摘要:
A process for producing a polyol by reacting an aliphatic aldehyde with formaldehyde in the presence of a basic catalyst, which comprises a step of concentration which comprises removing water and unreacted formaldehyde from a reaction liquid by distillation; a step of extraction which comprises extracting the polyol from a concentrated reaction liquid with an extracting reagent; a step of washing with water which comprises washing an extract liquid with water and separating the liquid into an oil layer containing the polyol and an aqueous layer; wherein by useing an specific aliphatic aldehyde as the extracting agent and recovering the extracting reagent from the oil layer containing the polyol after adjusting pH of the oil layer, a high purity polyhydric alcohol can be obtained at a high yield with suppressed formation of byproducts such as acetal compounds and aldol compounds.
摘要:
In the method of the present invention, a dimethylolcarboxylic acid is produced by reacting a trimethylolalkane and formaldehyde to prepare a cyclic formal having a formal protecting group, followed by the oxidation of the cyclic formal by using nitric acid as an oxidizing agent to prepare a cyclic carboxylic acid which is then subjected to cleavage to remove the formal protecting group. The formal protecting group protects two of the methylol groups against the oxidation to enable the production of the dimethylolcarboxylic acid with a high selectivity.
摘要:
In a cantilever which is used in a scanning probe microscope or the like and has a trapezoidal cross-sectional shape formed through anisotropic etching in a silicon process, a cantilever spring constant is determined without measuring a thickness directly. A cantilever thickness is determined based on upper base and lower base lengths of the trapezoidal cross-sectional shape and geometric regularity of a surface generated by the anisotropic etching. Then, the cantilever spring constant is determined based on the cantilever thickness, a cantilever length, and a Young's modulus.
摘要:
In detecting a displacement of a cantilever (2) by a displacement detecting mechanism (5) and allowing a probe (1) and a sample (8) to approach each other by at least one of a coarse-movement mechanism (13) and a vertical direction fine-movement mechanism (11) at the same time, an excitation mechanism (4) excites the cantilever (2) with a first excitation condition and the probe (1) and the sample (8) are allowed to approach each other with a first stop condition, and then the cantilever (2) is excited with a second excitation condition different from the first excitation condition, a second stop condition is set, and the probe (1) and the sample (8) are allowed to approach each other by the at least one of the vertical direction fine-movement mechanism (11) and the coarse-movement mechanism (13) until the second stop condition is satisfied.
摘要:
A method for producing flake-like dried DOG by making DOG containing from 10 to 50% by mass of a liquid go through a continuous melt-drying step of a specified condition and then making it go through, as a next step, a vacuum-drying step of a specified condition or a ventilation-drying step of a specified condition while holding a molten state thereof, to obtain DOG in which the liquid in DOG is reduced to not more than 0.5% by mass (dried DOG), and flaking the obtained dried DOG in a flake production step.
摘要:
A presentity service client has a presentity that issues presence information to a presence service and a watcher which observes presence information for other presentities; a presence change rule holding part holds a presence change rule; and a presence calculating part changes the presence information for the presentity, using as a trigger a change in presence information of other presentities, based on the presence information of other presentity acquired by the watcher and in accordance with the presence change rule held by a presence change rules holding part.
摘要:
When the status of a client X is changed to a status i, a group management unit generates a group agent Xi, corresponding to the status i and registers the generated group agent in the server S, and the presence issuing unit issues the status i and the identifier of the group agent Xi. Initially, a member management unit of the group agent xi manages the client X only. When other clients, such as clients B and C, that are observing the status of the client X send an instant message (IM) to the group agent Xi identified by the issued identifier, an IM delivery unit of the group agent Xi adds the clients B and C, which are IM senders, to the members managed by the member management unit and sends the IM to all members.
摘要:
A signal conversion circuit for converting an inputted differential signal into a single-ended signal comprises a differential amplifier circuit for amplifying the differential signal, and generating a first non-inverted signal and a first inverted signal being inverted the first non-inverted signal, a first inverter for generating a second non-inverted signal being inverted the first inverted signal and an interpolation unit for interpolating a phase difference between the first non-inverted signal and the second non-inverted signal.
摘要:
A PLL circuit according to an embodiment of the present invention includes: a first charge pump circuit to control an output current in accordance with an output signal of a phase comparator; an integrating filter to remove a predetermined frequency component; a second charge pump circuit to output a larger current than the first charge pump circuit in accordance with the output signal from the phase comparator; a ripple filter to remove a ripple component; a first voltage-current converting circuit to convert an output voltage from the integrating filter into a current; a second voltage-current converting circuit to convert an output voltage from the ripple filter into a current; and a current-controlled oscillator to control a frequency of output signal based on sum total of the output current from the first voltage-current converting circuit and the output current from the second voltage-current converting circuit.
摘要:
When the status of a client X is changed to a status i, a group management unit generates a group agent Xi, corresponding to the status i and registers the generated group agent in the server S, and the presence issuing unit issues the status i and the identifier of the group agent Xi. Initially, a member management unit of the group agent xi manages the client X only. When other clients, such as clients B and C, that are observing the status of the client X send an instant message (IM) to the group agent Xi identified by the issued identifier, an IM delivery unit of the group agent Xi adds the clients B and C, which are IM senders, to the members managed by the member management unit and sends the IM to all members.