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    Preparation of 2,4,6-trimethylbenzoic acid
    1.
    发明授权
    Preparation of 2,4,6-trimethylbenzoic acid 失效
    制备2,4,6-三甲基苯甲酸

    公开(公告)号：US5296636A

    公开(公告)日：1994-03-22

    申请号：US10058

    申请日：1993-01-28

    申请人： Wolfgang Siegel ,  Rudolf Kropp ,  Jochen Schroeder

    发明人： Wolfgang Siegel ,  Rudolf Kropp ,  Jochen Schroeder

    IPC分类号： C07C45/46 ,  C07C51/29 ,  C07C51/16 ,  C07C45/00

    CPC分类号： C07C45/46 ,  C07C51/29

    摘要： A process for the preparation of 2,4,6-trimethylbenzoic acid of the formula I ##STR1## in which .alpha.-chloro-2,4,6-trimethylacetophenone is reacted with an alkali hydroxide solution and chlorine in the presence of a phase-transfer catalyst at a temperature ranging from 0.degree. to 150.degree. C. and a pressure ranging from 0.01 to 50 bar, and a process for the preparation of 2,4,6-trimethylbenzoic acid I, in which .alpha.-chloro-2.4.6-trimethylacetophenone of the formula II ##STR2## is reacted with 1,3,5-trimethylbenzene and chloroacetyl chloride in the presence of a catalyst at a temperature ranging from 0.degree. to 150.degree. C. and a pressure ranging from 0.01 to 50 bar, the catalyst used being an iron oxide.

    摘要翻译： 制备式I的2,4,6-三甲基苯甲酸（I）的方法，其中α-氯-2,4,6-三甲基苯乙酮与碱金属氢氧化物溶液和氯在存在下反应 在0〜150℃的温度和0.01〜50巴的压力范围内的相转移催化剂，以及制备2,4,6-三甲基苯甲酸I的方法，其中α-氯 - 在催化剂存在下，在0℃至150℃的温度范围内，使式II（II）的2.4.6-三甲基苯乙酮与1,3,5-三甲基苯和氯乙酰氯反应， 使用的催化剂为0.01至50巴，所述催化剂为氧化铁。

    Process for preparation of arenebisphosphine oxides
    4.
    发明授权
    Process for preparation of arenebisphosphine oxides 失效
    芳烃二氧化膦的制备方法

    公开(公告)号：US5410060A

    公开(公告)日：1995-04-25

    申请号：US160153

    申请日：1993-12-02

    申请人： Jochen Schroeder ,  Wolfgang Siegel ,  Matthias Lokai

    发明人： Jochen Schroeder ,  Wolfgang Siegel ,  Matthias Lokai

    IPC分类号： A61K6/083 ,  A61K6/00 ,  C07F9/32 ,  C07F9/40 ,  C07F9/53 ,  C07F9/6571 ,  C07F9/6574 ,  C08F2/50 ,  C09D4/00 ,  C09D5/34 ,  C09D11/101 ,  C09J4/00 ,  G03F7/028 ,  G03F7/029 ,  C07F9/30

    CPC分类号： G03F7/029 ,  A61K6/0052 ,  C07F9/3252 ,  C07F9/4065 ,  C07F9/5337 ,  C07F9/657181 ,  C08F2/50 ,  C09D11/101 ,  C09D4/00 ,  C09D5/34 ,  C09J4/00

    摘要： Arenebisphosphine oxides of the general formula ##STR1## where R.sup.1 to R.sup.4 independently of one another are each hydrogen, C.sub.1 -C.sub.6 -alkyl, C.sub.1 -C.sub.6 -alkoxy, C.sub.5 -C.sub.10 -aryl, C.sub.5 -C.sub.12 -aryloxy or C.sub.7-C.sub.14 -arylalkoxy, R.sup.5 and R.sup.6 independently of one another may each be C.sub.1 -C.sub.6 -alkyl, C.sub.5 -C.sub.10 -cycloalkyl or C.sub.5 -C.sub.12 -aryl, each of which may furthermore contain one or two nitrogen or sulfur atoms in the ring system or carry one or two halogen atoms or C.sub.1 -C.sub.6 -alkyl or C.sub.1 -C.sub.6 -alkoxy groups as substituent on the ring system, or C.sub.1 -C.sub.6 -alkoxy, C.sub.3 -C.sub.8 -alkoxyalkoxy, C.sub.5 -C.sub.12 -aryloxy or C.sub.7 -C.sub.14 -arylalkoxy, or R.sup.5 and R.sup.6 together form a bridge of 2 to 10 carbon atoms, in which some of the carbon atoms may furthermore be part of an aromatic ring.

    摘要翻译： 其中R 1至R 4彼此独立的通式为：其中R 1至R 4各自为氢，C 1 -C 6 - 烷基，C 1 -C 6 - 烷氧基，C 5 -C 10 - 芳基，C 5 -C 12 - 芳氧基或C 7 -C 14 - 芳基烷氧基，R 5和R 6彼此独立地各自可以是C 1 -C 6 - 烷基，C 5 -C 10 - 环烷基或C 5 -C 12 - 芳基，其中每一个还可以在环系中含有一个或两个氮原子或硫原子或携带一个 或两个卤素原子或作为取代基的C 1 -C 6 - 烷基或C 1 -C 6 - 烷氧基，或C 1 -C 6 - 烷氧基，C 3 -C 8 - 烷氧基烷氧基，C 5 -C 12 - 芳氧基或C 7 -C 14 - 芳基烷氧基，或 R5和R6一起形成2至10个碳原子的桥，其中一些碳原子还可以是芳环的一部分。

    Preparation of polyacylated aromatric compounds
    5.
    发明授权
    Preparation of polyacylated aromatric compounds 失效
    多酰化芳香化合物的制备

    公开(公告)号：US5395975A

    公开(公告)日：1995-03-07

    申请号：US158788

    申请日：1993-12-01

    申请人： Wolfgang Siegel ,  Jochen Schroeder

    发明人： Wolfgang Siegel ,  Jochen Schroeder

    IPC分类号： B01J23/06 ,  B01J23/28 ,  B01J23/745 ,  C07B61/00 ,  C07C45/45 ,  C07C45/46 ,  C07C49/784 ,  C07C49/80 ,  C07C49/813 ,  C07C205/45 ,  C08G65/40

    CPC分类号： C07C201/12 ,  C07C45/46 ,  C08G65/40

    摘要： Polyacylated aromatic compounds of formula I ##STR1## where R.sup.1 is phenyl which is unsubstituted or has inert substituents or is .alpha.-halo-C.sub.1 -C.sub.6 -alkyl, it being possible for these radicals to be identical or different;R.sup.2 is C.sub.1 -C.sub.4 -alkyl;m is 2 or 3;n is 0 to 4, it being possible for the R.sup.2 substituents to be different when n>1,with the proviso that m+n.ltoreq.6, are prepared by reacting an acylaromatic compound of the formula II ##STR2## where p is 1 or 2, with a carbonyl halide of the formula III ##STR3## where X is halogen, in an amount appropriate for the desired degree of acylation, in the presence of Fe(II), Fe(III), Zn(II), Mo(VI), W(VI) or Sn(IV) compounds.

    摘要翻译： 式I的多酰化芳族化合物其中R 1是未被取代或具有惰性取代基或是α-卤代-C 1 -C 6 - 烷基的苯基，这些基团可能是相同或不同的; R2是C1-C4-烷基; m为2或3; n为0至4，当n> 1时，R2取代基可能不同，条件是m + n = 6，通过使式II的酰基芳族化合物II，其中p 在Fe（II），Fe（III），Zn（II）的存在下，具有式III的酰卤，其中X是卤素，其量适于所需的酰化度。 ），Mo（VI），W（VI）或Sn（IV）化合物。

    Process for Manufacturing Substituted 3-pyridylmethyl Ammonium Bromides
    7.
    发明申请
    Process for Manufacturing Substituted 3-pyridylmethyl Ammonium Bromides 有权
    制备取代的3-吡啶基甲基溴化铵的方法

    公开(公告)号：US20110224433A1

    公开(公告)日：2011-09-15

    申请号：US13128787

    申请日：2009-11-13

    申请人： Joachim Gebhardt ,  Frederik Menges ,  Michael Rack ,  Michael Keil ,  Jochen Schroeder ,  Stefan Orsten ,  Helmut Zech ,  David Cortes ,  Robert Leicht ,  Tony Yegerlehner ,  Rodney F. Klima

    发明人： Joachim Gebhardt ,  Frederik Menges ,  Michael Rack ,  Michael Keil ,  Jochen Schroeder ,  Stefan Orsten ,  Helmut Zech ,  David Cortes ,  Robert Leicht ,  Tony Yegerlehner ,  Rodney F. Klima

    IPC分类号： C07D251/00 ,  C07D213/80 ,  C07D237/00 ,  C07D241/00 ,  C07D401/04

    CPC分类号： C07D401/04 ,  C07D213/80 ,  C07D401/06 ,  C07D403/06 ,  C07D413/06 ,  C07D417/06

    摘要： A process for manufacturing 5,6-disubstituted-3-pyridylmethyl ammonium bromides (I), wherein Q is a tertiary aliphatic or cyclic, saturated, partially unsaturated or aromatic amine; Z is hydrogen or halogen; Z1 is hydrogen, halogen, cyano or nitro; Y and Y1 are each independently OR1, NR1R2, or when taken together YY1 is —O—, —S— or NR3—; R1 and R2 are each independently hydrogen, C1-C4 alkyl optionally substituted with C1-C4 alkoxy or phenyl optionally substituted with one to three C1-C4 alkyl groups, C1-C4 alkoxy groups or halogen atoms, or phenyl optionally substituted with one to three C1-C4 alkyl groups, C1-C4 alkoxy groups or halogen atoms; R3 is hydrogen or C1-C4 alkyl; comprises the steps of (i) reacting a compound of formula (II), wherein the symbols have the meaning given in formula (I), with bromine in the presence of a radical initiator in a solvent mixture comprising an aqueous phase and an organic phase, where the organic phase comprises a solvent selected from 1,2-dichloroethane, chlorobenzene, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene and tetrachloromethane, and where the pH-value of the aqueous phase is from 3 to

    摘要翻译： 制备5,6-二取代-3-吡啶基甲基溴化铵（I）的方法，其中Q是叔脂族或环状饱和的，部分不饱和的或芳族的胺; Z是氢或卤素; Z1是氢，卤素，氰基或硝基; Y和Y1各自独立地为OR 1，NR 1 R 2，或者当Y Y 1为-O - ， - S-或NR 3 - 时。 R 1和R 2各自独立地为氢，任选被C 1 -C 4烷氧基取代的C 1 -C 4烷基或任选被一至三个C 1 -C 4烷基，C 1 -C 4烷氧基或卤素原子取代的苯基，或任选被一至三个 C1-C4烷基，C1-C4烷氧基或卤原子; R3是氢或C1-C4烷基; 包括以下步骤：（i）在自由基引发剂存在下，将包含式（I）中给出的符号的式（II）化合物与溴在含水相和有机相的溶剂混合物中反应， 其中有机相包含选自1,2-二氯乙烷，氯苯，1,2-二氯苯，1,3-二氯苯，1,4-二氯苯和四氯甲烷的溶剂，其中水相的pH值来自 3至<8，得到3-溴甲基-5,6-二取代的吡啶化合物（III），其中Y，Y 1，Z和Z 1具有式（I）中给出的含义，和（ⅱ）使溴化合物 式（III）与叔胺碱Q在溶剂中在约0℃至100℃的温度范围内

    Process for manufacturing substituted 3-pyridylmethyl ammonium bromides
    8.
    发明授权
    Process for manufacturing substituted 3-pyridylmethyl ammonium bromides 有权
    制备取代的3-吡啶基甲基溴化铵的方法

    公开(公告)号：US09096570B2

    公开(公告)日：2015-08-04

    申请号：US13128787

    申请日：2009-11-13

    申请人： Joachim Gebhardt ,  Frederik Menges ,  Michael Rack ,  Michael Keil ,  Jochen Schroeder ,  Stefan Orsten ,  Helmut Zech ,  David Cortes ,  Robert Leicht ,  Tony Yegerlehner ,  Rodney F. Klima

    发明人： Joachim Gebhardt ,  Frederik Menges ,  Michael Rack ,  Michael Keil ,  Jochen Schroeder ,  Stefan Orsten ,  Helmut Zech ,  David Cortes ,  Robert Leicht ,  Tony Yegerlehner ,  Rodney F. Klima

    IPC分类号： C07D401/06 ,  C07D403/06 ,  C07D413/06 ,  C07D417/06 ,  C07D213/80 ,  C07D401/04

    CPC分类号： C07D401/04 ,  C07D213/80 ,  C07D401/06 ,  C07D403/06 ,  C07D413/06 ,  C07D417/06

    摘要： A process for manufacturing 5,6-disubstituted-3-pyridylmethyl ammonium bromides (I), wherein Q is a tertiary aliphatic or cyclic, saturated, partially unsaturated or aromatic amine; Z is hydrogen or halogen; Z1 is hydrogen, halogen, cyano or nitro; Y and Y1 are each independently OR1, NR1R2, or when taken together YY1 is —O—, —S— or NR3—; R1 and R2 are each independently hydrogen, C1-C4 alkyl optionally substituted with C1-C4 alkoxy or phenyl optionally substituted with one to three C1-C4 alkyl groups, C1-C4 alkoxy groups or halogen atoms, or phenyl optionally substituted with one to three C1-C4 alkyl groups, C1-C4 alkoxy groups or halogen atoms; R3 is hydrogen or C1-C4 alkyl; comprises the steps of (i) reacting a compound of formula (II), wherein the symbols have the meaning given in formula (I), with bromine in the presence of a radical initiator in a solvent mixture comprising an aqueous phase and an organic phase, where the organic phase comprises a solvent selected from 1,2-dichloroethane, chlorobenzene, 1,2-dichlorobenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene and tetrachloromethane, and where the pH-value of the aqueous phase is from 3 to

    摘要翻译： 制备5,6-二取代-3-吡啶基甲基溴化铵（I）的方法，其中Q是叔脂族或环状饱和的，部分不饱和的或芳族的胺; Z是氢或卤素; Z1是氢，卤素，氰基或硝基; Y和Y1各自独立地为OR 1，NR 1 R 2，或者当Y Y 1为-O - ， - S-或NR 3 - 时。 R 1和R 2各自独立地为氢，任选被C 1 -C 4烷氧基取代的C 1 -C 4烷基或任选被一至三个C 1 -C 4烷基，C 1 -C 4烷氧基或卤素原子取代的苯基，或任选被一至三个 C1-C4烷基，C1-C4烷氧基或卤原子; R3是氢或C1-C4烷基; 包括以下步骤：（i）在自由基引发剂存在下，将包含式（I）中给出的符号的式（II）化合物与溴在含水相和有机相的溶剂混合物中反应， 其中有机相包含选自1,2-二氯乙烷，氯苯，1,2-二氯苯，1,3-二氯苯，1,4-二氯苯和四氯甲烷的溶剂，其中水相的pH值来自 3至<8，得到3-溴甲基-5,6-二取代的吡啶化合物（III），其中Y，Y 1，Z和Z 1具有式（I）中给出的含义，和（ⅱ）使溴化合物 式（III）与叔胺碱Q在溶剂中在约0℃至100℃的温度范围内

    Circuit for motor vehicles with coding plug
    9.
    发明授权
    Circuit for motor vehicles with coding plug 有权

    公开(公告)号：US07129716B2

    公开(公告)日：2006-10-31

    申请号：US11336932

    申请日：2006-01-23

    申请人： Jochen Schroeder

    发明人： Jochen Schroeder

    IPC分类号： G01R27/08 ,  G06F7/00 ,  H01R27/02

    CPC分类号： H01R13/665 ,  H01R2201/26

    摘要： A circuit arrangement for motor vehicles for characterizing one of several variants of an electrically controllable subassembly is provided. A subassembly is connectable to a coding plug. The coding plug has at least one electric terminal which is directly or indirectly connectable to a measurement input of an analyzer unit. The coding plug has fixed electric wiring by means of which a defined electric state may be generated at the measurement input in the analyzer unit. The electric state is detected in the analyzer unit and compared with stored data, by means of which a defined electric state that can be differentiated from all other states is assigned to each possible variant of the subassembly.

    Circuit for motor vehicles with coding plug
    10.
    发明申请
    Circuit for motor vehicles with coding plug 有权
    带编码插头的汽车电路

    公开(公告)号：US20060119370A1

    公开(公告)日：2006-06-08

    申请号：US11336932

    申请日：2006-01-23

    申请人： Jochen Schroeder

    发明人： Jochen Schroeder

    IPC分类号： G01R27/08

    CPC分类号： H01R13/665 ,  H01R2201/26

    摘要： A circuit arrangement for motor vehicles for characterizing one of several variants of an electrically controllable subassembly is provided. A subassembly is connectable to a coding plug. The coding plug has at least one electric terminal which is directly or indirectly connectable to a measurement input of an analyzer unit. The coding plug has fixed electric wiring by means of which a defined electric state may be generated at the measurement input in the analyzer unit. The electric state is detected in the analyzer unit and compared with stored data, by means of which a defined electric state that can be differentiated from all other states is assigned to each possible variant of the subassembly.

    摘要翻译： 提供了用于表征电子可控子组件的几种变型之一的用于机动车辆的电路装置。 子组件可连接到编码插头。 编码插头具有至少一个电端子，其直接或间接地连接到分析器单元的测量输入端。 编码插头具有固定的电线，通过该布线可以在分析器单元中的测量输入处产生限定的电状态。 在分析器单元中检测电状态并将其与存储的数据进行比较，通过该状态，可以将与所有其他状态区分的定义的电状态分配给子组件的每个可能的变型。