Curable composition suitable as top coat and coated material using the
same
    1.
    发明授权
    Curable composition suitable as top coat and coated material using the same 失效
    适用作为外涂层和使用其的涂层材料的可固化组合物

    公开(公告)号:US5891958A

    公开(公告)日:1999-04-06

    申请号:US765366

    申请日:1997-01-08

    IPC分类号: C09D143/04 C08F8/00 C08L83/06

    CPC分类号: C09D143/04 Y10T428/31663

    摘要: A curable composition suitable as a top coat which contains a vinyl copolymer (A) having a main chain consisting of a vinyl copolymer chain, in which a reactive silyl group is combined with a carbon atom at the main chain end and/or side chain of the copolymer, the copolymer having an alcoholic hydroxyl group at its main chain end and/or side chain and having an alcoholic hydroxyl group equivalent of 400 to 2000 g/mole, a non-aqueous hydroxyl group-containing polymer dispersion (B), a silicon-containing compound and/or its partical hydrolysis condensation product (C), and a curing catalyst (D), wherein the amount of (B) is 5 to 100 parts by weight, in terms of solid matter, based on 100 parts by weight of (A), the amount of (C) is 2 to 100 parts by weight based on 100 parts by weight of (A), and the amount of (D) is 0.001 to 10 parts by weight based on 100 parts by weight of the total amount of solid matters of (A), (B) and (C), and a coated material using the same.

    摘要翻译: PCT No.PCT / JP96 / 01235 Sec。 371日期1997年1月8日 102(e)日期1997年1月8日PCT提交1996年5月9日PCT公布。 出版物WO96 / 35758 日期:1996年11月14日一种适用作为顶涂层的可固化组合物,其包含乙烯基共聚物(A),其具有由乙烯基共聚物链组成的主链,其中反应性甲硅烷基与主链端与碳原子结合, /或共聚物的侧链,所述共聚物在其主链端和/或侧链具有醇羟基,醇羟基当量为400至2000g / mol,非水羟基聚合物分散体 (B),含硅化合物和/或其分解水解缩合产物(C)和固化催化剂(D),其中(B)的量为固体成分为5〜100重量份, 基于100重量份(A),(C)的量为(A)100重量份为2〜100重量份,(D)的量为0.001〜10重量份, (A),(B)和(C)的固体成分总量的100重量份,以及使用其的涂布材料。

    Curable composition suitable as top coat
    2.
    发明授权
    Curable composition suitable as top coat 失效
    适合作为面漆的可固化组合物

    公开(公告)号:US5498666A

    公开(公告)日:1996-03-12

    申请号:US278340

    申请日:1994-07-21

    摘要: A curable composition suitable as top coats having an improved excellent acid resistance as well as excellent properties such as thermosetting property, appearance, water resistance, scratch resistance and weatherability, which comprises (A) a vinyl copolymer having a main chain substantially composed of a vinyl copolymer and having in its molecule both at least one hydrolyzable silyl group and at least one alcoholic hydroxyl group, (B) a silanol group-containing organopolysiloxne having at least one silanol group, and (C) a curing catalyst.

    摘要翻译: 适合作为顶涂层的可固化组合物具有改进的优异耐酸性以及优异的性能如热固性,外观,耐水性,耐擦伤性和耐候性,其包括(A)乙烯基共聚物,其主链基本上由乙烯基 共聚物,并且在其分子中具有至少一个可水解甲硅烷基和至少一个醇羟基,(B)具有至少一个硅烷醇基的含硅烷醇基的有机聚硅氧烷,和(C)固化催化剂。

    Curable composition for coatings, coated articles and resin composition for coatings
    3.
    发明授权
    Curable composition for coatings, coated articles and resin composition for coatings 失效
    涂料,涂料制品和涂料用树脂组合物的可固化组合物

    公开(公告)号:US06316572B1

    公开(公告)日:2001-11-13

    申请号:US09472189

    申请日:1999-12-27

    IPC分类号: C08G7704

    摘要: The present invention has its objects to provide a curable composition for coatings which can provide coatings or paint films excellent in acid resistance, scratch resistance, stain resistance and heat curability, with very good weather resistance and appearance; and coated articles and a resin composition obtained from the curable composition. The curable composition comprises: (A) a resin (A-1) obtained by mixing an epoxy group-containing compound (x) component and a carboxyl group-containing compound (y) component and/or a resin (A-2) based on an epoxy group-containing and carboxyl group-containing vinyl copolymer (z) component; (B) a vinyl copolymer whose main chain substantially consists of a vinyl copolymer chain and which has, within the molecule thereof, at least one hydrolyzable silyl group bound to a carbon atom as represented by the general formula (I): and (C) a silicon compound represented by the general formula (VII): (R3O)4−bSiR4b  (VII) and/or a partial hydrozylate condensate thereof.

    摘要翻译: 本发明的目的是提供一种能够提供耐酸性,耐擦伤性,耐污染性和热固化性优异的耐候性和外观的涂料或油漆膜的涂料用固化性组合物。 涂布制品和由可固化组合物获得的树脂组合物。 可固化组合物包含:(A)通过混合含环氧基化合物(x)组分和含羧基化合物(y)组分和/或树脂(A-2)基)得到的树脂(A-1) 含有环氧基和含羧基的乙烯基共聚物(z)组分; (B)乙烯基共聚物,其主链基本上由乙烯基共聚物链组成,并且在其分子内具有与通式(I)表示的碳原子结合的至少一个可水解甲硅烷基:和(C) 由通式(VII)表示的硅化合物:和/或其部分氢氯酸盐缩合物。

    Curable composition for coating, and articles coated with it
    4.
    发明授权
    Curable composition for coating, and articles coated with it 有权
    用于涂层的可固化组合物和用其涂覆的制品

    公开(公告)号:US06265470B1

    公开(公告)日:2001-07-24

    申请号:US09269962

    申请日:1999-04-08

    IPC分类号: C08K510

    摘要: The curable composition for coating of the invention comprises (A) 100 parts by weight of a resin having at least 2 epoxy groups in one molecule and having an epoxy equivalent of from 200 to 2,000 g/mol, and (B) from 0.001 to 100 parts by weight of a compound having at least 2 carboxyl groups in one molecule, in a molar ratio of the epoxy group to the carboxyl group (epoxy group/carboxyl group) of from 0.2/1 to 5.0/1, and contains (C) at least one organic solvent selected from glycol monoalkyl ethers, vinyl ethers and cyclic ethers, and at least one selected from monoalkyl alcohol compounds and compounds capable of giving alcohols through hydrolysis, each in an amount of from 1.0 to 50 parts by weight relative to 100 parts by weight of the total solid resin content of the composition. The composition has good storage stability and good thermal curability, and the coating films from it have good acid resistance, scratch resistance and weather resistance.

    摘要翻译: 本发明的涂布用固化性组合物包含(A)100重量份在一分子中具有至少2个环氧基的树脂,其环氧当量为200〜2000g / mol,(B)0.001〜100 重量份在一分子中具有至少2个羧基的化合物,环氧基与羧基(环氧基/羧基)的摩尔比为0.2 / 1至5.0 / 1,并含有(C) 选自二醇单烷基醚,乙烯基醚和环醚的至少一种有机溶剂,以及选自单烷基醇化合物和能够通过水解产生醇的化合物中的至少一种,其量相对于100重量份为1.0至50重量份 占组合物总固体树脂含量的重量份。 该组合物具有良好的储存稳定性和良好的热固化性,并且其涂膜具有良好的耐酸性,耐擦伤性和耐候性。

    Curable composition for top coating and articles coated therewith
    5.
    发明授权
    Curable composition for top coating and articles coated therewith 失效
    用于顶部涂层和涂覆的制品的可固化组合物

    公开(公告)号:US06255392B1

    公开(公告)日:2001-07-03

    申请号:US09297385

    申请日:1999-04-30

    IPC分类号: C08F3008

    摘要: A curable topcoat composition comprising (A) 100 to 30 parts by weight of a vinyl copolymer having a main chain substantially composed of a vinyl copolymer, having both at least one specific hydrolyzable silyl group and at least one hydroxyl group in its main chain end and/or side chain, and having a carbonato structure in its main chain and/or side chain, (B) 0.001 to 70 parts by weight of a hydroxyl group-containing compound having no hydrolyzable silyl group, and (C) a solvent, the total of the components (A) and (B) being 100 parts by weight. The coating films formed from the curable composition are excellent in acid resistance, scratch resistance, appearance and thermosetting property and, in particular, the composition can be suitably used as a top coat for automobiles.

    摘要翻译: 一种可固化面漆组合物,其包含(A)100至30重量份的具有主链基本上由乙烯基共聚物构成的乙烯基共聚物的乙烯基共聚物,其主链端具有至少一个特定的可水解甲硅烷基和至少一个羟基, /或侧链,其主链和/或侧链具有碳原子结构,(B)0.001〜70重量份的不含水解性甲硅烷基的含羟基化合物,(C)溶剂, 组分(A)和(B)的总计为100重量份。 由可固化组合物形成的涂膜具有优异的耐酸性,耐擦伤性,外观和热固性,并且特别地,该组合物可以适合用作汽车用顶涂层。

    Curable composition for top coating and articles coated using the same
    6.
    发明授权
    Curable composition for top coating and articles coated using the same 失效
    用于顶涂层的可固化组合物和使用其涂覆的制品

    公开(公告)号:US06265073B1

    公开(公告)日:2001-07-24

    申请号:US09242147

    申请日:1999-02-09

    IPC分类号: B32B2738

    摘要: The curable composition for coating of the invention comprises (A) 100 parts by weight of an epoxy group-having resin, (B) from 0.001 to 100 parts by weight of a carboxyl group-having compound or resin, and (C) from 1.0 to 100 parts by weight of a silicon compound of the following general formula (I) and/or its partially-hydrolyzed condensate: (R1O)4-aSiR2a  (I) wherein R1 represents a hydrogen atom, an alkyl group having from 1 to 10 carbon atoms, an aryl group having from 6 to 10 carbon atoms, or an aralkyl group having from 7 to 10 carbon atoms; R2 represents an alkyl group having from 1 to 10 carbon atoms, an aryl group having from 6 to 10 carbon atoms, an aralkyl group having from 7 to 10 carbon atoms, or an alkoxy group having from 1 to 10 carbon atoms; and a represents an integer of from 0 to 2. The composition has good thermal curability, and the coating films from the composition have excellent and well-balanced physical properties including excellent acid resistance, scratch resistance, weather resistance, appearance and recoating adhesiveness, and additionally have extremely excellent stain resistance.

    摘要翻译: 本发明的涂布用固化性组合物包含(A)100重量份的环氧基树脂,(B)0.001〜100重量份的含羧基化合物或树脂,(C)1.0 相对于100重量份的下述通式(I)的硅化合物和/或其部分水解缩合物:其中R1表示氢原子,具有1至10个碳原子的烷基,具有6个 至10个碳原子,或具有7至10个碳原子的芳烷基; R2表示碳原子数1〜10的烷基,碳原子数6〜10的芳基,碳原子数7〜10的芳烷基或碳原子数1〜10的烷氧基。 a表示0〜2的整数。该组合物具有良好的热固化性,并且来自该组合物的涂膜具有优异且平衡良好的物理性能,包括优异的耐酸性,耐刮擦性,耐候性,外观和重涂粘合性,以及 另外具有非常优异的耐污性。

    Method of inspecting secondary battery
    7.
    发明授权
    Method of inspecting secondary battery 有权
    检查二次电池的方法

    公开(公告)号:US09091733B2

    公开(公告)日:2015-07-28

    申请号:US13949272

    申请日:2013-07-24

    申请人: Seigo Nakamura

    发明人: Seigo Nakamura

    摘要: A method of inspecting a secondary battery includes: discharging the secondary battery initially charged, at a discharge current, from an initial voltage to a discharge ending voltage; calculating an interval capacity in a voltage interval from a check starting voltage to a check ending voltage, based on the discharge current, and discharge time taken in the voltage interval; measuring a voltage change amount from a point in time when the voltage reaches a first voltage to a point in time when a length of time elapses from the above point in time, when the secondary battery is discharged from the initial voltage to the discharge ending voltage; and determining whether a total capacity satisfies a performance requirement, by comparing the calculated interval capacity with a first threshold value, and determining whether an output satisfies a performance requirement, by comparing the measured voltage change amount with a second threshold value.

    摘要翻译: 检查二次电池的方法包括:以初始电压从放电电流初始充电的二次电池放电到放电结束电压; 根据放电电流计算从检查开始电压到检查结束电压的电压间隔的间隔容量,以及在电压间隔中取得的放电时间; 从电压达到第一电压的时间点到从上述时间点经过的时间长度的时间点,当二次电池从初始电压放电到放电结束电压时,测量电压变化量 ; 以及通过将所计算的间隔容量与第一阈值进行比较,并且通过将所测量的电压变化量与第二阈值进行比较来确定输出是否满足性能要求,来确定总容量是否满足性能要求。

    Method of manufacturing a semiconductor integrated circuit device and a method of manufacturing a thin film probe sheet for using the same
    8.
    发明授权
    Method of manufacturing a semiconductor integrated circuit device and a method of manufacturing a thin film probe sheet for using the same 有权
    半导体集成电路器件的制造方法以及使用该半导体集成电路器件的薄膜探针片的制造方法

    公开(公告)号:US08206997B2

    公开(公告)日:2012-06-26

    申请号:US12836580

    申请日:2010-07-15

    IPC分类号: H01L21/66 G01R31/26

    CPC分类号: G01R3/00 G01R1/07342

    摘要: A probe having a sufficient height is manufactured by selectively depositing, over the main surface of a wafer, a copper film in a region in which a metal film is to be formed and a region which will be outside an adhesion ring when a probe card is fabricated; forming the metal film, polyimide film, interconnect, another polyimide film, another interconnect and a further polyimide film; and then removing the wafer and copper film. According to the present invention, when probe testing is performed using a prober (thin film probe) having the probe formed in the above-described manner while utilizing the manufacturing technology of semiconductor integrated circuit devices, it is possible to prevent breakage of the prober and a wafer to be tested.

    摘要翻译: 通过选择性地在晶片的主表面上沉积在要形成金属膜的区域中的铜膜和当探针卡是在粘合环外部时将在粘合环外部的区域,制造具有足够高度的探针 制造的 形成金属膜,聚酰亚胺膜,互连,另一聚酰亚胺膜,另一互连和另外的聚酰亚胺膜; 然后取出晶片和铜膜。 根据本发明,在利用半导体集成电路器件的制造技术的情况下,使用具有以上述方式形成的探针的探测器(薄膜探针)进行探针测试时,可以防止探测器的破损, 待测试的晶圆。

    METHOD OF MANUFACTURING A SEMICONDUCTOR INTEGRATED CIRCUIT DEVICE AND A METHOD OF MANUFACTURING A THIN FILM PROBE SHEET FOR USING THE SAME
    9.
    发明申请
    METHOD OF MANUFACTURING A SEMICONDUCTOR INTEGRATED CIRCUIT DEVICE AND A METHOD OF MANUFACTURING A THIN FILM PROBE SHEET FOR USING THE SAME 有权
    制造半导体集成电路装置的方法和制造薄膜探针片的方法

    公开(公告)号:US20080160657A1

    公开(公告)日:2008-07-03

    申请号:US11958369

    申请日:2007-12-17

    IPC分类号: H01L21/66 H01L21/308

    CPC分类号: G01R3/00 G01R1/07342

    摘要: A probe having a sufficient height is manufactured by selectively depositing, over the main surface of a wafer, a copper film in a region in which a metal film is to be formed and a region which will be outside an adhesion ring when a probe card is fabricated; forming the metal film, polyimide film, interconnect, another polyimide film, another interconnect and a further polyimide film; and then removing the wafer and copper film. According to the present invention, when probe testing is performed using a prober (thin film probe) having the probe formed in the above-described manner while utilizing the manufacturing technology of semiconductor integrated circuit devices, it is possible to prevent breakage of the prober and a wafer to be tested.

    摘要翻译: 通过选择性地在晶片的主表面上沉积在要形成金属膜的区域中的铜膜和当探针卡是在粘合环外部时将在粘合环外部的区域,制造具有足够高度的探针 制造的 形成金属膜,聚酰亚胺膜,互连,另一聚酰亚胺膜,另一互连和另外的聚酰亚胺膜; 然后取出晶圆和铜膜。 根据本发明,在利用半导体集成电路器件的制造技术的情况下,使用具有以上述方式形成的探针的探测器(薄膜探针)进行探针测试时,可以防止探测器的破损, 待测试的晶圆。