公开(公告)号：US06848501B2

公开(公告)日：2005-02-01

申请号：US10356428

申请日：2003-01-31

申请人： Harunori Hirao ,  Yukihiro Matsumoto ,  Sei Nakahara ,  Osamu Dodo ,  Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Kazuhiko Sakamoto ,  Hiroo Iwato

发明人： Harunori Hirao ,  Yukihiro Matsumoto ,  Sei Nakahara ,  Osamu Dodo ,  Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Kazuhiko Sakamoto ,  Hiroo Iwato

IPC分类号： B01J19/00 ,  F28D7/16 ,  F28D9/00 ,  F28F19/00 ,  F28F27/02

CPC分类号： F28D9/0068 ,  B01J19/002 ,  B01J2219/00252 ,  F28D7/1607 ,  F28D7/1623 ,  F28D9/0062 ,  F28F9/0278 ,  F28F19/00 ,  F28F2250/102

摘要： In an apparatus provided with a plate type heat exchanger as a heater and/or a cooler and operated to treat a gas containing an easily blocking substance, a method for preventing the plate type heat exchanger from being blocked is disclosed which is characterized by i) setting the width of a flow path on a plate of the plate type heat exchanger in the apparatus in a range of 6-25 mm and ii) setting the average flow rate of the gas passing the plate type heat exchanger in the apparatus per unit cross-sectional area of the flow path on the plate in the range of 3-15 m/s. In the exchange of heat of an easily blocking substance by the use of a plate type heat exchanger, a method for preventing the plate type heat exchanger from blockage is disclosed which has the plate type heat exchanger provided in the port for introducing a gas containing an easily blocking substance with a gas dispersion plate. This invention, in the heat exchange of an effluent gas emanating from a process for the production of (meth)acrylic acid or an ester thereof or the disposal of the gas, significantly allays blockage of the interior of the plate type heat exchanger.

摘要翻译： 在设置有作为加热器和/或冷却器的板式热交换器并且被操作以处理含有易阻塞物质的气体的装置中，公开了一种防止板式热交换器被堵塞的方法，其特征在于i） 将设备中板式热交换器的板上的流路宽度设置在6-25mm的范围内，以及ii）将通过板式热交换器的气体的平均流量设置在每单位十字的装置中 板上流路的截面面积在3-15 m / s的范围内。 在通过使用板式热交换器交换容易堵塞物质的热的情况下，公开了一种防止板式热交换器堵塞的方法，其具有设置在用于引入含有 用气体分散板容易地堵塞物质。 本发明在从（甲基）丙烯酸或其酯的制备方法产生的流出气体的热交换或气体的处理中显着地阻止了板式热交换器的内部堵塞。

公开(公告)号：US06382313B2

公开(公告)日：2002-05-07

申请号：US09792469

申请日：2001-02-23

申请人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Kazuhiko Sakamoto ,  Hiroo Iwato

发明人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Kazuhiko Sakamoto ,  Hiroo Iwato

IPC分类号： F28D700

CPC分类号： F28F9/0278 ,  B01J19/002 ,  B01J2219/00252 ,  F28D7/1607 ,  F28D7/1623

摘要： A heat exchanger for an easily polymerizing substance-containing gas provided with a shell possessed of a heat-exchanging gas inlet and a heat-exchanging gas outlet and a heat-exchanging part adapted to circulate fluid introduced from outside the shell between the gas inlet and said gas outlet, which heat exchanger is characterized by being provided with a gas distributing plate between the gas inlet and the heat-exchanging part. The heat exchanger is characterized by the gas distributing plate having a cross-sectional area in the range of 1.0-10.0 times the cross-section of the gas inlet. When an easily polymerizing substance-containing gas contacts a structure, the gas is condensed on the contact surface of the structure and suffered to generate a polymer. According to the heat exchanger of this invention, by uniformly distributing a gas in the heat-exchanging part, it is made possible to attain uniform distribution of heat, depress the possible condensation of the gas, and prevent the easily polymerizing substance from succumbing to polymerization.

摘要翻译： 一种用于容易聚合的含物质气体的热交换器，其具有壳体，该壳体具有热交换气体入口和热交换气体出口，以及热交换部分，其适于使从壳体外部引入的流体在气体入口和 所述气体出口，其特征在于在气体入口和热交换部分之间设置有气体分配板。 热交换器的特征在于气体分布板的横截面积在气体入口横截面的1.0-10.0倍的范围内。 当容易聚合的物质的气体接触结构时，气体在结构的接触表面上被冷凝，并产生聚合物。 根据本发明的热交换器，通过在热交换部中均匀分布气体，可以获得均匀的热分布，抑制气体的可能的冷凝，并且防止容易聚合的物质屈服于聚合 。

公开(公告)号：US07048834B2

公开(公告)日：2006-05-23

申请号：US09745896

申请日：2000-12-21

申请人： Yoshitake Ishii ,  Kouji Ueno ,  Kazuhiko Sakamoto ,  Sei Nakahara ,  Masatoshi Ueoka ,  Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Mamoru Takamura ,  Hisao Nakama

发明人： Yoshitake Ishii ,  Kouji Ueno ,  Kazuhiko Sakamoto ,  Sei Nakahara ,  Masatoshi Ueoka ,  Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Mamoru Takamura ,  Hisao Nakama

IPC分类号： B01D3/34 ,  B01D3/42 ,  C07C51/44 ,  C07C51/487 ,  C07C57/07

CPC分类号： C07C51/44 ,  C07C51/487 ,  C07C57/04

摘要： The present invention provides an industrially easy and economical method for purification of acrylic acid which enables to efficiently eliminate impurities from a crude acrylic acid containing aldehydes as the impurities while the formation of acrylic acid polymer is inhibited. The method for purification of acrylic acid includes the step of distilling a crude acrylic acid which is charged with an aldehyde treatment chemical, wherein the concentration ratio of furfural to acrolein by weight in the crude acrylic acid is adjusted so as to satisfy the following equation: (furfural concentration by weight)/(acrolein concentration by weight)≦100.

摘要翻译： 本发明提供了一种工业上容易和经济的丙烯酸纯化方法，其能够在抑制丙烯酸聚合物形成的同时，有效地除去含粗醛的丙烯酸作为杂质的杂质。 纯化丙烯酸的方法包括蒸馏装入醛处理化学品的粗丙烯酸的步骤，其中调整粗丙烯酸中的糠醛与丙烯醛的重量比，以满足下列等式： （糠醛浓度按重量计）/（丙烯醛浓度重量）<= 100。<？in-line-formula description =“In-line formula”end =“lead” “公式”end =“tail”？>

公开(公告)号：US06831195B2

公开(公告)日：2004-12-14

申请号：US10224677

申请日：2002-08-21

申请人： Takeshi Nishimura ,  Tetsuji Mitsumoto ,  Kazuhiko Sakamoto ,  Hidefumi Haramaki

发明人： Takeshi Nishimura ,  Tetsuji Mitsumoto ,  Kazuhiko Sakamoto ,  Hidefumi Haramaki

IPC分类号： C07C2710

CPC分类号： F01K3/188 ,  C07C51/252 ,  C07C67/08 ,  F01K3/185 ,  C07C57/04 ,  C07C69/54

摘要： A method for producing an organic acid and/or an organic acid ester which utilizes a steam system permitting stable production of an organic acid and/or an organic acid ester and realizing a high thermal efficiency constantly relative to the waste heat generated in the process of the production is provided. More particularly, this invention concerns a method for the production of an organic acid and/or an organic acid ester, wherein heat generated in the process for producing an organic acid and/or an organic acid ester is recovered in the form of steam, and the steam is used in any of the following forms: {circle around (1)} thermal energy, {circle around (2)} dynamic energy, and {circle around (3)} electrical energy in the process for producing an organic acid and/or an organic acid ester.

摘要翻译： 一种生产有机酸和/或有机酸酯的方法，其利用允许有机酸和/或有机酸酯稳定生产的蒸汽系统，并相对于在 提供生产。 更具体地说，本发明涉及生产有机酸和/或有机酸酯的方法，其中在生产有机酸和/或有机酸酯的方法中产生的热量以蒸汽的形式回收， 蒸汽以下列任何一种形式使用：{围绕（1个热能，{围绕（2个动态能量）和{围绕周围（在产生有机酸和/或有机酸酯的方法中为3个电能 。

公开(公告)号：US07147048B2

公开(公告)日：2006-12-12

申请号：US10254379

申请日：2002-09-25

申请人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Osamu Dodo

发明人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Osamu Dodo

IPC分类号： F28D7/10 ,  F28D7/00 ,  F28F9/02 ,  C07C51/16

CPC分类号： B01J8/067 ,  B01J2208/0015 ,  F28D7/1615 ,  F28F9/22 ,  F28F2009/029 ,  F28F2009/224

摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.

公开(公告)号：US06657079B1

公开(公告)日：2003-12-02

申请号：US09640630

申请日：2000-08-17

申请人： Tetsuji Mitsumoto ,  Tatsuaki Yoshimura ,  Takeshi Nishimura ,  Sei Nakahara

发明人： Tetsuji Mitsumoto ,  Tatsuaki Yoshimura ,  Takeshi Nishimura ,  Sei Nakahara

IPC分类号： C07C4534

CPC分类号： C07C45/35 ,  C07C45/33 ,  C07C47/22

摘要： A method for mixing a plurality of gases including forming a helical flow within a mixing vessel thereby allowing simplification of construction, avoiding pressure drop to the fullest possible extent, and expediting the mixture lest the volume of a gas within the explosion limits should increase, and an apparatus to be used for the method.

摘要翻译： 一种用于混合多种气体的方法，包括在混合容器内形成螺旋流，从而允许简化构造，避免压力下降到最大可能程度，并加速混合物，以免爆炸极限内的气体体积增加， 用于该方法的装置。

公开(公告)号：US07326811B2

公开(公告)日：2008-02-05

申请号：US11584233

申请日：2006-10-20

申请人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Osamu Dodo

发明人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Osamu Dodo

IPC分类号： C07C51/42 ,  C07C51/16

CPC分类号： B01J8/067 ,  B01J2208/0015 ,  F28D7/1615 ,  F28F9/22 ,  F28F2009/029 ,  F28F2009/224

摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.

摘要翻译： 公开了一种能够获得壳侧流体的均匀流动分布并且基本上消除了对壳体侧面的结构限制的壳体管式热交换器，其具有热交换所需的尽可能小的长度。 这种管壳型热交换器设置有一个环形导管，其具有不少于两个隔板，同时用作用于引入和排出壳侧流体的膨胀接头，并且允许将所述壳侧流体的流动路径分离成 引入部分和排出部分，并且包括在用于所述壳侧流体的流动路径中不具有热传递管阵列的位置。 它防止了由于壳体侧面的结构限制而使设备不必要地增大，并且使得壳侧流体能够产生均匀的流动。

公开(公告)号：US07282118B2

公开(公告)日：2007-10-16

申请号：US09828093

申请日：2001-04-06

申请人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Hidefumi Haramaki

发明人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Hidefumi Haramaki

IPC分类号： B01D3/32 ,  C07C51/42

CPC分类号： B01D3/225 ,  B01D3/326 ,  Y10S203/11

摘要： This invention resides in providing a method for the prevention of possible polymerization of the easily polymerizable substance during the purification thereof by a column provided with (a) at least one tray directly fixed to a support ring with a bolt and a nut and/or (b) at least one tray fixed to a support ring with a vertical clamp or a distillation column provided in the lower part thereof with a splash collision plate.

摘要翻译： 本发明在于提供一种防止易于聚合的物质在其净化过程中可能的聚合的方法，所述塔具有（a）至少一个直接用螺栓和螺母固定在支撑环上的托盘和/或（ b）至少一个托架，其具有垂直夹具或蒸馏塔固定在支撑环上，该塔板在其下部设有飞溅碰撞板。

公开(公告)号：US20070034363A1

公开(公告)日：2007-02-15

申请号：US11584233

申请日：2006-10-20

申请人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Osamu Dodo

发明人： Tetsuji Mitsumoto ,  Takeshi Nishimura ,  Sei Nakahara ,  Osamu Dodo

IPC分类号： F28F9/22

CPC分类号： B01J8/067 ,  B01J2208/0015 ,  F28D7/1615 ,  F28F9/22 ,  F28F2009/029 ,  F28F2009/224

摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.

摘要翻译： 公开了一种能够获得壳侧流体的均匀流动分布并且基本上消除了对壳体侧面的结构限制的壳体管式热交换器，其具有热交换所需的尽可能小的长度。 这种管壳型热交换器设置有一个环形导管，其具有不少于两个隔板，同时用作用于引入和排出壳侧流体的膨胀接头，并且允许将所述壳侧流体的流动路径分离成 引入部分和排出部分，并且包括在用于所述壳侧流体的流动路径中不具有热传递管阵列的位置。 它防止了由于壳体侧面的结构限制而使设备不必要地增大，并且使得壳侧流体能够产生均匀的流动。

公开(公告)号：US06642414B2

公开(公告)日：2003-11-04

申请号：US09772458

申请日：2001-01-30

申请人： Tetsuji Mitsumoto ,  Yukihiro Matsumoto ,  Sei Nakahara ,  Tatsuaki Yoshimura

发明人： Tetsuji Mitsumoto ,  Yukihiro Matsumoto ,  Sei Nakahara ,  Tatsuaki Yoshimura

IPC分类号： C07C5142

CPC分类号： C07C51/44 ,  C07C51/252 ,  C07C51/48 ,  C07C57/04

摘要： A method for producing (meth)acrylic acid of high purity by repressing formation of a polymer possibly generated during the course of production is disclosed. The production is accomplished by returning the waste liquid generated at the step of the addition of aldehyde treating agents (d) to the step of the absorption (b) and/or the step of separation (c).

摘要翻译： 公开了通过抑制可能在生产过程中产生的聚合物的形成来生产高纯度（甲基）丙烯酸的方法。 通过将在醛加工剂（d）的添加步骤中产生的废液返回到吸收步骤（b）和/或分离步骤（c）中来完成生产。