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公开(公告)号：US06946582B2
公开(公告)日：2005-09-20
申请号：US10498933
申请日：2002-11-20
申请人： Toshiyuki Katsube , Kouzou Noda , Jun Miki
发明人： Toshiyuki Katsube , Kouzou Noda , Jun Miki
IPC分类号： C07B61/00 , C07C17/08 , C07C17/087 , C07C19/16 , C07C67/11 , C07C69/653 , C07C21/18 , C07C69/66
CPC分类号： C07C17/087 , C07C17/08 , C07C67/11 , Y02P20/582 , C07C19/16 , C07C69/653
摘要： The present invention provides a process for producing a fluoroalkyl iodide represented by the general formula (II): Rf-CH2CH2I (II) wherein Rf is a perfluoroalkyl or polyfluoroalkyl group comprising 1 to 20 carbons, the process comprising reacting hydrogen iodide gas with a fluoroalkene in the presence of a catalyst. The present invention also provides a process for producing a fluoroester by reacting the fluoroalkyl iodide with a carboxylate.
摘要翻译： 本发明提供一种由通式（II）表示的氟代烷基碘的制备方法：<？in-line-formula description =“In-line formula”end =“lead”？> Rf-CH 2 其中Rf是包含1至20个全氟烷基或多氟烷基的全氟烷基或多氟烷基， 碳，该方法包括在催化剂存在下使碘化氢气体与氟代烯烃反应。 本发明还提供了通过氟代烷基碘与羧酸酯反应制备氟酯的方法。
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公开(公告)号：US20050090699A1
公开(公告)日：2005-04-28
申请号：US10498933
申请日：2002-11-20
申请人： Toshiyuki Katsube , Kouzou Noda , Jun Miki
发明人： Toshiyuki Katsube , Kouzou Noda , Jun Miki
IPC分类号： C07B61/00 , C07C17/08 , C07C17/087 , C07C19/16 , C07C67/11 , C07C69/653 , C07C19/07 , C07C19/08
CPC分类号： C07C17/087 , C07C17/08 , C07C67/11 , Y02P20/582 , C07C19/16 , C07C69/653
摘要： The present invention provides a process for producing a fluoroalkyl iodide represented by the general formula (II): Rf—CH2CH2I (II) wherein Rf is a perfluoroalkyl or polyfluoroalkyl group comprising 1 to 20 carbons, the process comprising reacting hydrogen iodide gas with a fluoroalkene in the presence of a catalyst. The present invention also provides a process for producing a fluoroester by reacting the fluoroalkyl iodide with a carboxylate.
摘要翻译： 本发明提供一种由通式（II）表示的氟代烷基碘的制备方法：<？in-line-formula description =“In-line formula”end =“lead”？> Rf-CH 2 其中Rf是包含1至20个全氟烷基或多氟烷基的全氟烷基或多氟烷基， 碳，该方法包括在催化剂存在下使碘化氢气体与氟代烯烃反应。 本发明还提供了通过氟代烷基碘与羧酸酯反应制备氟酯的方法。
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公开(公告)号：US07098166B2
公开(公告)日：2006-08-29
申请号：US11028327
申请日：2005-01-04
申请人： Toshiyuki Katsube , Yuuki Matsuda , Jun Miki
发明人： Toshiyuki Katsube , Yuuki Matsuda , Jun Miki
CPC分类号： B01J29/85 , B01J29/064 , B01J29/072 , B01J29/83 , C07C29/124 , C07C31/38
摘要： A process for preparing a fluorine-containing alcohol compound, the process comprising the step of reacting water with a halogenated fluorine compound in the presence of a catalyst for preparing a fluorine-containing alcohol compound, the catalyst obtained by supporting an ammine complex containing at least one component selected from the group consisting of the elements in Group 1B, Group 2B, Group 6A, Group 7A and Group 8 of the periodic table on at least one complex oxide selected from the group consisting of Si—Al complex oxides, Al—P complex oxides and Si—Al—P complex oxides.
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4.发明申请公开(公告)号：US20050119511A1
公开(公告)日：2005-06-02
申请号：US11028327
申请日：2005-01-04
申请人： Toshiyuki Katsube , Yuuki Matsuda , Jun Miki
发明人： Toshiyuki Katsube , Yuuki Matsuda , Jun Miki
IPC分类号： B01J29/064 , B01J29/072 , B01J29/83 , B01J29/85 , C07B61/00 , C07C29/124 , C07C31/38 , C07C29/00
CPC分类号： B01J29/85 , B01J29/064 , B01J29/072 , B01J29/83 , C07C29/124 , C07C31/38
摘要： A process for preparing a fluorine-containing alcohol compound, the process comprising the step of reacting water with a halogenated fluorine compound in the presence of a catalyst for preparing a fluorine-containing alcohol compound, the catalyst obtained by supporting an ammine complex containing at least one component selected from the group consisting of the elements in Group 1B, Group 2B, Group 6A, Group 7A and Group 8 of the periodic table on at least one complex oxide selected from the group consisting of Si—Al complex oxides, Al—P complex oxides and Si—Al—P complex oxides.
摘要翻译： 一种制备含氟醇化合物的方法，该方法包括在用于制备含氟醇化合物的催化剂存在下使水与卤代氟化合物反应的步骤，所述催化剂通过将至少含有至少 选自元素周期表第1B族，第2B族，第6A族，第7A族和第8族元素中的至少一种选自Si-Al复合氧化物，Al-P 复合氧化物和Si-Al-P复合氧化物。
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5.发明授权公开(公告)号：US06855662B2
公开(公告)日：2005-02-15
申请号：US10242688
申请日：2002-09-13
申请人： Toshiyuki Katsube , Yuuki Matsuda , Jun Miki
发明人： Toshiyuki Katsube , Yuuki Matsuda , Jun Miki
IPC分类号： B01J29/064 , B01J29/072 , B01J29/83 , B01J29/85 , C07B61/00 , C07C29/124 , C07C31/38 , B01J27/13
CPC分类号： B01J29/85 , B01J29/064 , B01J29/072 , B01J29/83 , C07C29/124 , C07C31/38
摘要： A catalyst for preparing a fluorine-containing alcohol compounds, the catalyst is obtained by supporting an ammine complex containing at least one component selected from the group consisting of the elements in Group 1B, Group 2B, Group 6A, Group 7A and Group 8 of the periodic table on at least one complex oxide selected from the group consisting of Si—Al complex oxide, Al—P complex oxides and Si—Al—P complex oxides.
摘要翻译： 一种制备含氟醇化合物的催化剂，该催化剂通过将含有至少一种选自组1B，组2B，组6A，组7A和组8中的元素的组分的氨络合物 选自由Si-Al复合氧化物，Al-P复合氧化物和Si-Al-P复合氧化物组成的组中的至少一种复合氧化物的周期表。
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公开(公告)号：US06313357B1
公开(公告)日：2001-11-06
申请号：US09444401
申请日：1999-11-22
IPC分类号： C07C3134
CPC分类号： B01D61/362 , B01D61/364 , C07C29/76 , C07C29/82 , C07C31/38
摘要： In a method for recovering a fluoroalcohol from a mixture comprising a fluoroalcohol and water, (i) a method for recovering a fluoroalcohol by distilling the mixture comprising the fluoroalcohol and water to separate water as an azeotropic or azeotrope-like composition; and (ii) a method for recovering a fluoroalcohol, wherein water is separated by pervaporation.
摘要翻译： 在从包含氟代醇和水的混合物中回收氟代醇的方法中，（i）通过将包含氟代醇和水的混合物蒸馏以分离作为共沸或类共沸组合物的水来回收氟代醇的方法; 和（ii）回收氟代醇的方法，其中水通过渗透蒸发分离。
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公开(公告)号：US06245953B1
公开(公告)日：2001-06-12
申请号：US09444402
申请日：1999-11-22
IPC分类号： C07C2976
摘要： In a method for recovering a fluorine-containing solvent from the mixture comprising the fluorine-containing solvent and dyes, (i) a method for recovering a fluorine-containing solvent by distillation; and (ii) a method for recovering a fluorine-containing solvent comprising the steps of adding to the mixture the second solvent which uniformly mixes with the fluorine-containing solvent but does not dissolve the dyes; separating a precipitate from the resulting mixture; and separating the second solvent.
摘要翻译： 在由含氟溶剂和染料的混合物中回收含氟溶剂的方法中，（i）通过蒸馏回收含氟溶剂的方法; 和（ii）回收含氟溶剂的方法，包括以下步骤：向混合物中加入与含氟溶剂均匀混合但不溶解染料的第二溶剂; 从所得混合物中分离出沉淀物; 并分离第二溶剂。
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公开(公告)号：US06187969B1
公开(公告)日：2001-02-13
申请号：US09394679
申请日：1999-09-13
IPC分类号： C07C2900
摘要： A process for producing a fluoroalcohol of the following formula (1) H(CFR1CF2)nCH2OH (1) (n=1 or 2, wherein R1 represents F or CF3 when n=1; R1 represents F when n=2) comprising reacting methanol with tetrafluoroethylene or hexafluoropropylene in the presence of an initiator wherein the fluoroalcohol of formula (1) is distilled after decomposing the remaining initiator contained in the reaction mixture.
摘要翻译： 一种制备下式（1）的氟代醇的方法（n = 1或2，当n = 1时，R1表示F或CF3;当n = 2时，R1表示F），包括使甲醇与四氟乙烯或六氟丙烯反应， 其中在分解反应混合物中所含的剩余引发剂之后蒸馏出式（1）的氟代醇的引发剂。
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