifice is limited by a rim, the rim is wider than the thickness of the window, the rim of the window is fused with the rim of the orifice.The invention further relates to a method of producing the sample cell. The window is inserted into the orifice. The rim of the orifice is heated several times from the exterior in such a way that the glass melts and a fused joint is formed between the window and the rim of the orifice.The sample cell produced by the method has a particularly rigid joint between the window and the glass body. Therefore, this glass cell is able to withstand pressures above 10 bar and allows the passage of light without lens effects owing to its plane-parallel windows.The sample cell is used in a polarizer for inert gas.
摘要翻译： 本发明涉及一种具有玻璃体的样品池，该玻璃体包括气体入口和气体出口以及至少一个孔口，平面玻璃窗口被熔化到孔中，窗口的形状和尺寸对应于 孔口由边缘限制，边缘比窗口的厚度更宽，窗口的边缘与孔口的边缘熔合。 本发明还涉及一种生产样品池的方法。 窗口插入孔中。 孔的边缘从外部被加热几次，使得玻璃熔化并且在窗口和孔的边缘之间形成熔接接头。 通过该方法制造的样品池在窗口和玻璃体之间具有特别刚性的接头。 因此，这种玻璃电池能够承受10巴以上的压力，并且由于其平面平行的窗口而允许通过光而没有透镜效应。 样品池用于惰性气体的偏振器。
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4.发明申请Method for determining phase distribution coefficients, in addition to a corresponding device 审中-公开用于确定相位分布系数的方法，以及相应的装置公开(公告)号：US20050074366A1
公开(公告)日：2005-04-07
申请号：US10499746
申请日：2002-12-12
IPC分类号： G01N1/22 , G01N1/10 , G01N1/28 , G01N1/34 , G01N1/40 , G01N25/14 , G01N30/04 , G01N30/88 , G01N33/00
CPC分类号： G01N1/40 , G01N1/405 , G01N25/14 , G01N2001/4066
摘要： The invention relates to a method for determining phase distribution coefficients of substances for the solid/gas and liquid/gas compartments. According to the invention, a gas that has been pre-treated with active charcoal is fed through a housing (1), in which a sample has been provided. If the sample is a solid, the gas enters through openings in a shaft (11), which traverses the housing (1) and is equipped with propellers. If the sample is a liquid, the gas enters through a separate opening (8a, b, c) and the surface area of the liquid is increased by a rotating cylinder (9). The gas emerges from the housing (1) and traverses an adsorption tube, which is subjected to thermodesorption after the experiment. The substance released by said thermodesorption is subjected to a quantitative analysis.
摘要翻译： 本发明涉及一种确定固体/气体和液体/气体隔室物质相分布系数的方法。 根据本发明，已经用活性炭预处理的气体通过其中已经提供样品的壳体（1）进料。 如果样品是固体，则气体通过穿过壳体（1）并且配备有螺旋桨的轴（11）中的开口进入。 如果样品是液体，则气体通过单独的开口（8a，b，c）进入，并且通过旋转圆筒（9）增加液体的表面积。 气体从壳体（1）出来，穿过吸附管，实验后进行热解吸。 通过所述热释放释放的物质进行定量分析。
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