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    Polymers containing sulphonyl and carboxylic ester groups
    1.
    发明授权
    Polymers containing sulphonyl and carboxylic ester groups 失效
    含有磺酰基和羧酸酯基团的聚合物

    公开(公告)号：US4535139A

    公开(公告)日：1985-08-13

    申请号：US491682

    申请日：1983-05-05

    Applicant: Wolfgang Brauer ,  Siegfried Korte ,  Theo Neukam ,  Carlhans Suling

    Inventor： Wolfgang Brauer ,  Siegfried Korte ,  Theo Neukam ,  Carlhans Suling

    IPC: C08F218/00 ,  C08F20/00 ,  C08F20/38 ,  C08F218/02 ,  C08F220/00 ,  C08F220/04 ,  C08F228/02 ,  C08J5/18 ,  D01F6/38

    CPC classification number: C08F228/02

    Abstract: Polymers obtained by radical polymerization and containing(A) from 0.1 to 80 mole percent of polymerized units corresponding to the following formula ##STR1## in which R.sub.1 represents hydrogen or methyl,R.sub.2 represents alkyl, particularly primary or secondary alkyl containing from 1 to 4 carbon atoms, andR.sub.3 represents hydrogen or alkyl, particularly primary or secondary alkyl containing from 1 to 4 carbon atoms, and in which the sulphonic acid group may be present in the form of a salt, and(B) from 20 to 99.9 mole percent of polymerized units of one or more ethylenically unsaturated monomers, are particularly suitable for the production of filaments, fibres and films having a high absorption capacity for basic dyes.

    Abstract translation: 通过自由基聚合获得的聚合物，其含有（A）0.1至80摩尔％的对应于下式的成像单元（IMAGE），其中R 1表示氢或甲基，R 2表示烷基，特别是含有1至4个碳原子的伯或仲烷基 原子，R 3表示氢或烷基，特别是含有1至4个碳原子的伯或仲烷基，其中磺酸基团可以盐形式存在，（B）20-99.9摩尔％ 一种或多种烯键式不饱和单体的聚合单元特别适用于生产碱性染料具有高吸收能力的长丝，纤维和薄膜。

    Process for the production of polymers containing acrylonitrile
    3.
    发明授权
    Process for the production of polymers containing acrylonitrile 失效
    生产含丙烯腈的聚合物的方法

    公开(公告)号：US4384091A

    公开(公告)日：1983-05-17

    申请号：US310575

    申请日：1981-10-09

    Applicant: Siegfried Korte ,  Theo Neukam ,  Carlhans Suling

    Inventor： Siegfried Korte ,  Theo Neukam ,  Carlhans Suling

    IPC: C08F220/00 ,  C08F2/06 ,  C08F2/18 ,  C08F20/44 ,  C08F220/42

    CPC classification number: C08F20/44

    Abstract: Acrylonitrile polymers and copolymers with good affinity for basic dyes without sulfonic acid groups containing comonomers are obtained by polymerizing at a temperature of from 0.degree. to 60.degree. C. in an aliphatic hydrocarbon having a boiling point of from -10.degree. to 80.degree. C. or in a mixture of aliphatic hydrocarbons having boiling points in the range from -10.degree. to 80.degree. C. using an initiator system comprising from 0.1 to 8.0 mole percent of sulfur dioxide, from 0.1 to 2.0 mole percent of a hydroperoxide which is soluble in the reaction medium and from 0.01 to 1.0 mole percent of an acid which is soluble in the reaction system in that polymerization is carried out continuously and in that an average residence time of from 10 minutes to 2 hours is maintained.

    Abstract translation: 通过在0〜60℃的温度下在沸点为-10〜80℃的脂肪族烃中进行聚合，得到丙烯腈聚合物和对具有不含磺酸基团的共聚单体的碱性染料具有良好亲和性的共聚物。 或者在沸点为-10℃至80℃的脂族烃的混合物中，使用引发剂体系，其包含0.1至8.0摩尔％的二氧化硫，0.1至2.0摩尔％的可溶于 在该聚合反应中可以连续进行反应介质和0.01〜1.0摩尔％的可溶于反应体系的酸，维持10分钟〜2小时的平均停留时间。

    Acrylonitrile polymerization with organic solvent
    4.
    发明授权
    Acrylonitrile polymerization with organic solvent 失效
    丙烯腈与有机溶剂聚合

    公开(公告)号：US4326051A

    公开(公告)日：1982-04-20

    申请号：US170376

    申请日：1980-07-21

    Applicant: Carlhans Suling ,  Siegfried Korte ,  Theo Neukam

    Inventor： Carlhans Suling ,  Siegfried Korte ,  Theo Neukam

    IPC: C08F20/44 ,  C08F2/06 ,  C08F22/30

    CPC classification number: C08F20/44

    Abstract: The invention relates to a homopolymer or copolymer of acrylonitrile which comprises from 0 to 30% by weight, incorporated by polymerization, of comonomer units which are free from ionic groups, said polymers having a K-value of from 50 to 100, a dye absorption capacity for cationic dyes of at least 0.5% by weight, a conductivity, measured in dimethylformamide solution, of at least 10.mu. Siemens, and from 0.2 to 1.5% by weight of sulphur fixed to said polymer as well as to a process for the production thereof.

    Abstract translation: 本发明涉及丙烯腈的均聚物或共聚物，其包含0-30重量％，通过聚合引入，不含离子基团的共聚单体单元，所述聚合物的K值为50至100，染料吸收 阳离子染料的能力为至少0.5重量％，在二甲基甲酰胺溶液中测量的至少10微米西门子的电导率和0.2至1.5重量％的固定在所述聚合物上的硫以及生产方法 其中。

    Acrylonitrile polymerization in fluorinated hydrocarbons
    5.
    发明授权
    Acrylonitrile polymerization in fluorinated hydrocarbons 失效
    氟化烃中的丙烯腈聚合

    公开(公告)号：US4255546A

    公开(公告)日：1981-03-10

    申请号：US077460

    申请日：1979-09-20

    Applicant: Carlhans Suling ,  Siegfried Korte ,  Theo Neukam

    Inventor： Carlhans Suling ,  Siegfried Korte ,  Theo Neukam

    IPC: C08F2/00 ,  C08F2/04 ,  C08F2/06 ,  C08F4/00 ,  C08F4/40 ,  C08F20/00 ,  C08F20/44

    CPC classification number: C08F20/44

    Abstract: The invention relates to a process for the production of polyacrylonitrile or acrylonitrile copolymers, the polymerization being carried out at a temperature of from -40.degree. to +60.degree. C. optionally under pressure in an aliphatic chlorofluorine or fluorine substituted hydrocarbon containing up to 8 carbon atoms and having a boiling point of from -60.degree. to +50.degree. C. or in mixtures thereof having boiling ranges of from -60.degree. to +50.degree. C. and using a starter system comprising a hydroperoxide sulphur dioxide and an acid. The system may also contain aliphatic hydrocarbons in such quantities that a non-inflammable mixture is formed.

    Abstract translation: 本发明涉及一种生产聚丙烯腈或丙烯腈共聚物的方法，该聚合反应在-40℃至+ 60℃的温度下进行，任选在压力下进行，在含有最多8个碳原子的脂族氯氟氟或氟取代烃中 原子，沸点为-60℃至+ 50℃，或其沸点范围为-60至+50℃的混合物，并使用包含氢过氧化物二氧化硫和酸的起始系统。 该系统还可以含有以不可燃混合物形成的量的脂族烃。

    Polymerization process
    9.
    发明授权
    Polymerization process 失效
    聚合过程

    公开(公告)号：US4501865A

    公开(公告)日：1985-02-26

    申请号：US505655

    申请日：1983-06-20

    Applicant: Joachim Konig ,  Carlhans Suling ,  Siegfried Korte

    Inventor： Joachim Konig ,  Carlhans Suling ,  Siegfried Korte

    IPC: C08F2/00 ,  C08F2/16

    CPC classification number: C08F2/16 ,  C08F2/00

    Abstract: It is possible to remove quantities of heat from exothermically running polymerization reactions of vinyl monomers in heterogeneous phase, in a sophisticated manner by adding liquids to the reaction medium for the removal of heat and to regulate the reaction temperature, which liquids do not dissolve the polymer under the reaction conditions and the boiling temperatures of which are lower than or are identical to the technically predetermined reaction temperatures under the polymerization conditions which are applied, and the heat which is released in the reaction system is removed by evaporating these liquids.

    Abstract translation: 可以通过向反应介质中加入液体以除去热量并调节反应温度（这些液体不溶解聚合物），以复杂的方式从异构相中的乙烯基单体的放热运行的聚合反应中除去热量 在反应条件下，其沸点温度低于或等于在所施加的聚合条件下的技术上预定的反应温度，并且通过蒸发这些液体除去反应体系中释放的热量。

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