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    Cyclic acetals of 2-methyl-2-pentenal and food flavor uses thereof
    1.
    发明授权
    Cyclic acetals of 2-methyl-2-pentenal and food flavor uses thereof 失效
    2-甲基-2-戊烯醛的环状缩醛和食品香料的用途

    公开(公告)号：US4198393A

    公开(公告)日：1980-04-15

    申请号：US19927

    申请日：1979-03-12

    申请人： Takao Yoshida ,  Manfred H. Vock

    发明人： Takao Yoshida ,  Manfred H. Vock

    IPC分类号： A23G4/00 ,  A23G4/06 ,  A23L27/20 ,  A61K8/49 ,  A61K31/335 ,  A61Q11/00 ,  C07D317/12 ,  A61K7/16

    CPC分类号： C07D317/12 ,  A23G4/06 ,  A23L27/2052 ,  A61K8/4973 ,  A61Q11/00

    摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuffs, chewing gum, toothpaste and medicinal product aroma imparting materials of cyclic acetals of 2-methyl-2-pentenal having the generic structure: ##STR1## wherein R represents either hydrogen or methyl and the wavy lines signify that the cyclic acetal moiety is in either a "cis" or "trans" configuration with respect to the ethyl moiety bonded to the ethylenic moiety of the molecule. Addition of one or more cyclic acetals of 2-methyl-2-pentenal to foodstuffs, chewing gums, toothpastes and/or medicinal products produces sweet, fruity, gooseberry, green, aniseed, licorice, floral and herbal aroma characteristics and sweet, fruity, gooseberry, green, spearmint-like, aniseed, licorice, floral and herbal flavor characteristics with albedo-like flavor nuances.

    摘要翻译： 本发明描述了用于食品，口香糖，牙膏和药用香料以及香气增强，改性，增强和赋予组合物的食品，口香糖，牙膏和赋予2-甲基环状缩醛的药用香料赋予材料的方法和组合物 -2-戊烯醛，其具有以下通用结构：其中R表示氢或甲基，波浪线表示环状缩醛部分相对于键合到的乙基部分为“顺式”或“反式”构型 分子的烯属部分。 将一种或多种2-甲基-2-戊烯醛的环状缩醛添加到食品，口香糖，牙膏和/或药用产品中，产生甜味，果香，醋栗，绿色，茴香，甘草，花香和草本香气特征，甜美，果香， 醋栗，绿色，薄荷状，大茴香，甘草，花卉和草药风味特征与反照率一样的风味细微差别。

    Cyclic acetals of 2-methyl-2-pentenal and food flavor uses thereof
    2.
    发明授权
    Cyclic acetals of 2-methyl-2-pentenal and food flavor uses thereof 失效
    2-甲基-2-戊烯醛的环状缩醛和食品香料的用途

    公开(公告)号：US4289700A

    公开(公告)日：1981-09-15

    申请号：US827253

    申请日：1977-08-24

    申请人： Takao Yoshida ,  Manfred H. Vock

    发明人： Takao Yoshida ,  Manfred H. Vock

    IPC分类号： A23G4/00 ,  A23G4/06 ,  A23L27/20 ,  A61K8/49 ,  A61Q11/00 ,  C07D317/12 ,  C07D317/10

    CPC分类号： C07D317/12 ,  A23G4/06 ,  A23L27/2052 ,  A61K8/4973 ,  A61Q11/00

    摘要： Processes and compositions are described for the use in foodstuffs, chewing gum, toothpaste and medicinal product flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste and medicinal product aroma imparting materials of cylic acetals of 2-methyl-2-pentenal having the generic structure: ##STR1## wherein R represents either hydrogen or methyl and the wavy lines signify that the cyclic acetal moiety is in either a "cis" or "trans" configuration with respect to the ethyl moiety bonded to the ethylenic moiety of the molecule. Addition of one or more cyclic acetals of 2-methyl-2-pentenal to foodstuffs, chewing gums, toothpastes and/or medicinal products produces sweet, fruity, gooseberry, green, aniseed, licorice, floral and herbal aroma characteristics and sweet, fruity, gooseberry, green, spearmint-like, aniseed, licorice, floral and herbal flavor characteristics with albedo-like flavor nuances.

    摘要翻译： 描述的方法和组合物用于食品，口香糖，牙膏和药用产品香料和香气增强，改性，增强和赋予组合物以及作为食品，口香糖，牙膏和药用香料赋予2-甲基乙缩醛的材料 -2-戊烯醛，其具有以下通用结构：其中R表示氢或甲基，波浪线表示环状缩醛部分相对于键合到的乙基部分为“顺式”或“反式”构型 分子的烯属部分。 将一种或多种2-甲基-2-戊烯醛的环状缩醛添加到食品，口香糖，牙膏和/或药用产品中，产生甜味，果香，醋栗，绿色，茴香，甘草，花香和草本香气特征，甜味，果香， 醋栗，绿色，薄荷状，大茴香，甘草，花卉和草药风味特征与反照率一样的风味细微差别。

    Flavoring with cyclic acetals of 2-methyl-2-pentenal
    3.
    发明授权
    Flavoring with cyclic acetals of 2-methyl-2-pentenal 失效
    用2-甲基-2-戊烯醛的环状缩醛调味

    公开(公告)号：US4159347A

    公开(公告)日：1979-06-26

    申请号：US939911

    申请日：1978-09-05

    申请人： Takao Yoshida ,  Manfred H. Vock

    发明人： Takao Yoshida ,  Manfred H. Vock

    IPC分类号： A23G4/00 ,  A23G4/06 ,  A23L27/20 ,  A61K8/49 ,  A61Q11/00 ,  C07D317/12 ,  A23L1/226

    CPC分类号： C07D317/12 ,  A23G4/06 ,  A23L27/2052 ,  A61K8/4973 ,  A61Q11/00

    摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma augmenting, modifying, enhancing and imparting compositions and as foodstuff, chewing gum, toothpaste and medicinal product aroma imparting materials of cyclic acetals of 2-methyl-2-pentenal having the generic structure: ##STR1## wherein R represents either hydrogen or methyl and the wavy lines signify that the cyclic acetal moiety is in either a "cis" or "trans" configuration with respect to the ethyl moiety bonded to the ethylenic moiety of the molecule. Addition of one or more cyclic acetals of 2-methyl-2-pentenal to foodstuffs, chewing gums, toothpastes and/or medicinal products produces sweet, fruity, gooseberry, green, aniseed, licorice, floral and herbal aroma characteristics and sweet, fruity, gooseberry, green, spearmint-like, aniseed, licorice, floral and herbal flavor characteristics with albedo-like flavor nuances.

    摘要翻译： 描述了用于食品，口香糖，牙膏和药用产品风味和香气增强，改性，增强和赋予组合物以及作为食品，口香糖，牙膏和药用香料赋予材料的方法和组合物，其中2-甲基的环状缩醛 -2-戊烯醛，其具有以下通用结构：其中R表示氢或甲基，波浪线表示环状缩醛部分相对于键合到乙基的乙基部分为“顺式”或“反式”构型 分子的烯属部分。 将一种或多种2-甲基-2-戊烯醛的环状缩醛添加到食品，口香糖，牙膏和/或药用产品中，产生甜味，果香，醋栗，绿色，茴香，甘草，花香和草本香气特征，甜味，果香， 醋栗，绿色，薄荷状，大茴香，甘草，花卉和草药风味特征与反照率一样的风味细微差别。

    Process for preparing compositions containing unsaturated lactones, products produced thereby and organoleptic uses of said products
    4.
    发明授权
    Process for preparing compositions containing unsaturated lactones, products produced thereby and organoleptic uses of said products 失效
    制备含有不饱和内酯的组合物，由此生产的产品和所述产品的感官用途的方法

    公开(公告)号：US4946782A

    公开(公告)日：1990-08-07

    申请号：US228512

    申请日：1988-08-05

    申请人： Mohamad I. Farbood ,  James A. Morris ,  Mark A. Sprecker ,  Lynda J. Bienkowski ,  Kevin P. Miller ,  Manfred H. Vock ,  Myrna L. Hagedorn

    发明人： Mohamad I. Farbood ,  James A. Morris ,  Mark A. Sprecker ,  Lynda J. Bienkowski ,  Kevin P. Miller ,  Manfred H. Vock ,  Myrna L. Hagedorn

    IPC分类号： A24B15/40 ,  C11B9/00 ,  C12P7/40 ,  C12P7/42 ,  C12P17/02

    CPC分类号： C12P17/02 ,  A24B15/403 ,  C11B9/0073 ,  C12P7/40 ,  C12P7/42

    摘要： Described is a process for the preparation of compositions of matter containing unsaturated lactones defined according to the generic structure: ##STR1## wherein R represents C.sub.6 alkyl or alkenyl; and X represents C.sub.2, C.sub.4 or C.sub.6 alkylene or alkenylene; with the provisos that R is C.sub.6 alkyl when X is alkenylene and R is C.sub.6 alkenyl when X is alkylene by means of the sequential steps of (i) fermentation of castor oil or ricinoleic acid using a microorganism selected from the group consisting of:Candida petrophilum, ATCC 20226;Candida oleophila, ATCC 20177;Candida sp., ATCC 20504; andCandida sake, ATCC 28137whereby gamma hydroxydecanoic acid and a mixture of other acids defined according to the generic structure: ##STR2## is formed wherein Y represents an oxo-saturated, oxo-unsaturated or di-unsaturated C.sub.9, C.sub.11 or C.sub.13 moiety according to the reaction: ##STR3## (ii) lactonization of the resulting gamma hydroxydecanoic acid by means of simultaneous acidification and heating according to the reaction: ##STR4## and (iii) lactonization (via distillation) of one or more of the resulting acids defined according to the structure: ##STR5## to form one or more lactones defined according to the generic structure: ##STR6## according to the reaction: ##STR7## wherein the sum of the number of carbon atoms in the X moiety and in the R moiety is equal to the number of carbon atoms in the Y moiety minus 1.Also described are the products produced according to such process as well as their organoleptic utilities for augmenting or enhancing the aroma or taste of consumable materials selected from the group consisting of perfume compositions, colognes, perfumed articles, foodstuffs, chewing gums, medicinal products, toothpastes, chewing tobaccos and smoking tobaccos.

    摘要翻译： 描述了根据通用结构定义的含有不饱和内酯的物质组合物的方法：其中R表示C6烷基或烯基; X表示C2，C4或C6亚烷基或亚烯基; 条件是当X是亚烯基时R是C6烷基，当X是亚烷基时，R是C6链烯基，通过以下顺序的步骤：（i）使用选自以下的微生物来蓖麻油或蓖麻油酸发酵：念珠菌 ，ATCC 20226; 嗜油假丝酵母，ATCC 20177; 念珠菌属，ATCC 20504; 和念珠菌，ATCC 28137，由此形成根据通用结构定义的γ-羟基癸酸和其它酸的混合物：其中Y表示氧代饱和的，不饱和的或不饱和的C 9，C 11或C 13部分，根据 （ii）通过根据以下反应的同时酸化和加热来对所得的γ-羟基癸酸进行内酯化：（ⅲ）内酯化（经蒸馏） 根据以下结构定义的一种或多种所得酸：以形成根据通用结构定义的一种或多种内酯：根据该反应：其中，碳原子数 X部分和R部分等于Y部分中的碳原子数减1。还描述了根据这种方法产生的产物以及它们的感官效用，用于增强或增强co的香气或味道 选自香水组合物，古龙水，香料制品，食品，口香糖，药用产品，牙膏，咀嚼烟草和吸烟烟草的可选材料。