Trialkylsilylating agent and process for preparing N,N-disubstituted
aminotrialkylsilane using the same
    4.
    发明授权
    Trialkylsilylating agent and process for preparing N,N-disubstituted aminotrialkylsilane using the same 失效
    三烷基甲硅烷基化剂及使用其制备N,N-二取代氨基三烷基硅烷的方法

    公开(公告)号:US5227504A

    公开(公告)日:1993-07-13

    申请号:US882898

    申请日:1992-05-14

    IPC分类号: C07F7/02 C07F7/10

    CPC分类号: C07F7/10

    摘要: A silylating agent comprising an N-(trialkylsilyl)benzanilide having the following general formula: ##STR1## wherein R.sup.1 is a lower alkyl group. This agent is reacted with a secondary amine to produce an N,N-dialkylaminotrialkylsilane. This process is free of formation of amine hydrochlorides as by-products. Therefore, the problem associated with disposal of such amine hydrochlorides and the problem of limitations on the use of the silane compound product due to mixing of such amine hydrochlorides can be obviated effectively.

    摘要翻译: 甲硅烷基化剂,其包含具有以下通式的N-(三烷基甲硅烷基)-N-苯甲酰苯胺:其中R 1是低级烷基。 该试剂与仲胺反应以产生N,N-二烷基氨基三烷基硅烷。 该方法没有形成作为副产物的胺盐酸盐。 因此,与这种胺盐酸盐的处理相关的问题以及由于这种胺盐酸盐的混合而使用硅烷化合物产品的问题的问题可以有效地被消除。

    Thexyl trialkoxy silane
    5.
    发明授权
    Thexyl trialkoxy silane 失效
    THEXYL TRIALKOXY SILANE

    公开(公告)号:US5136073A

    公开(公告)日:1992-08-04

    申请号:US796360

    申请日:1991-11-22

    IPC分类号: C07F7/18

    CPC分类号: C07F7/1836

    摘要: Several thexyl trialkoxy silanes as a novel class of organosilicon compounds were synthesized by the reaction of dehydrochlorination condensation between thexyl trichlorosilane and an alcohol, e.g., methyl, ethyl, isopropyl and isobutyl alcohols, and characterized by the analytical data. These compounds are useful as an intermediate in the synthetic preparation of other organosilicon compounds, starting material of various silicones, surface-treatment agent of inorganic materials and additive in complex catalysts.

    Method for preparing hexamethylcyclotrisilazane
    6.
    发明授权
    Method for preparing hexamethylcyclotrisilazane 失效
    六甲基环三氮氮烷的制备方法

    公开(公告)号:US5245066A

    公开(公告)日:1993-09-14

    申请号:US933202

    申请日:1992-08-21

    IPC分类号: C07F7/21

    CPC分类号: C07F7/21

    摘要: Hexamethylcyclotrisilazane is prepared by reacting dimethyldichlorosilane with ammonia at a temperature between -20.degree. C. and 20.degree. C. Preferably, ammonia is blown into dimethyldichlorosilane at the temperature, and the reaction mixture is washed with 20% or higher alkaline water within one hour from the end of reaction for removing ammonium chloride by dissolving it in the water. Then hexamethylcyclotrisilazane of high purity is prepared in high yields. The method can be scaled up for commercial manufacture.

    摘要翻译: 六甲基环三硅氮烷通过二甲基二氯硅烷与氨在-20℃至20℃的温度下反应制备。优选在该温度下将氨吹入二甲基二氯硅烷中,并将反应混合物用20%或更高的碱性水在1小时内洗涤 通过将其溶解在水中来除去氯化铵的反应结束。 然后以高产率制备高纯度的六甲基环三硅氮烷。 该方法可以扩大到商业制造。

    Protective coat-forming coating composition, coated article, and multilayer laminate
    7.
    发明申请
    Protective coat-forming coating composition, coated article, and multilayer laminate 审中-公开
    保护涂层形成涂料组合物,涂覆制品和多层层压材料

    公开(公告)号:US20060240268A1

    公开(公告)日:2006-10-26

    申请号:US11454979

    申请日:2006-06-19

    IPC分类号: B32B17/10 B32B27/06 B32B9/04

    摘要: A coating composition primarily comprising a disilane compound of the formula (A): XmR13-mSi—Y—SiR13-mXm  (A) wherein R1 is a monovalent hydrocarbon group, Y is a divalent fluorinated organo group, X is a hydrolyzable group, and m is 1, 2 or 3, or a (partial) hydrolyzate thereof is applied and cured to form a protective coat having excellent chemical resistance and antireflection.

    摘要翻译: 主要包含式(A)的乙硅烷化合物的涂料组合物:<?in-line-formula description =“In-line formula”end =“lead”?> X&lt; (A)3-m Si-Y-SiR 1 - 3-m X(A) 其中R 1是一价烃基,Y是二价氟化有机基团,X是可水解的 基团,m为1,2或3,或其(部分)水解产物被施加和固化以形成具有优异的耐化学性和抗反射性的保护涂层。

    Aqueous coating composition
    9.
    发明授权
    Aqueous coating composition 失效
    水性涂​​料组合物

    公开(公告)号:US06656598B2

    公开(公告)日:2003-12-02

    申请号:US09973768

    申请日:2001-10-11

    IPC分类号: B32B904

    摘要: An aqueous coating composition including (A) an amino group-containing organopolysiloxane, (B) water and (C) at least one of a surface-active agent represented by the general formula (I): wherein R1 to R4are a C1-C8 alkyl group, R5 and R6 are a C1-C6 alkylene group, R7 and R8 are selected from a hydrogen atom, a C1-C6 alkyl group and a C2-C6 acyl group, and m and n are an integer of 0 to 40, provided that m and n are not 0 at the same time and that of m+n ranges from 1 to 40 on the average; and a nonionic surface-active agent containing a perfluoroalkyl group and an alkylene oxide group. In the composition, (C) is present in a content of 0.01% to 5% by weight based on the total of (A), (B) and (C), and an alcohol is present in an amount not more than 10% by weight of the composition. The aqueous coating composition has superior uniform-coating properties and storage stability.

    摘要翻译: 一种水性涂料组合物,其包含(A)含氨基的有机聚硅氧烷,(B)水和(C)由通式(I)表示的表面活性剂中的至少一种:其中R 1至R 4 >是C 1 -C 8烷基,R 5和R 6是C 1 -C 6亚烷基,R 7和R 8选自氢原子,C 1 -C 6烷基和 C2-C6酰基,m和n为0〜40的整数,条件是m和n不同时为0,m + n的平均值为1〜40; 和含有全氟烷基和环氧烷基的非离子表面活性剂。 在组合物中,(C)的含量相对于(A),(B)和(C)的总量为0.01〜5重量%,醇的含量不超过10重量% 的组合物。 水性涂​​料组合物具有优异的均匀涂布性能和储存稳定性。